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JCHS D-03004/B
Walio Mix

GENERAL CHARACTERISTIC OF CRUDE OIL

Specific Gravity @ 60/60F

0.8438

API Gravity @ 60F

36.2
cSt

5.17

@ 100 F

cSt

3.94

@ 122 F

cSt

3.19

@ 140F

cSt

2.89

Pour Point

-20

Flash Point

Below 0

Reid Vapor Pressure @ 100F

PSI

3.5

Kinematic Viscosity @ 70 F

Water Content

Vol. %

<0.05

Water and Sediment

Vol. %

<0.05

Salt Content as NaCl

lbs/1000 bbl

Salt Content as NaCl

Weight %

0.0003

Total Acid Number

MgKOH/g

0.156

Strong Acid Number

MgKOH/g

Nil

Sulphur Content

Weight %

0.62

Asphaltenes

Weight %

0.44

Wax Content

Weight %

4.83

Congealing Point of Pet. Wax

124

Conradson Carbon Residue

Weight %

1.60

Ash Content

Weight %

0.0067

Hydrogen Sulphide

ppm Wt.

Nil

Mercaptan Sulphur

ppm Wt

71.2

Weight %

0.031

KUOP

11.9

Basic Nitrogen
Characterization Factor

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JCHS D-03004/B
Walio Mix

HEMPEL DISTILLATION

1.

At Atmospheric Pressure

2.

YIELD ON CRUDE
CUMM.
WT%
VOL.%

CUMM.
VOL.%

SPECIFIC
GRAVITY
60/60F

REF.
INDEX
N20D

0.31

0.31

2.67

3.07

3.37

0.6768

1.3803

2.41

5.08

2.96

6.33

0.6870

1.3855

75 100

3.06

8.14

3.67

10.00

0.7035

1.3941

4.

100 125

4.46

12.60

5.18

15.18

0.7272

1.4063

5.

125 150

5.94

18.54

6.64

21.82

0.7547

1.4205

6.

150 175

5.83

24.37

6.31

28.13

0.7793

1.4332

7.

175 200

6.03

30.40

6.38

34.51

0.7974

1.4426

8.

200 225

6.04

36.44

6.28

40.79

0.8121

1.4502

9.

225 250

5.83

42.27

5.94

46.73

0.8275

1.4582

10.

250 275

6.12

48.39

6.12

52.85

0.8443

1.4668

FRACT
NO.

TEMP.
RANGE C

WT.%

Gas & Loss

0.21

0.21

1.

IBP 50

2.46

2.

50 75

3.

At Absolute Pressure of 40 mm Hg
11.

175 200

6.82

55.21

6.67

59.52

0.8630

1.4765

12.

200 225

6.69

61.90

6.42

65.94

0.8787

1.4846

13.

225 250

6.37

68.27

6.01

71.95

0.8940

1.4925

14.

250 275

4.86

73.13

4.54

76.49

0.9042

15.

275 300

3.94

77.07

3.63

80.12

0.9164

16.

Residue > 300

22.93

100.00

19.88

100.00

0.9731

Temp. at 40 mm Hg
175
200
225
250
275
300

Temp. at Atmospheric Press.


275
306
335
365
395
421

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JCHS D-03004/B
Walio Mix

CRUDE OIL CLASSIFICATION

Key Fraction I API @ 60F

36.1

Key Fraction II API @ 60F

22.9

This Crude Oil is classified as Intermediate-Intermediate according to the Land and


Garton classification (U.S. Bureau of Mines).

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JCHS D-03004/B
Walio Mix

TRUE BOILING POINT DISTILLATION (*)


MATERIAL BALANCE OF WIDE CUTS

FRACT.

TEMPERATURE
RANGE C

YIELD ON CRUDE
CUMM

CUMM

Wt. %

Wt. %

Vol. %

Vol. %

Condensate to 25

0.28

0.28

0.41

0.41

25 100

7.02

7.30

8.58

8.99

100 150

11.30

18.60

12.81

21.80

150 180

8.00

26.60

8.66

30.46

180 250

16.60

43.20

17.05

47.51

250 300

12.00

55.20

11.85

59.36

300 375

14.83

70.03

14.11

73.47

375 EP (500)

16.13

86.16

14.72

88.19

Residue>EP (500)

13.84

100.00

11.81

100.00

Note: *) A material balance calculation was performed on the above distillation, on a no losses basis to check
its validity. This data is graphically represented in page 16 & 17 of this report.

