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Bi 4: Cht rn
1. Gii thiu chung 1.1. ngha mi trng
con ngi.
Bi 4: Cht rn
1.2. Cc nh ngha Cht rn tng cng (TS) = Cht rn l lng (SS) + Cht
rn ha tan (TDS)
Cht rn n nh ( thnh phn l cc cht v c): L phn cn li ca cht rn tng cng sau khi t 5500 C
2. Thc hnh
1. Gii thch tm quan trng ca vic phn tch cht rn trong cc lnh vc: a. Hm lng cht rn ha tan v vic cp nc th b. Cht rn tng cng v cht rn bay hi i vi nc thi v bn lng c. Cht lng c v nc thi sinh hot.
2. D on kt qu phn tch v gi tr thc khi xc nh hm lng cht rn trong cc iu kin sau: a. Cc nung cn m b. Xc nh tng cht rn bay hi khi t l Mangan cacbonat cha trong mu cao.
Cu 3
212 mg/l
Bi 7: Chloride
1. Gii thiu chung 1.1. ngha mi trng Chloride l ion chnh trong nc thin nhin v nc thi Mu cha 250 mg Cl-/l c th nhn ra v mn nu nc c cha ion Na+ Hm lng Clo cao s gy n mn cc kt cu ng
kim loi
Bi 7: Chloride
1.2. Nguyn tc Trong mi trng trung ha hay kim nh K2CrO4 c th lm cht ch th mu ti im kt thc trong pp nh phn Clo bng AgNO3 Da vo s khc bit v tch s tan ca AgCl (Ts= 3.10-10) v Ag2CrO4 (Ts= 3.10-12), Ion Ag+ s kt ta hon ton vi Cl- trc , sau mi kt ta gch
vi CrO4-
Bi 7: Chloride
1.3. cc tr ngi Ion Br-, I-, CN- c xem nh tng ng vi ClS2-, SO32-, S2O32Fe trn 10mg/l s che lp s i mu ti im kt thc 2. Thc hnh 3. Cng thc tnh
82,5 mg/l
2/ Xc nh li nng dung dch chun AgNO3 bng dung dch chun gc NaCl 0,02N. Lng AgNO3 chun ht 11,5ml vi th tch NaCl 0,02N s dng l 10ml. Nng dung dch chun AgNO3 l: 0,017 N
3/ Xc nh li nng dung dch chun AgNO3 bng dung dch chun gc NaCl 0,02N. Lng AgNO3 chun ht 9,5ml
Bi 8: Acid
1. Gii thiu chung 1.1. ngha mi trng axit biu th kh nng phng thch H+ ca nc Nguyn nhn:
Bi 8: Acid
1. Gii thiu chung 1.1. ngha mi trng Nc thin nhin thng ng thi mang hai tnh cht i nhau: tnh acid v tnh kim Khi b nhim bi cc acid v c v cc mui acid t khu vc hm m, t phnth nc c pH b hn 7 rt nhiu
Bi 8: Acid
Bi 8: acid
1.2. Nguyn tc Dng cc dd kim mnh nh phn cc axit v c mnh, axit hu c, axit yu. acid do nh hng ca acid v c c gi l acid methyl cam acid tng cng c xc nh bng im i mu ca ch th pp
Bi 8: acid
1.3. cc tr ngi
u ca mu
2. Thc hnh
3. Cng thc tnh
metyl l:
120mg CaCO3/l 2/ Ly 50ml mu nc thi em chun xc nh axit
Bi 9: Kim
Bi 8: Kim
1.2. Nguyn tc Dng cc dd acid mnh nh phn kim vi cc ch th PP, methyl cam ( hoc ch th hn hp bromoresol lc + methyl ) kim phenol? kim tng cng?
48,8 mg/l
6/ kim OH- trong nc bng 80 mgCaCO3/l. Vy nng ion OH- l: 27,2 mg/l 7/ kim phenol trong nc bng 120 mgCaCO3/l,
nhiu?
10,2 mg/l
Mc tiu bi hc
Nm c th no l cng? Nguyn tc, cc tr ngi khi xc nh cng trong nc? Nm c kin thc l thuyt trc khi tin hnh th nghim: kin thc v ha cht s dng, quy trnh xc nh T c th kim tra ng cng trong bt k loi nc no.
