Bài 1 Phương Pháp Kiểm Nghiệm Thóc

BO CO PHN TCH THC PHM
CHUYN : LNG THC THC PHM

NHM 3 | GING VIN: VNH LONG

1
I. Phng php ly mu
Ly mu l mt giai on quan trng trong vic nh gi cht lng ca ht
thc.
Mu phi phn nh chnh xc mi c im cht lng ca ht v phi c
trng cho thnh phm trung bnh ca ton th l ht.
ly mu phn tch, trc ht phi ly mu u tin.
Mu u tin bao gm cc nhm ht ly cc v tr khc nhau ca khi ht ri
tp trung li.
Nu khi ht cng ln, s nhm ht phi ly cng nhiu s khng thun li cho
vic phn tch. V vy t mu u tin s ly ra mu trung bnh.
Nu mu u tin c khi lng khng qu 4kg th n ng thi l mu trung
bnh.
xc nh cc ch s cht lng ca ht thc, t mu trung bnh li chia thnh
nhiu mu nh gi l mu phn tch.
Th t ly mu nh sau:
Khi ht mu u tin mu trung bnh mu phn tch
II. Cc ch tiu cht lng ca thc
1. Ch tiu cm quan
Mu sc c mu t nhin ca thc
Mi c mi c trng ca thc
V khng c v l
Nm mc khng c nm mc
2. Cc ch tiu ha l
Ch tiu Hng cht lng
1 2 3 4
1. m (%) nh hn
2. Tp cht (%) nh hn
3. Ht bc bng
4. Ht bin vng
5. Ht khng hon thin
14
2
7
0,5
3
14
2
12
1
4
14
2
20
2
6
14
2
40
4
8


2
6. Ht h hng
7. Ht rn nt
8. Ht ln loi
9. Ht
10. Su mt (con /kg)
0,5
10
5
1
5
1
15
10
3
5
3
25
15
8
5
5
40
20
15
5

III. o m
Hin nay c 2 phng php xc nh m ca thc:
a) Phng php sy nhanh
1. Nguyn tc
Dng sc nng lm bay hi ht lng hi nc t do c trong mu thc (n khi
lng khng i). Cn trng lng thc trc v sau khi ly sy kh, t tnh ra
lng hi nc (%) c trong thc.
2. Dng c v ha cht
T sy
Chn sy
Cn phn tch
Bnh ht m
Kp gp
My nghin ht hoc ci xay c ph
Ry kim loi kch thc l 0,5-0,8 mm
3. Cch tin hnh
Cn mi nhm 50 g mu thc
Nghin thc bng my nghin
Phn nghin c cho qua ry kim loi kch thc l 0,5-0,8 mm
Cn 3 g phn lt ry cho vo chn sy c lm kh v bit trc khi lng
Cho vo t sy, sy nhit 130 trong 40 pht (n khi lng khng i)
Ly mu ra v lm ngui trong bnh ht m.
Sau em cn khi lng chn sy v mu sau khi sy.
Ghi nhn li kt qu v tin hnh tnh ton.



3

Hnh 1.1. Chn sy trc khi sy Hnh 1.2.Chn sy v mu thc sau khi sy
4. Tnh kt qu
m ca thc c tnh theo cng thc sau:
W =
. 100 (%)
Vi:
W: m ca thc
: Khi lng mu v chn sy trc khi sy
Khi lng mu v chn sy sau khi sy

m: Khi lng chn sy
Kt qu t c:
m = 50,7568 g
= 53,772 g
= 52, 3718 g
Vy W =
. 100 =

. 100 = 46,43 %


4
b) o m bng my o m
1. Nguyn tc
Dng my o m trong thc, o 3 ln sau ly gi tr trung bnh.
2. Dng c
My o m (Model: Kett F511)
THNG S K THUT RI CETER-F SERI ES
Phng php o Tr khng in
ng dng v khong o
La ht di (9-30%), go xay ht di
(9-20%), la m (10-30%), u phng
(10-24%), tiu en (7-20%), tiu trng
(9-20%)
chnh xc 0,5% o trong khong 10 ~ 20% m
Hin th Mn hnh LCD backlight
Ngun in 4 pin 1,5V (loi AA Alkaline)
Kch thc (rng x di x cao) 164 x 94 x 65mm
Trng lng 445g (Net)