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JCHS D-03004/B
Walio Mix

TRUE BOILING POINT DISTILLATION


YIELD AND CUTTING RANGE OF FRACTIONS

Temperature Range
C

Yield From Crude


Wt. %

Vol. %

Yield Range From Crude


Wt. %

Vol. %

Condensate to

25 C

0.28

0.41

0.00

0.28

0.00

0.41

Gasoline :

25 100

7.02

8.58

0.28

7.30

0.41

8.99

Naphtha :

100 180

19.30

21.47

7.30

26.60

8.99

30.46

Kerosene :

150 300

36.60

37.56

18.60

55.20

21.80

59.36

180 250

16.60

17.05

26.60

43.20

30.46

47.51

180 375

43.43

43.01

26.60

70.03

30.46

73.47

Heavy Distillates : 375 EP (500)

16.13

14.72

70.03

86.16

73.47

88.19

Residue :

>375

29.97

26.53

70.03

100.00

73.47

100.00

> EP (500)

13.84

11.81

86.16

100.00

88.19

100.00

Gas Oil :

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6 of 19
JCHS D-03004/B
Walio Mix

COMPOSITIONAL ANALYSIS OF LIGHT GASEOUS HYDROCARBONS

Temperature Range, C

Condensate to 25C

Yield from Crude, % weight

0.28

Yield from Crude, % Vol.

0.41

Yield range from Crude, % weight

0.00-0.28

Yield range from Crude, % Vol.

0.00-0.41

COMPONENT

WEIGHT % FROM CRUDE

Methane

Nil

Ethane

Trace

Propane

0.03

Iso-Butane

0.07

N-Butane

0.14

Iso-Pentane

0.03

N-Pentane

0.02

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7 of 19
JCHS D-03004/B
Walio Mix

GASOLINE ANALYSIS
Temperature Range

25-100

Yield from crude

Weight.%

7.02

Yield from crude

Vol.%

8.58

Yield range from crude

Weight.%

0.28-7.30

Yield range from crude

Vol.%

0.41-8.99

Specific Gravity @ 60/60F

0.6901

API Gravity @ 60F

73.5

Refractive Index

N20D

1.3871

Reid Vapor Pressure @ 100F

PSI

12.6

Weight %

0.03

Doctor test

Positive

Copper Strip Corrosion, 3 hrs @ 50C

ASTM No. 4A

Copper Strip Corrosion, 2 hrs @ 100C

ASTM No. 4B

Total Sulphur

Hydrogen Sulphide

ppm Wt.

328.2

Mercaptan Sulphur

ppm Wt.

32.1

63.5

KUOP

12.2

Research Octane Number F1 clear


Characterization Factor
ASTM DISTILLATION : D-86
IBP

30

5 % vol.

38

10 % vol.

42

20 % vol.

46

30 % vol.

50

40 % vol.

54

50 % vol.

59

60 % vol.

64

70 % vol.

70

80 % vol.

76

90 % vol.

82

EP

98

Recovery, vol. %

99.0

Residue, vol. %

0.5

Loss, vol. %

0.5

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8 of 19
JCHS D-03004/B
Walio Mix

NORMALIZED PERCENT DISTRIBUTION GASOLINE RANGE HYDROCARBONS


25-100C

COMPONENT
Ethane
Propane
Iso-Butane
Normal-Butane
Iso-Pentane
Normal-Pentane
2, 2-Dimethylbutane
Cyclopentane
2, 3-Dimethylbutane
2-Methylpentane
3-Methylpentane
Normal-Hexane
2, 2-Dimethylpentane
Methylcyclopentane
2,2,3-Trimethylpentane
2,4-Dimethylpentane
Benzene
1trans3- Dimethylcyclopentane
Cyclohexane
2-Methylhexane
3-Methylhexane
1cis3-Dimethylcyclopentane
1trans2- Dimethylcyclopentane
3-Ethylpentane
Normal-Heptane
1cis2-Dimethylcyclopentane
2,2-Dimethylhexane
Methylcyclohexane
2,4-Dimethylhexane
Ethylcyclohexane
3,3-Dimethylhexane
Toluene +

NORMALIZED WT.%
(C2)
(C3)
(iC4)
(nC4)
(iC5)
(nC5)
(22DMB)
(CP)
(23DMB)
(2MP)
(3MP)
(nC6)
(22DMP)
(MCP)
(223TMP)
(24DMP)
(BZ)
(1t3DMCP)
(CH)
(2MH)
(3MH)
(1c3DMCP)
(1t2DMCP)
(3EP)
(nC7)
(1c2DMCP)
(22DMH)
(MCH)
(24DMH)
(ECP)
(33DMH)
(TOL +)

0.00
0.00
0.55
2.46
5.59
6.95
1.07
0.40
1.64
7.69
5.08
12.50
0.00
5.12
0.07
1.24
7.16
0.72
7.38
7.47
6.07
0.00
1.34
0.00
9.17
0.40
0.23
8.64
0.00
0.00
0.18
0.88

