Professional Documents
Culture Documents
i hc Nng - 2008
1. M U Thuc l c s vt cht iu tr v d phng cc bnh tt. c tnh ca thuc c lin quan ti l ho tnh v cu trc ho hc ca thuc, ch cn mt vi thay i nh trong cu trc ho hc ca thuc c th nh hng ln n hot tnh ca thuc v lm thay i tc dng ca thuc trong c th. V vy, vic s dng thuc v bo qun thuc, c bit l vic bo qun thuc l rt quan trng v lun c ch trng. Cu hi t ra l lm sao c th bo qun thuc lu di m khng lm thay i cht lng cng nh tc dng ca thuc? Cng tc kim nghim cht lng ca thuc l rt quan trng. Hin ny, vi s tin b ca KHKT c rt nhiu phng php kim nghim khc nhau. Mt trong s c s dng rng ri nht l phng php quang ph hp th UV-Vis. i tng kho st y rt a dng, c mt s cng trnh tin hnh kho st c s nh hng ca cc yu t nh: nhit , m, nh sng n vic bo qun thuc. Vi nh sng th ch gii hn nh sng kh kin. Vy liu nh sng t ngoi c nh hng g n cu to v thnh phn ca thuc khng? Khi m nh sng mt tri chiu ti tri t c thm thnh phn ny do l thng tng zn. Vi iu kin hin c ca Phng th nghim chuyn Khoa Vt L Trng i hc S phm, chng ti tin hnh kho st nh hng ca nhit v nh sng t ngoi n ph hp th ca mt s thuc tn dc, qua rt ra c mt s cc kt lun cn thit cho vic bo qun mt s tn dc. chnh l l do chng ti chn ti: Nghin cu tc ng ca nh sng c nng lng ln v nhit cao ln mt s thuc tn dc 2. PHNG PHP V VT LIU Phng php quang ph hp th UV-Vis l mt trong nhng phng php phn tch da trn s hp th bc x in t c bc sng nm trong vng t ngoi gn (200 400nm) v trong vng kh kin (400 700nm). y cng l mt phng php hin i c p dng rng ri trong nhiu lnh vc. Phng php ny c s tr gip ca my quang ph hai chm tia SPECTROSCAN - 80DV, kt qu ph hp th ca cc cht kho st c hin th ngay trn mn hnh vi tnh.
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i hc Nng - 2008
Vic x l ph rt thun tin vi phn mm UVWin tin tin cho php thc hin nhiu chc nng cng mt lc. Ph hp th thng c biu din di dng mt ng cong cho thy s ph thuc hp th ca mt cht bt k trng thi dung dch vo bc sng ca nh sng chiu ti. Mi ng cong nh th c c trng bi bc sng max m ti s hp th l ln nht. phn tch s nh hng ca cc tc nhn bn ngoi ti cht m ta kho st thng qua ph hp th ca chng, ta tin hnh o ph hp th trc v sau khi x l, sau so snh s thay i ca cc nh ph v rt ra cc kt lun cn thit. Vt liu kho st trong ti l Calcium corbire. y l loi thuc b sung calci, thnh phn chnh l calcium glucoheptonat. Bn trn th trng di dng dung dch ng trong ng 10ml, 5ml. Mi mililit cha 110mg calcium glucoheptonat hoc 9mg ion Ca2+. Chng c pha trong dung mi nc ct thnh cc dung dch c nng thch hp ( tho mn nh lut Lambert Beer). Dung dch c pha vo cc Cuvet ra sch, dung dch cha x l c o ph v lu gi lm ph chun. Sau chia lm 2 phn, phn 1 em chiu t ngoi trong 15ph, 30ph, 45ph, 60ph bi n Xenon 75W vi khong cch 10cm. Phn 2 c sy nhit 35oC, 40oC, 50oC trong 30ph, 45ph, 60ph bi l sy. 3. KT QU V NHN XT Sau khi tin hnh x l mu, em o ph v thu c cc kt qu nh sau: 3.1. Ph hp th ca dung dch Calcium corbire cha x l v sau khi sy nhit 35oC, 40oC, 50oC: Nng dung dch l 0,1mg/ml.