3. Cch tin hnh
Nhp v gi nt Average xa b nh trc.
La chn ch o cho thc , la (paddy) trn mn hnh hin th.
Cho lng thc va vo chn o, sau lp chn vo my. Gi c nh chn
v vn trc quay n vch quy nh.
Nhp nt Measure xc nh ch s m


5

Thc hin 3 ln lin tc, sau nhp nt Average ly gi tr trung bnh
4. Kt qu o c
o ln 1: 18,3 %
o ln 2: 18,4 %
o ln 1: 18,7 %
Gi tr m trung bnh: W
tb
= 18,46 %
Bn lun
Gia 2 phng php o m trong phng th nghim th:
Phng php s dng my o c u im: n gin, d thc hin, kt qu tng
i chnh xc nu thao tc ng. Tuy nhin, nhc im phng php ny: ph
thuc vo my, ch quan, d sai kt qu nu khng bit cch iu chnh my.
Phng php sy nhanh c nhc im: mt nhiu thi gian, i hi phi kho
lo trong tng bc, d cho kt qu sai lm (ph thuc vo cc yu t: con
ngi, my mc, mi trng xung quanh). Tuy vy, phng php ny cho kt
qu kh chnh xc, chp nhn c v thng c gi l Phng php trng
ti.
V kt qu o c:
Phng php s dng my o: W
tb
= 18,46 %
Phng php sy nhanh: W = 46,43 %


6
C mt s chnh lch kh ln gia 2 phng php, iu ny chng t trong lc th
nghim nhm cn nhiu sai st. C th:
phng php sy, c th qu trnh sy chn cha t yu cu ( n khi khi
lng khng i), lc cn chu nhiu nh hng cc yu t mi trng dn n
sai s
Cn i vi phng php my o, y l ln u tin nhm s dng my o m
nn khng trnh khi nhng thiu st ( vn trc quay cha ng ti vch).
Kt lun:
Nhn chung, in kin phng th nghim th phng php o m bng sy nhanh s
c nhiu bt li hn (iu kin phng th nghim cha tht s ph hp, sai st ca
ngi thc hin) v cho kt qu sai khc qu xa so vi dng my o m. Nn ta chp
nhn kt qu o c t phng php my o: W = 18,46 %
So snh vi ch tiu cht lng ca thc th m (%) thc nh hn m yu cu hay
18,46 % > 14%. Do , mu la ang th nghim khng t yu cu cht lng.
IV. Xc nh khi lng tuyt i ca thc
nh ngha
Khi lng tuyt i ca thc l khi lng ca 1000 ht nguyn vn
ngha
c trng cho ln ca ht thc. Nu khi lng tuyt i ca ht cng ln th chng
t ht cng to ngha l phn ni nh cng nhiu, khi ch bin t l ht go thu c
cng cao.
1. Nguyn tc
Cn 1000 ht nguyn m c t mu trung bnh v biu din theo n v (g/ 1000
ht)
2. Dng c v ha cht
Cn in t
Khay nha vung 20 x 30 cm
Cc 100 ml


7
Cc 250 ml
Que gt
3. Cch tin hnh
Sau khi ly mu trung bnh, trn u khi ht thc nhiu ln, dn u trn
khay
Dng que gt gch 2 ng cho

m chnh xc tam gic th nht 250 ht ri gp vi 250 ht tam gic i
din, em cn c khi lng ca 500 ht l m
1
(g)
Lm tng t vi 2 tam gic i din cn li, cn c m
2
(g)
Nu chnh lch gia 2 kt qu ca 2 mu 500 ht khng vt qu 5% th chp
nhn, cn vt qu 5% th phi tin hnh lm li.
4. Tnh kt qu
Kt qu o c:
m
1
= 11,4352 g
m
2
= 11,626 g
Chnh lch (%) gia 2 mu 500 ht c tnh theo cng thc
%CL =
. 100 =

. 100 = 1,64 %


8
Do 1,64% < 5% nn ta chp nhn kt qu o c ca 2 mu 500g
Vy khi lng tuyt i (KLTD) ca mu thc theo cht kh c tnh theo cng
thc:
KLTD = (m
1
+ m
2
) .

