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I,Nguyn tc.
Acid ascorbic ( Vitamin C ) l 1 hp cht cha no c cha nhm endiol. Acid ascorbic b ph hu rt nhan di tc dng ca cc cht oxy ho v bn trong mi trng acid . Phng php da trn nguyn tc l acid ascorbic c kh nng oxy ho kh thun nghch nh trong phn t ca n cha nhm endiol. V vy , acid ascorbic c xc nh bng phng php chun vi KIO3/KI theo phn ng sau: KIO3 + 5KI + 6HCl 3I2 + 6KCl + 3H2O Acid ascorbic + I2 Acid dehydroascorbic + 6HI
- Ly vo erlen 10ml dung dch cha Vitamin C t bnh nh mc , thm vi git tinh bt 1% v em nh phn bng KIO3/KI 0.001N ti khi xut hin mu xanh en . Lp li 3 ln c kt qu chnh xc. Sau ly kt qu trung bnh V (ml) dung dch KIO3/KI 0.001N dung chun vitamin C. - Tin hnh song song cc mu kim chng . Ht 10ml dung dch HCl 1% thm vi git h tinh bt 1% v em nh phn bng KIO3/KI 0.001N ti khi xut hin mu xanh en . Lp li 3 ln c kt qu chnh xc hn. Sau ly kt qu trung bnh V (ml) dung dch KIO3/KI 0.001N dung chun vitamin C.
IV.Kt lun.
Kt qu:
a: S ml KIO3/KI 0.001N dung nh phn dch chit vitamin C b: S ml KIO3/KI 0.001N dung nh phn mu kim chng. m: Lng mu th nghim ( Khi lng sri) X: hm lng vitamin C (mg/100g) 0.088: S mg acid ascorbic ng vi 1ml dung dch KIO3/KI 0.001N 100 : th tch bnh nh mc (ml)
m = 3g
Hm lng vitamin C trong mu th nghim c tnh bng cng thc: X = ((a b) x 0.088 x 100 x 100) / (10.m) = ( (0.7 0.6) x 0.088 x 100 x 100) / (10 x 3 ) = 2,93 ( mg/100g)