Trong : A l ml EDTA tham gia phn ng trong mu B mg CaCO3 tng ng 1ml EDTA nh phn
Mu nc c phn tch c cc kt qu nh sau: Na+ = 20mg/l Cl- = 40mg/l K+ = 30mg/l HCO3- = 40mg/l Ca2+ = 5mg/l CO32- = 12mg/l Mg2+ =10mg/l SO42- = 0mg/l Sr2+ = 3mg/l NO3- = 10mg/l
Bit Ca=40.08, Mg=24.305, Sr=87.62, Na=22.9, K=39.09. cng tng cng, cng carbonate & phi carbonate ln lt l? 57,043 & 52,78 & 64,403 mg CaCO3/l
1/ Vi cng thc xc nh nng Ca2+ l: Canxi(mg/l) = VEDTA x 400,8/ Vml mu ng vi nng ca EDTA? 0,02 N 2/ cng canxi c xc nh, ng vi nng ca EDTA 0,01M l: cng canxi (mg/l) = VEDTA x 400,8/ Vmu cng canxi (mgCaCO3/l) = VEDTA x 1000/ Vmu
Bi 13: St
1. Gii thiu chung 1.1. ngha mi trng
Bi 13: St
1. Gii thiu chung 1.1. ngha mi trng
Bi 13: St
1.2. Nguyn tc
Cc dng st ha tan trong mu nc c kh v st (II) bng cch un si mu vi hydroxylamine (NH2OH) trong mi trng axit pH 3,2 3,3. St (II) to phc mu cam vi 1,10 phenanthroline trong khong pH t 3,0 9,0. Phc gia st (II) v 1,10 phenanthroline tng i bn v cng mu khng i khong 6 thng.
Bi 13: St
Phng trnh phn ng ha hc:
Fe(OH )3 H Fe3 H 2O
H+ (HCldd) gip ha tan Fe(OH)3, v trong th nghim ny, nht thit ton b st trong mu phi di dng ha tan.
Fe NH 2OH Fe N2O H 2O H
Phi kh thnh Fe+2 v 1,10 phenanthroline ch to phc vi Fe+2 nn Fe+3 phi kh thnh Fe+2. Hydroxylamine c dng lm tc nhn kh.
Bi 13: St
+ Fe2+
1,10phenanthroline
Phc mu cam
to phc mu cam
Bi 13: St
3. Thc hnh
3.1. St tng cng ( Fetc) 3.2 St ha tan 3.3. St hai ( Fe2+ )
Ngay sau khi ly Phi thc hin mu, lc mu bng giy lc c m, sau acid ha nc lc, tin hnh tng t nh Fetc ti v tr ly mu, khng cho NH2
Bi 13: St
Bi 13: St
Bi 13: St
hu c
Nitrite dng cho ngnh cp nc nh mt cht chng n mn
25g/l
Kt qu phn tch bng phng php o quang trong mu nc cho cc s liu nh sau:
DO l yu t xc nh s thay i xy ra do vsv k kh
hay hiu kh L ch tiu quan trng nht lin quan ti vic kim sot
3. Thc hnh
1/Xc nh li nng dung dch chun Na2S2O3 bng dung dch chun gc K2Cr2O7 0,05N khi c mt KI trong mi trng
3/ Xc nh DO trong mu nc bng phng php Winkler ci tin vi dung dch chun Na2S2O3 sau khi kim tra li c nng 0,025N ht 5,3ml, th tch mu em chun l 200ml. Tnh DO 5,3 mgO2/l 4/ Xc nh DO trong mu nc bng phng php Winkler ci tin vi dung dch chun Na2S2O3 0,022N ht 5,3ml, th tch mu em chun l 200ml. Tnh DO 4,67 mgO2/l 5/ Xc nh DO trong mu nc bng phng php Winkler ci tin vi dung dch chun Na2S2O3 0,02N ht 6,3ml, th tch mu em chun l 200ml. Tnh DO 5,04 mgO2/l
BOD - COD
Oxy ha tan DO
NI DUNG
I. BOD 1. nh ngha
2. Cc yu t nh hung
3. Phung php xc nh BOD II. COD 1. nh ngha 2. Cc yu t nh hung
I.BOD
1. nh ngha:
BOD: lng oxy tiu hao cho qu trnh h hp ca vi sinh vt trong iu kin nht nh
Vi sinh vt oxy ha cht hu c theo phng trnh:
Cht hu c + O2 CO2 +H2O + sn phm trung gian
BOD l tiu chun nh gi hiu qu ca cc nh my hay phng php x l nc thi BOD phn nh mc nhim hu c ca nc thi. BOD cng ln th nc thi b nhim cng cao v ngc li.