= (11,4352 + 11, 626).

= 18,8 (g / 1000 ht)

5. Bn lun
Vy khi lng ca 1000 ht thc ang kho st t 18,8 g.
V. Xc nh chiu di ca ht thc
1. Nguyn tc
Dng thc cp xc nh chiu di ca ht go lt.
o chiu di ca mt s lng ht thc i din cho ton b l mu, sau ly gi tr
trung bnh. Tra bng tiu chun xp loi c tnh ca thc.
ngha
Ht thc cng di th ht go sau khi xay ra cng di. Ngi ta ng dng sn xut ra
ht go ng kch thc yu cu ca n hng.
2. Dng c
Thc cp
Cc thy tinh 100 ml
Kp gp
My bc v thc
Khay nha
3. Cch tin hnh
Chn ngu nhin 50 ht thc nguyn vn sau bc v tng ht bng tay (hoc
bng my bc v).


9

Dng thc cp o phn ni nh bn trong (n v: mm). Ly mt s l.
Ghi li kt qu o c v tnh ra gi tr trung bnh.
4. Tnh kt qu
Kt qu o chiu di 50 ht go nh sau:
Ht Chiu
di(mm)
Ht Chiu
di(mm)
Ht Chiu
di(mm)
Ht Chiu
di(mm)
Ht Chiu
di(mm)
1
2
3
4
5
6
7
8
9
10
6,7
5,2
5
5,4
5,7
5,2
5,4
5,9
5,2
5,5
11
12
13
14
15
16
17
18
19
20
5
5,6
5,4
5,1
5
5,7
5,3
5,6
5,5
5,9
21
22
23
24
25
26
27
28
29
30
5,5
5,3
5,1
5,7
5,6
5,6
5,3
5,5
5,5
6
31
32
33
34
35
36
37
38
39
40
5,6
5,2
5,1
5,3
5
5,5
5,4
6,5
5,3
5,4
41
42
43
44
45
46
47
48
49
50
5,1
5,9
5,4
5,4
5,7
5,2
5,5
5,6
5,4
5,3

Chiu di ht trung bnh c tnh ra kt qu nh sau: L
tb
= 5,464 mm.
5. Bn lun
Tra bng tiu chun go, mu go ang kho st thuc loi go ht trung bnh (chiu
di t 5mm n 6mm).


10
VI. Xc nh tp cht
1. Nguyn tc
Loi nhng ht khng phi l thc nguyn vn t trong mu thc. T tnh ra % tp
cht trong mu.
2. Dng c
B sng gm 3 loi c kch thc l: 2,5; 1,7; 1,0.
Cn phn tch
3. Tin hnh
Cn 400g mu thc, dng sn phn ly v tay nht tch cc tp cht. Cn v biu din
tng tp cht theo %.

Hnh 1.3.Mu thc c chn. Hnh 1.4.Tp cht trong mu thc.
4. Tnh kt qu
% Tp cht trong mu c tnh theo cng thc
X =

Vi m: khi lng tp cht (ht lp, bi vn) (g)
M: khi lng mu (g).


11
Kt qu th nghim thu c: m = 4,174 g ; M = 400 g
Vy X=
= 1,0435 %
5. Bn lun
Vy mu thc ang kho st t yu cu v ch tiu tp cht (1,0435 % < 2 %).
VII. Xc nh ht rn nt
1. Nguyn tc
Dng my hoc tay bc v tru ca mu thc. Quan st ht go lt pht hin cc
ht rn nt, t tnh ra % ht rn nt.
2. Dng c
Cn phn tch
Khay nha
My bc v
Knh lp
3. Tin hnh
Cn 20g thc t mu trung bnh, a vo my bc v thu c ht go lt. Dng knh
lp pht hin nhng ht rn nt trn ht go.
4. Tnh kt qu
% Ht rn nt c tnh theo cng thc
R =
(%)
Vi m: khi lng ht rn nt (g)
M: khi lng mu phn tch (g)
Kt qu thc nghim: m= 0,4g
Tuy nhin trong qu trnh bc v, vn cn nhng ht thc cha c tch v hon
ton. Do vy khi lng mu s bng khi lng thc tr i khi lng ht thc bc v
cn st (M
1
= 1,688g).


