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A So ung solubilities inassume ni troy n grams per 100 ml So una ung kay acetone na 10 ml Si compound A meron syang 2.

0 g tpos ung solubility nya kay hot acetone ay 20

Ung 2 g un ung madidisolve Tpos kay B

0.8 g nman ung madidisolve kay B So sa solution, ung A completely dissolved ung B 0.8 g lng ung dissolved so may 7.2 g n matitirang solid Tpos ififilter sya ang matitira nlng sa solution is the 2g na dissolved A tsaka ung 0.8 g n B kse ung natirang solid na B maiiwan na sa filter paper So habang pinapalamig sya at room temp, magcrystallize ung compound A at B so meron nang solid na A na 2 g tpos solid n B na 0.8 grams tpos ilalagay sa icebath From there ung ibang solids madidisolve sa cold n solvent so for A

So may 0.5 g na madidisolve from the 2 g so ung final na A is 1.5 g nlng For B

May 0.01 g na madidisolve from the 0.8 g so 0.79 nlng ung makukuha from B

tatlo ginawa ko una +10mL acetone hot 2nd + 20mL ethnanol hot 3rd + 15mL water hot then tiningnan ko which of the resulting solids would be the most "separated" with acetone i get 1.5g A + 0.79g B with ethanol i get 1.99g A + 3g B

with water i get 1.91g A + 1.425gB so i choose acetone, kase un ung haols 2:1 ration ratio* 7:08pm Angel Manaloto wait. nalito ako bigla. malapit values natin ng narecover for A bakit yung B ibaaa 7:09pm Troy Delos Santos diba, we filter for example if i add 10mL acetone ung solution magiging 2g A dissolved + 0.8g B dissolved + 7.2g B solid upon hot filtration magiging 2g A dissolved + 0.8g B dissolved, maiiwan si solid sa filter paper un ung ilalagay sa ice bath, ung dissolved. tama ba? or ibang procedures ba sinasabi ko hahaha so ang lalabas sa dulo, kapag naicebath mo na ung dissolved shit 7:11pm Angel Manaloto wait wait. tama yung procedures. yung value nung nadissolve and naiwan yung tinitingnan ko 7:11pm Troy Delos Santos 0.5g A dissolved na lang + 0.01g B dissolved na lang so 1.5g A recrystallized + 0.79B recrystallized upon one crystallization. i think ung natitirang 7.2 g sa filter paper, pede pa un irecrystallize using 2nd filtration

7:29pm

Angel Manaloto meron kang 2gA + 8gB na magkahalo nagdagdag ka ng 10mL acetone, for example so that 10mL acetone dissolves all of A, and only something of B that something is 0.8g 7:22pm Angel Manaloto then? 7:23pm Troy Delos Santos so sa solution mo, meron kang 2gA dissolved + 0.8gB dissolved +7.2gB nondissolved

filter mo para makuha lang ung dissolved 7:25pm Angel Manaloto then pano mo nakuha yung recrystallized? 7:25pm Troy Delos Santos ung 2gA dissolved plus 0.8gB dissolved lubog mo sa ice para magamit mo ung solubility na cold

Introduction to Organic Laboratory Techniques: A Small Scale Approach

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