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Nc thi
Phng php xc nh nhu cu sinh ha oxy
Nhm I
TCVN
4566 88
Waste water
C hiu lc t
Method for the derter mination of biochemiccal 01/7/1989
oxygen demand (BOD)
Tiu chun ny quy nh phng php Winkler xc nh nhu cu sinh ha oxy
(c vit tc l BOD) (biochemical oxygen demad).
1. Phng php ly mu
1.1. Ly mu theo TCVN 4556-88
1.2. Mu ly xc nh nhu cu sinh ha oxy ly nh mu xc nh oxy ho
tan. Nc cha phn tch ngay phi bo qun iu kin nh hn 4oC.
1.3. Chai cha mu xc nh nhu cu sinh ha oxy phi sy tit trng
150oC.
2. Phng php xc nh
2.1. Nguyn tc
Nhu cu sinh ha oxy l lng oxy cn thit vi sinh vt phn hu cc cht
hu c trong mt n v th tch nc nht nh (1000 ml) trong mt n v thi
gian nht nh, trong iu kin nhit l 20oC v khng c nh sng.
xc nh lng oxy cn phi cung cp cho nc thi mt lng oxy tha
cho qu trnh phn hu cc cht hu c do cc vi sinh vt (qu trnh c th
l: 5; 10; 15; 20 ngy ty theo yu cu nghin cu).
Lng oxy trong nc gim i so vi ngy u cho bit s mg oxy m cc vi
sinh vt tiu th.
2.2. Yu t cn tr
Kim hoc axit nh hng n kt qu xc nh, do phi thc hin trong mi
trng trung tnh. C th dng axit sunfuric H2SO4 0,05M hay natri hidroxit
NaOH 0,1 M xc nh iu chnh.
Nc c, c nhiu cn phi lng ri ly phn nc trong xc nh.
Nc cha clo hot ng cn tr phi loi tr clo nh sau:
Trong 100 ml nc nghin cu cho vo 10 ml kali iodua KI 10%, 10 ml axit
axetic 5%, nh vi git h tinh bt nu xut hin mu tm xanh, r natri thiosunfat
Na2S2O3 0,0125 M cho ti khi mt mu.
2.3. Dng c v thuc th
2.3.1. Dng c
Chai Winkler c th tch bit sn hay chai 250 ml nt mi.
Burt, pipt, bnh nn, t iu nhit.
2.3.2. Thuc th