12
M = 20 M
1
= 20 -1,688 = 18,312 g
Vy: R=
= 2,18 %
5. Kt qu
Mu thc ang kho st t hng 1 cht lng v ch tiu ht rn nt.
VIII. Xc nh % cc loi ht
1. Nguyn tc
Chn cc loi ht: bc bng, ht bin vng, ht xanh non, ht h hng, ht , ht ln
loi c trong mu phn tch. T tnh ra % cc loi ht.
2. Dng c
Cn phn tch
Khay nha
My bc v
Cc 50ml
3. Tin hnh
Cn 20g mu thc t mu trung bnh, dng my xay tch v tru, dng tay nht tng
loi ht ri biu din theo %.
4. Tnh kt qu
Trong qu trnh bc v, vn cn nhng ht thc cha c tch v hon ton. Do vy
khi lng mu s bng khi lng thc tr i khi lng ht thc bc v cn st
(M
1
= 2,765g).
M = 20 M
1
= 20 2,765 = 17,235 g
Kt qu thc nghim, khi lng cc ht:
Ht xanh non: 0,45 g
Ht : 0,116 g
Ht bc bng: 0,602 g
Ht h hng: 0,095 g


13
Biu din theo thnh phn % cc loi ht, ta c:
% Ht xanh non
.100 = 2,61 %
% Ht
.100 = 0,67 %
% Ht bc bng
.100 = 3,49 %
% Ht h hng
.100 = 0,55 %
5. Bn lun
Mu thc ang kho st t hng 1 cht lng v ch tiu ht khng hon thin
(2,61 % < 3 %).
Mu thc ang kho st t hng 1 cht lng v ch tiu ht (0,67 % < 1 %).
Mu thc ang kho st t hng 1 cht lng v ch tiu ht bc bng (3,49 % < 7 %).
Mu thc ang kho st t hng 2 cht lng v ch tiu ht h hng
(0,5 % < 0,55 % < 1%).



14

I. o m:
1/ Nguyn tc:
Dng my o m trong thc, o 3 ln sau ly gi tr trung bnh.
2/ Dng c:
My o m dng cm bin
3/ Cch tin hnh:
Nhn nt Power khi ng my.
Nhn nt Select chn loi ht cn o. y chn ch Rice 12.
Nhn nt Measure chun b o m ca ht. i mn hnh hin th ch
pour ri bt u go vo my o, ch tc ht phi u trnh sai
s.
i mt vi giy mn hnh hin th kt qu, ghi nhn kt qu. Tip tc tin hnh
nh vy t bc go thm 2 ln na, sau bm nt Average tnh kt
qu trung bnh sau 3 ln o. Ghi nhn kt qu trung bnh.

Hnh 2.1. My o m


15
4/ Kt qu o c:
Ln 1: W
1
= 13%
Ln 2: W
2
= 13,1%
Ln 3: W
3
= 13,3%
1 2 3
W W W 13 13,1 13, 3
W 13,1%
3 3

Gi tr m trung bnh l: 13,1%.
5/ Bn lun:
Kt qu sau 3 ln o khng chnh lch nhau nhiu. Ngoi ra kt qu thu c so vi
cc nhm khc cng khng chnh lch nhiu nn kt qu ng tin cy.
II. Xc nh chiu di ca go
1/ Nguyn tc:
Dng thc cp xc nh chiu di ca ht go. T tra bng tiu chun xp
loi c tnh ca go.
2/ Dng c:
- Cn phn tch
- Khay nha
- Thc cp
3/ Tin hnh:
Cn 20 g mu go, chn ngu nhin 50 ht thc nguyn vn. Dng thc cp o
chiu di 50 ht go ri tnh chiu di trung bnh ca mt ht go