2. Cc yu t nh hng BOD
Nc thi cng nghip BOD cao
Cht lng nc
1-2 3-5
6-9
10+
Hi nhim
Rt nhim
Sng nguyn s BOD nh hn 1 mg/L. Sng nhim mc nh BOD khong 2-8 mg/L. Nc thi th c x l BOD khong 20 mg/L. Nc thi cng nghip cha x l BOD trung bnh khong 600 mg/L
3. Xc nh BOD
BOD c th c tnh ton bng: Khng pha long = DO ban u DO cui Pha long: (DO ban u - DO cui cng) x H s pha long
Xc nh BOD:
PP trc tip : thu mu nc sng v phn tch ngay ti ch. Mu nc nguyn(hoc pha long) 5 ngy, 200C, trong bng ti (BOD5) . Phng php chai o BOD Oxitop: t chai trong t 200C trong 5 ngy.
II. COD
1. nh ngha:
COD thch hp nui thy sn 15-20ppm, ti a <35ppm n v o l mg/L, ch ra khi lng oxy cn tiu hao trn mt lt dung dch. Xc nh mc nhim hu c trong nc
2. Cc yu t nh hng COD
3 tc nhn chnh: Nc thi hu c Nc thi sinh hot Nc thi ha cht
BOD v COD cao s lm gim nng DO, c hi cho sinh vt v h sinh thi nc
BI TP
1/Tnh COD ca mu bit th tch FAS 0,1N dng chun mu trng v mu phn tch ln lt l 2,5mlv 0,2 ml. Th tch mu em i phn tch l 10ml. Mu phn tch c pha long 100 ln. 18400 mgO2/l 2/Tnh COD ca mu bit th tch FAS 0,1N dng chun mu trng v mu phn tch ln lt l 3mlv 2,2 ml. Th tch mu em i phn tch l 5ml. Mu phn tch c pha long 100 ln. 12800 mgO2/l 3/Tnh COD ca mu bit th tch FAS 0,1N dng chun mu trng v mu phn tch ln lt l 6mlv 2,2 ml. Th tch mu em i phn tch l 10ml. Mu phn tch c pha long 10 ln. 3040mgO2/l
BI TP
4/ Tnh COD ca mu bit th tch FAS 0,08N dng chun mu trng v mu phn tch ln lt l 6,5mlv 2,8 ml. Th tch mu em i phn tch l 10ml. Mu phn tch c pha long 10 ln. 2368mgO2/l 5/ Trong xc nh COD, kim tra dung dch chun FAS ngi ta s dng dung dch chun gc l K2Cr2O7 0,05N. Kt qu: khi ly 10ml FAS chun ht 14ml dung dch K2Cr2O7. Tnh nng dung dch chun FAS: 0,07N 6/ Trong xc nh COD, kim tra dung dch chun FAS ngi ta s dng dung dch chun gc l K2Cr2O7 0,1N. Kt qu: khi ly 10ml FAS chun ht 9,5ml dung dch K2Cr2O7. Tnh nng dung dch chun FAS: 0,095N
Bi 24: Chun b mu t
Bi 24: Chun b mu t
1. Ly mu phn tch
Ly mu t i din theo TCVN 7538-1: 2007 (ISO 10381-1) 5.2 S dng mu t kh khng kh, c x l s b theo TCVN 6647 : 2007 (ISO 11464 : 2006).
Bi 24: Chun b mu t
Bi 24: Chun b mu t
3. Nguyn tc Da trn s chnh lch v khi lng gia mu t kh khng kh v mu t kh kit sau sy nhit t 100 0C n 105
0C
ca mu t.
Bi 24: Chun b mu t
4. Cch phn tch
Sy hp ng mu (4.4) nhit t 100 0C n 105
0C,
Bi 24: Chun b mu t
4. Cch phn tch
Sy hp c mu t trong t sy (4.1) nhit t 100 0C n 105 0C n khi lng khng i. Lm ngui hp c mu t trong bnh ht m n nhit trong phng (t 20 min n 45 min). Ly hp c mu t ra khi bnh ht m, xc nh ngay khi lng bng cn phn tch (P2 ).
Bi 24: Chun b mu t
5. Cng thc tnh m (A) ca mu t tnh bng phn trm nc theo t kh kit (%), c tnh theo cng thc
P 1 P 2 A% x100 P 1 P 3
Bi 24: Chun b mu t
5. Cng thc tnh
H s kh kit (k) c tnh theo cng thc
1.1. ngha
1.2. Nguyn tc
Dng picnomet c th tch 50-100ml. C th thay bng bnh nh c c hp, lm bng loi thy tinh bn c th un nu c
Bi 27: chua ca t
I. chua trao i
1. ngha Bit tnh cht t. Bit nguyn nhn gy nn tnh cht t.
dch KCl 1N
2. Nguyn tc