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9 of 19
JCHS D-03004/B
Walio Mix

NAPHTHA ANALYSIS

Temperature Range

100-180

Yield from crude


Yield from crude

Weight.%
Vol.%

:
:

19.30
21.47

Yield range from crude


Yield range from crude

Weight.%
Vol.%

:
:

7.30-26.60
83.99-30.46

N20D
Weight.%

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0.7586
55.0
1.4225
0.06
Positive
ASTM No. 4A

Vol. %
Vol. %
Vol. %
Vol. %
KUOP

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63.19
0.24
26.51
10.06
12.0

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103
114
122
128
132
136
139
143
148
153
162
179
99.0
0.5
0.5

Specific Gravity @ 60/60F


API Gravity @ 60F
Refractive Index
Total Sulphur
Doctor test
Copper Strip Corrosion, 3 hrs @ 50 C
PONA Analysis :
Paraffines
Olefins
Naphthenes
Aromatics
Characterization factor
ASTM DISTILLATION: D-86
IBP
5 % vol.
10 % vol.
20 % vol.
30 % vol.
40 % vol.
50 % vol.
60 % vol.
70 % vol.
80 % vol.
90 % vol.
EP
Recovery, vol %
Residue, vol %
Loss, vol %

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10 of 19
JCHS D-03004/B
Walio Mix

KEROSENE ANALYSIS

Temperature Range

180-250

Yield from crude


Yield from crude

Weight.%
Vol.%

:
:

16.60
17.05

Yield range from crude


Yield range from crude

Weight.%
Vol.%

:
:

26.60-43.20
30.46-47.51

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0.8214
40.8
1.4550
0.14
-67 (minus 67)
26
150
14.20
158
Positive
ASTM No. 4A
11.7

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183
193
199
204
207
210
213
216
219
224
232
251

:
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:

98.5
1.0
0.5

Specific Gravity @ 60/60F


API Gravity @ 60F
Refractive Index
Total Sulphur
Freezing Point
Smoke Point
Flash Point
Aromatic Content
Aniline Point
Doctor Test
Copper Strip Corrosion, 2 hrs @ 100 C
Characterization Factor
ASTM DISTILLATION: D-86
IBP
5 % vol.
10 % vol.
20 % vol.
30 % vol.
40 % vol.
50 % vol.
60 % vol.
70 % vol.
80 % vol.
90 % vol.
EP
Recovery, vol %
Residue, vol %
Loss, vol %

N20D
Weight.%
F
mm
F
Vol.%
F
KUOP
C

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11 of 19
JCHS D-03004/B
Walio Mix

KEROSENE ANALYSIS

Temperature Range

150-300

Yield from crude


Yield from crude

Weight.%
Vol.%

:
:

36.60
37.56

Yield range from crude


Yield range from crude

Weight.%
Vol.%

:
:

18.60-55.20
21.80-59.36

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0.8222
40.6
1.4554
0.18
-64 (minus 64)
22
135
17.10
162
Positive
ASTM No. 4A
11.7

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154
177
185
194
204
213
224
235
246
257
271
298

:
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98.5
1.0
0.5

Specific Gravity @ 60/60F


API Gravity @ 60F
Refractive Index
Total Sulphur
Freezing Point
Smoke Point
Flash Point
Aromatic Content
Aniline Point
Doctor Test
Copper Strip Corrosion, 2 hrs @ 100 C
Characterization Factor
ASTM DISTILLATION: D-86
IBP
5 % vol.
10 % vol.
20 % vol.
30 % vol.
40 % vol.
50 % vol.
60 % vol.
70 % vol.
80 % vol.
90 % vol.
EP
Recovery, vol %
Residue, vol %
Loss, vol %

N20D
Weight.%
F
mm
F
Vol.%
F
KUOP
C

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12 of 19
JCHS D-03004/B
Walio Mix

GAS OIL ANALYSIS

Temperature Range

180-375

Yield from crude


Yield from crude

Weight.%
Vol.%

:
:

43.43
43.01

Yield range from crude


Yield range from crude

Weight.%
Vol.%

:
:

26.60-70.03
30.46-73.47

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:
:
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0.8521
34.6
1.4708
0.39
169
165
0
-5
0.5
58.4
48
ASTM No. 3B
11.7

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184
210
218
229
241
254
268
282
299
315
338
373

:
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:

98.0
1.5
0.5

Specific Gravity @ 60/60F


API Gravity @ 60F
Refractive Index
Total Sulphur
Aniline Point
Flash Point
Cloud Point
Pour Point
ASTM Color
Diesel Index
Calculated Cetane Index
Copper Strip Corrosion, 2 hrs @ 100C
Characterization factor
ASTM DISTILLATION: D-86
IBP
5 % vol.
10 % vol.
20 % vol.
30 % vol.
40 % vol.
50 % vol.
60 % vol.
70 % vol.
80 % vol.
90 % vol.
EP
Recovery, vol %
Residue, vol %
Loss, vol %

N20D
Wt.%
F
F
F
F

KUOP
C

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13 of 19
JCHS D-03004/B
Walio Mix

HEAVY DISTILLATE ANALYSIS

Temperature Range

375-EP (500)

Yield from crude

Weight.%

16.13

Yield from crude

Vol.%

14.72

Yield range from crude

Weight.%

70.03-86.16

Yield range from crude

Vol.%

73.47-88.19

Specific Gravity @ 60/60F

0.9249

API Gravity @ 60F

21.5

Kinematic Viscosity :
@ 140F

cSt

33.65

@ 160 F

cSt

22.25

@ 210 F

cSt

Total Sulphur

9.50

Weight %.

0.96

110

Conradson Carbon Residue

Weight %.

0.09

Wax Content

Weight %.

17.76

128

Weight %.

0.026

ppm

<0.1

ppm

0.3

KUOP

11.8

Pour Point

Congealing Point of Petroleum Wax.


Total Nitrogen
Metal Content :
V
Ni
Characterization factor

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14 of 19
JCHS D-03004/B
Walio Mix

RESIDUE ANALYSIS

Temperature Range

>375

Yield from crude

Weight.%

29.97

Yield from crude

Vol.%

26.53

Yield range from crude

Weight.%

70.03-100.00

Yield range from crude

Vol.%

73.47-100.00

Specific Gravity @ 60/60F

0.9532

API Gravity @ 60F

16.9

Kinematic Viscosity :
@ 140F

cSt

364.26

@ 160F

cSt.

183.70

@ 210F

cSt

56.34

Weight %.

1.45

110

Weight %.

16.11

132

KUOP

11.7

Total Sulphur
Pour Point
Wax Content
Congealing Point Of Pet. wax
Characterization factor

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JCHS D-03004/B
Walio Mix

RESIDUE ANALYSIS

Temperature Range

>EP (500)

Yield from crude

Weight.%

13.84

Yield from crude

Vol.%

11.81

Yield range from crude

Weight.%

86.16-100.00

Yield range from crude

Vol.%

88.19-100.00

Specific Gravity @ 60/60F

0.9884

API Gravity @ 60F

11.7

Kinematic Viscosity :
@ 140F

cSt

17,475.4

@ 160F

cSt

10,694.7

@ 210F

cSt

795.9

Weight %.

2.02

130

Weight.

14.23

138

KUOP

11.3

Total Sulphur
Pour Point
Wax Content
Congealing Point Of Pet. wax
Characterization Factor

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JCHS D-03004/B
Walio Mix

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JCHS D-03004/B
Walio Mix

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18 of 19
JCHS D-03004/B
Walio Mix

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19 of 19
JCHS D-03004/B
Walio Mix

METHOD ANALYSIS

Specific Gravity
Kinematic Viscosity
Pour Point
Flash Point
Reid Vapor Pressure
Water Content
Water and Sediment
Salt Content as NaCl
Total Acid Number
Strong Acid Number
Sulfur Content
Hydrogen Sulfide
Mercaptan
Asphaltenes
Wax Content
Congealing Point of Pet. Wax
Conradson Carbon Residue
Ash Content
Compositional Analysis
Refractive Index
Doctor Test
Copper Strip Corrosion
Octane Number
Freezing Point
Smoke Point
Aromatic Content
ASTM Distillation
PONA Analyses
Diesel Index
Calculated Cetane Index
Aniline Point
Nitrogen Content
Basic Nitrogen
Metal Content
Characterization factor

ASTM D-1298
IP 190
ASTM D-445
ASTM D-97
IP 170
ASTM D-93
ASTM D-323
ASTM D-95
ASTM D-1796
IP 77
ASTM D-664
ASTM D-664
ASTM D-129-64
UOP 163-80
UOP 163-80
IP 143
UOP A-46
ASTM D-938
ASTM D-189
ASTM D-482
Gas Chromatography
Refractometer
IP 30
ASTM D-130
ASTM D-2699
ASTM D-2386-84
IP 57/55
ASTM D-1319
ASTM D-86
ASTM D-1319
IP 21
ASTM D-976
ASTM D-611
ASTM D-3228
UOP 269-70T
AAS
UOP 375

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