16
4/ Tnh kt qu:
Kt qu o chiu di 50 ht go nh sau:
Bng 1: Kt qu chiu di ca 50 ht
Ht Chiu
di ht
(mm)
Ht Chiu
di ht
(mm)
Ht Chiu
di ht
(mm)
Ht Chiu
di ht
(mm)
Ht Chiu
di ht
(mm)
1 6,3 11 6,1 21 6,6 31 6,2 41 5,6
2 6,6 12 6,0 22 6,4 32 6,9 42 5,5
3 6,7 13 7,0 23 7,1 33 6,4 43 5,3
4 6,6 14 6,5 24 6,6 34 6,7 44 6,5
5 6,9 15 6,7 25 6,5 35 6,2 45 7,0
6 6,2 16 6,7 26 7,1 36 5,9 46 6,3
7 7,0 17 6,3 27 6,4 37 6,3 47 6,6
8 6,7 18 6,4 28 6,7 38 6,0 48 6,6
9 6,4 19 6,6 29 6,7 39 6,1 49 6,8
10 6,8 20 6,5 30 6,5 40 5,7 50 6,1

Ta c:
6, 3 6, 6 6, 7 ... 6, 6 6,8 6,1
6, 47( )
50
l mm

5/ Bn lun:
Go ca nhm o c c chiu di trung bnh nm trong khong t 6mm n 7mm
nn c xp trong loi ht go di.



17
III. Xc nh t l tm:
1/ Nguyn tc:
S dng my chn ht tch ring phn go nguyn vn v tm. tnh ra phn %
tm so vi khi ht.
2/ Dng c:
- My chn ht.
3/ Tin hnh:
Ly 100g go vo my chn ht, cho my hot ng tch ring tm v go
nguyn. T tnh ra % ht tm so vi khi ht.

Hnh 2.2 My tch tm
4/ Tnh kt qu
Kt qu thu c l: 27,95g tm.



18
Suy ra:
T l tm trong 100g l 27,95%
T l go nguyn trong 100g l 72,05%
5/ Bn lun:
T l tm so vi khi ht khng ln vo khong 27,95%. Kt lun l cht lng go
kh tt.
IV. Xc nh % cc loi ht:
1/ Nguyn tc:
Chn cc loi ht: bc bng, ht bin vng, ht xanh non, ht h hng, ht , ht ln
loi c trong mu phn tch. T tnh ra % cc loi ht.
2/ Dng c:
- Cn phn tch
- Khay nhm
3/ Cch tin hnh:
Cn 20g go t mu trung bnh dn u trn mt khay hoc mt knh. Nht cc ht ni
trn thnh tng phn ring bit vo cc ng mu. Cn ring tng loi v t suy ra
kt qu % khi lng cho tng ch tiu cn xc nh.
4/ Tnh kt qu:
Khi lng ht bc phn l 0,67g.
% ht bc phn =
0, 67.100
3, 35%
20

5/ Bn lun: phn trm (%) theo khi lng ca ht bc phn l 3,35%. T l ny
khng ln lm nn kt lun go t cht lng. Do go kim nghim c ty trng
t trc nn cc loi ht b h hng, , xanh non, bin vng hu nh khng cn.


19
V. Xc nh hm lng tinh bt:
1/ Nguyn tc:
Thy phn tinh bt bng HCl sau xc nh hm lng ng tng bng phng
php Bectrand.
Glucid kh Cu(OH)
2
mi trng kim mnh, to kt ta di dng Cu
2
O mu
gch. S lng Cu
2
O tng ng vi s lng glucid.
RCHO + 2Cu(OH)
2
RCOOH + Cu
2
O + 2H
2
O
Cu
2
O c tnh cht kh, tc dng vi Fe(III) lm cho mui ny chuyn sang dng
Fe(II) mi trng acid.
Cu
2
O + Fe
2
(SO
4
)
3
+ H
2
SO
4
2CuSO
4
+ H
2
O + 2FeSO
4

FeSO
4
c tnh kh, tc dng vi KMnO
4
. Do , c th dng KMnO
4
chun
FeSO
4
mi trng acid.
FeSO
4
+ 8H
2
SO
4
+ 2 KMnO
4
K
2
SO
4
+ 2MnSO
4
+ 5Fe
2
(SO
4
)
3
+ 8H
2
O
T s ml KMnO
4
0,1N dng chun FeSO
4
hnh thnh, tra bng c s mg
ng glucoza, maltoza, lactoza hoc saccaroza nhn vi h thng pha long ta c
hm lng ng trong 1g bt go.
2/ Dng c:
- Cn phn tch
- Bnh tam gic 250ml
- Bnh nh mc 250ml
- Cc thy tinh 250ml
- Phu lc
- Bp in
- Ni inox
- Burret
- Pipet 0,5ml