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i hc Nng - 2008
*Nhn xt: Dung dch Calcium Corbire khi c sy cc nhit khc nhau trong nhng khong thi gian khc nhau, ta thy: + Khi chu tc ng bi nhit , cc cc i dch chuyn v pha sng di. Trong khong bc sng nh hn 240nm th nh ph b mt. Nhit sy cng cao, thi gian sy cng ln th t l cng hp th thay i r rt, dng ph cng thay i theo. nhit 500C ph hp th thay i hon ton, nh ph mt. V tr tng i ca hai nh ph thay i r rt so vi mu cha x l. 3.2. Ph hp th ca dung dch Calcium corbire khi cha x l v sau khi chiu nh sng t ngoi: Nng dung dch Calcium corbire l 0,1mg/ml.
*Nhn xt: Khi b chiu x bng t ngoi trong thi gian 15ph dng ph thay i rt t. Tng thi gian chiu n 45ph th ph hp thay i, t l cng hp th gia hai nh thay i r rt. V khi chiu n thi gian 60ph th ph hp th thay i hon ton, nh ph mt. Sau mt thi gian tin hnh thc nghim chng ti rt ra c kt lun sau: Khi chu tc ng ca nh sng t ngoi v nhit , ph hp th ca dung dch Calcium Corbire thay i. Chng t nhit v nh sng t ngoi u nh hng n thuc Calcium Corbire, c bit l nhit . Mc chu tc ng loi yu. So snh vi kt qu o ph hp ca dung dch Vitamin nhm B cng bng phng php ny v cng kho st nh hng ca nhit v nh sng t ngoi. Kt qu nh sau:
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i hc Nng - 2008
*Nhn xt: Nhit v nh sng t ngoi c nh hng n Vitamin. Vi Vitamin B1, B5 tng i n nh, ph c phn thay i c phn khng, mc chu tc dng tng i tt. Cn vi Vitamin B6 ph c s thay i r rt c bit vi vic chiu tia t ngoi. 4. KT LUN Vi nhng kt qu thc nghim thu c, so snh kt qu kho st i vi Vitamin nhm B ca cc tc gi khc, chng ti rt ra mt s kt lun nh sau: Tc ng ca nhit cao: Khi kho st nhit cao hn nhit phng, ph hp th ca dung dch Calcium Corbire thay i chng t c tc ng rt mnh n Calcium Corbire. Mc chu tc dng loi yu. Cn Vitamin nhm B n nhit 80 0C mi c s thay i, mc chu tc dng ca Vitamin tng i n nh.
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i hc Nng - 2008
Tc ng ca nh sng c nng lng ln: C s thay i ca ph hp th r rt khi chiu nh sng t ngoi. Cng ging nh Vitamin nhm B. Thy thuc Calcium Corbire v Vitamin nhm B u chu tc ng ca nh sng c nng lng ln v nhit cao. Tu thuc vo tng loi m c s tc ng khc nhau. i vi dung dch Calcium Corbire chu tc ng mnh ca nhit hn nh sng t ngoi, cn Vitamin nhm B th chu tc ng mnh ca nh sng t ngoi hn nhit , mc chu tc ng ca Vitamin tng i n nh. Vi cc kt lun nh trn cho php xut mt s kin ngh: Vic bo qun thuc tn dc, c th y l Calcium Corbire v Vitamin nhm B cn quan tm n cc yu t mi trng xung quanh nh: nhit v nh sng c nng lng ln. i vi thuc Calcium Corbire chu tc ng mnh ca nhit , cn Vitamin nhm B chu tc ng ca nh sng c nng lng ln. TI LIU THAM KHO [1] L Tn Ngha (1997), Phn tch, nh gi tc ng ca mi trng bo qun n cht lng ca mt s loi thuc tn dc bng phng php hp th phn t, Lun vn thc s, Trng i hc khoa hc - i hc Hu. [2] Trn L Ngc Trm (2007), Tm hiu my quang ph UV Vis, kho st nh hng ca nhit n ph hp th ca mt s Vitamin thng thng, Lun vn tt nghip, Trng i hc s phm Nng. [3] L Ho (1975), Cu trc ph phn t, Nxb i hc v Trung hc Chuyn nghip, H Ni. [4] DS. Phm Thip DS. V Ngc Thu (2000), Thuc bit dc v cch s dng, Nxb Y hc, H Ni. [5] http://www.en.wikipedia.org/wiki/calcium
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