Ti phng th nghim ca cng ty TNHH Tn Thun Phong c thc hin phn tch cc ch tiu ca nc v bn thi. Mt trong s l hm lng Cu 2+ .

. Chng ti phn tch ch tiu ny bng 3 phng php l: chun , trc quang, phn tch khi lng v ng thi i chiu kt qu phn tch ca c ba phng php a ra gi tr xc thc nht. Phng php phn tch khi lng l phng php rt gn vi sn xut v vy thc hin o bng phng php ny l bt buc ti phng th nghim v kt qu phn tch dng i chiu vi hiu sut trong qu trnh sn xut ti nh my. Phng php quang ph l phng php o nhanh cho kt qu chnh xc, gip nhanh chng bo co cho gim c hm lng ng trong bn thi, nc thi c nhp v. Phng php chun cng c kt qu chnh xc trong thi gian ngn, tuy nhin phng php trc quang c nhiu u im hn nn gn y chng ti ch s dng phng php chun tham kho, so snh. Xc nh Cu bng phng php khi lng : phng php da trn phn ng ca st hoc km vi dung dich mui ng cho sn phm l ng kim loi. Lng st, km d ln trong ng c ha tan bng axit sunfuric Cn m(g) mu t Ph mu bng axit H2SO4 c Cho thm vi git H2O2 Sau khi phn ng ht ,lc ly dung dch CuSO4 Cho Fe kim loi vo dung dch y Cu Sau khi ht Cu,vt Fe, lc ra ht axit Cho vo t sy Cn Cu Xc nh Cu bng phng php trc quang: C s ca phng php ny da no mu c trng ca phc [Cu(NH3)4]Br2 bn vng. Cc bc thc hin phn tch nh sau Cn 1 5g t ( ty thuc nng ln hay nh ) Ha tan bng dung dch 100ml H2SO4 2M. Cho thm 10ml H2O2 50% Lc v thu c dung dch CuSO4. Trung ha dung dch bng NaOH 2M v pH = 3 - 4. Thm 10g KBr cho vo dung dch trn.

 Chuyn ton b dung dch va thu c vo bnh nh mc 250ml. Cho thm 25ml NH3. nh mc bng nc ti vch. Nu dung dch thu c c kt ta ca Fe th lc bng giy lc ri mang o mt quang bc sng 800nm. Kt qu mt quang hc thu c, s dng ng chun tnh ton ra hm lng Cu2+ ng chun c xy dng bng CuSO 4.5H2O tinh khit vi cc gi tr nng Cu2+ tng ng l 50, 100, 200, 400, 600, 800 ppm

ng chun phn tch Cu2+ dng vo ngy 25/6/2013 o hm lng ng trong nc thi cng nh trong bn thi, ti phng th nghim chng ti c s dng my quang ph Visible Spectrophotometer hiu Jenway 6300 c sn xut ti Anh Quc. Nguyn tc hot ng ca my l trc mi ln o cn bt my trc 30 pht nh sng ca n chiu t n nh. Sau hiu chun (calibration) bng curvet ng nc ct. V my Visible Spectrophotometer l my o tng i da trn im zero c hiu chun trc mi ln o v ng chun c dng sn nn khng cn bo dng nh k ca chuyn gia, tr khi n chiu gp trc trc. m bo tnh chnh xc ca phng php o, trnh tc ng ca yu t thi tit, nhit , nh k chng ti thc hin vic dng ng chun 2 thng 1 ln.