20
- Bnh tia
- Ch th PP 1%
- Dd HCl
- Dd NaOH 20%
- Dd Fe
2
(SO
4
)
3

- Felling A, B
- KMnO
4
0,1N
3/ Cch tin hnh:
1g Bt go Thy phn 4ml HCl +100ml nc Lm ngui Trung ha
nh mc V
m
= 15ml + FA 20ml + FB 20ml un si (3 pht) Lng
Ha tan Chun = KMnO
4
V tiu tn.

Hnh 2.3. un cch thy thy phn mu.


21

Hnh 2.4. Cho dung dch NaOH 20% to MT kim.

Hnh 2.5. Cho dung dch vo bnh nh mc 250ml.

Hnh 2.6. un dung dch sau khi cho Fel A, B.


22

Hnh 2.7. Xut hin kt ta gch.

Hnh 2.8. Lc qua giy lc tch kt ta.
4/ Tnh kt qu:
Th tch tiu tn KMnO
4
l 3,2 ml.
ng nghch o (mg) KMnO
4
0,1N (ml)
10 3,24
11 3,55
Ta c : TB =
.
.100.0, 9
.1000.
dm
m
aV
m V

Trong : a khi lng ng nghch o


23
V
dm
: th tch nh mc
m: khi lng mu
V
m
: th tch mu.
0,9 l h s chuyn i t glucose sang tinh bt

11 10
10 . 3, 3 3, 24 10,19
3, 55 3, 24
a mg

TB =
. 10, 91.250
.100.0, 9 .100.0, 9 16, 365%
.1000. 1.1000.15
dm
m
aV
m V

5/ Bn lun:
Hm lng tinh bt trong go tng i ch so vi tiu chun. C th trong qu
trnh tin hnh th nghim cha c chun xc. Ngoi ra sau qu trnh lc tch kt
ta th tht thot nhiu kt ta, kt ta cn bm trn b mt dng c th nghim vv



24
I. Xc nh m ca bt m
- S dng my o in t, o 3 ln, sau ly kt qu trung bnh.
- m t yu cu ca bt m phi nh hn 13.5%.

Kt qu:

Kt lun: m ca bt m l 13.07% < 13.5% => bt m t tiu chun v m.
II. Xc nh chua ca bt m (hm lng axit)
- nh ngha:
chua ca bt m l s ml NaOH 1N dung trung ha lng acid c trong 100g
bt m.
1. Nguyn tc:
Trung ha lng acid c trong mu dung dch NaOH 0.1N vi ch th PP 1%.
2. Dng c v ha cht:
Cn phn tch
Bnh 150 ml
ng ong 50 ml
Bnh xt tia
S ln Kt qu (%)
Ln 1 12.9
Ln 2 13.1
Ln 3 13.2
Trung bnh 13.07
Hnh 3.1. Xc nh m ca bt m


25
Burete 10 ml
DD NaOH 0.1N
DD PP 1%
Nc ct.
3. Tin hnh:
Cn khong 5g bt cho vo 2 bnh tam
gic 150ml, thm vo 100ml nc ct
trung tnh, lc u tan ht bt. Dng
bnh tia ra nhng ht bt dnh trn thnh
bnh.

Bnh 1: thm vo 2-3 git PP 1% v em
chun bng dd NaOH 0.02N cho n khi
xut hin mu hng, bn sau 30 giy th dng
li v ghi th tch tiu tn ca dung dch
NaOH 0.02N.
Bnh 2: lc trn phu thy tinh, thu ly dch
lc. Sau thm vo dch lc 2-3 git PP 1%
v em chun bng dd NaOH 0.02N cho
n khi xut hin mu hng, bn sau 30 giy
th dng li v ghi th tch tiu tn ca dung
dch NaOH 0.02N.

Hnh 3.2. Ha tan bt m
Hnh 3.3. Chun bng dd NaOH 0.02N


26
4. Kt qu:
chua ca bt tnh bng (
0
) theo cng thc sau:

Trong :
V: s ml dung dch NaOH 0.1N dng trung ha lng axit c trong 50 gam mu,
(ml).
m: s gam mu cn phn tch, (g).
Bnh 1:

Bnh 2:

5. Bn lun:
Kt qu ca bnh 1 (bnh cha lc) c chua cao hn bnh 2 (bnh lc). iu
ny chng t bt m cha tan trong bnh 1 s cn tr im dng ca phng php
chun bng NaOH 0.02N (khi xut hin mu hng, bn trong 30 giy), do kt
qu s b sai lch.
Nhn chung, vic lc cn bt b cha tan (bnh 2) s cho kt qu chnh xc v ng
tin cy hn.
III. Xc nh mn ca bt m
1. Nguyn tc: s dng ry c l = 125 m.
Yu cu: phn lt ry 95% lt trng = 125 m.
2. Tin hnh:
Cn 100g bt ry t t (Lu : trong qu trnh
ry khng s dng tay ch p bt xung) cn
phn khng lt ry => biu din theo phn trm
khi lng.
Hnh 3.4. Ry bt m


27
Yu cu: phn khng lt ry < 5%.
3. Kt qu:
Khi lng phn bt khng lt ry: 0.75g ~ 0.75% => t yu cu.
IV. Xc nh hm lng v cht lng ca gluten
1. Nguyn tc:
To khi bt nho t bt m, ra khi bt nho loi b ht tinh bt, p kit nc.
T xc nh hm lng v cht lng gluten.
2. Dng c v ha cht
Cn phn tch
Cc thy tinh 100ml
a thy tinh
Ry c k l = 125m
Thc k
Khn kh
Chu nha
Dung dch I
2

3. Cch tin hnh
a. To khi bt nho
- Cn 25g bt m cho vo cc thy tinh 100ml
cha sn 15ml nc.
- Dng a thy tinh trn u sao cho tt c
bt u thm nc v khi bt t m l
40 45%.
- Ly bt ra, dng tay nho nn cho tht u,
vo thnh hnh trn v li trong cc vi
thi gian 20.
Ra khi bt nho
Hnh 3.5. Khi bt m sau khi nho nn


28
Cch 1: ra trc tip di vi nc
t khi bt vo lng bn tay tri, nm cc ngn tay li v a vo di vi nc,
pha di t mt ry kim loi v dng tay phi iu chnh tc dng nc (1l
trong 5 pht). Dng tay phi nho nn khi bt nh nhng tinh bt b tch ra theo
dng nc. Tip tc ra cho n khi gluten tr thnh mt khi n hi th tng tc
nc ra cho n khi gluten sch ht tinh bt.
Cch 2: ra trong chu nc
t khi bt trong lng bn tay tri vo chu
nc c sn 2-3l nc. t mt ry kim loi
pha di tay nm khi bt. Dng tay phi nho
nn khi bt nh nhng tch tinh bt ra khi
gluten. Khi nc c th thay nc mi v tin
hnh cho n khi ht tinh bt.
b. p nc:
Sau khi ra khi bt nho xong, dng tay vt kit
nc trong khi gluten, lau tay kh v p ht
nc ra khi khi gluten.

c. Nhn xt mu sc khi gluten:
Bt tt c gluten t mu trng ng nht
Bt xu c gluten t mu sm
Bt hng c gluten t mu ti hn
Kt qu:
Lng gluten thu c: 6.85g.
Gluten t c mu sm chng t bt xu.

Hnh 3.6. Khi gluten thu c

Bài 1 Phương Pháp Kiểm Nghiệm Thóc

Uploaded by

Document Information

Copyright

Available Formats

Share this document

Share or Embed Document

Sharing Options

Did you find this document useful?

Is this content inappropriate?

Copyright:

Available Formats

Bài 1 Phương Pháp Kiểm Nghiệm Thóc

Uploaded by

Copyright:

Available Formats

BO CO PHN TCH THC PHM

CHUYN : LNG THC THC PHM

: Khi lng mu v chn sy trc khi sy

Khi lng mu v chn sy sau khi sy

= (11,4352 + 11, 626).

= 18,8 (g / 1000 ht)

You might also like