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contents
05 Industry news
PAGE 17
The latest compounding industry news including international acquisitions and alliances, plus new investments and plant openings.
PAGE 25
Peter Mapleston reviews recent developments in screen-changers and melt ltration systems from 12 suppliers in Europe, America and Asia.
70 Compounder of the month: GCR Group - Granic 72 Dates for your diary
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Applied Market Information Ltd AMI House, 45-47 Stokes Croft, Bristol, BS1 3QP, United Kingdom Tel:+44 (0)117 924 9442 Fax:+44 (0)117 989 2128 www.amiplastics.com Head of business publishing: Senior editor: Contributing editor: Designer: Advertisement manager: Andy Beevers Chris Smith Jennifer Markarian Nicola Crane Claire Bishop E-mail: abe@amiplastics.com E-mail: cs@amiplastics.com E-mail: editorial@compoundingworld.com E-mail: claire@amimagazines.com Direct tel: +44 (0)20 8686 8139
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Tosaf has expanded its lab capabilities for developing formulations for films These new and expanded laboratory lines provide strong support to our own development activities. We can now test products by simulating both harsh environments and all the major film packaging production steps that are commonly used in the food and non-food industry, said Tosaf development manager Yafit Moyal. Founded in 1985, Tosaf is a joint venture between Megides and Ravago.
a range of high-performance antioxidants, UV absorbers, nucleating agents and PP clarifiers. Rich Yu has an office and a warehouse in the Netherlands to manage its REACH registrations and its additives distribution in Europe.
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July 2013 | compounding world 5
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Compounding World that the Herne compounding operation (pictured below) would close by the end of the year. She said the cost of updating the facility, which began production in 1980, was not considered viable by the company.
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6 compounding world | July 2013 www.compoundingworld.com
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16 23 October 2013
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Compounding World, Coperion has recently added a new facility for assembling modular lines at its Shanghai site. Going forward, we will benefit from the continually improved efficiency and
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10 compounding world | July 2013
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Compounding World apps, which are helping to grow the truly global audience for our magazine, said Andy Beevers, head of business publishing at AMI. European downloads account for 37% of the total, the Americas represent 33%, Asia stands at 26%, and The Middle East and Africa are at 4%.
12 compounding world | July 2013
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Automation systems.
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International conference on compounding of polyolens focusing on PP and PE materials and applications
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Giulia Esposito, Conference Organiser ge@amiplastics.com Ph: +44 117 924 9442 Fax: +44(0)117 311 1534
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Colloids carried out trials across seven colours of PE film and measured the opacity levels in correlation with Duos own opacity meters to achieved the required 97% level across seven thicknesses between 40 and 100 microns. It then developed a bespoke opacity chart which detailed the required masterbatch addition level for each colour and thickness so the company could avoid over-dosing. As a result, Duo says that it has reduced masterbatch usage by 5% and cut spool rejects by 20%. Duo is celebrating its 25th year in business this year and has just announced a E1.3 million investment in a new co-extrusion line, printing equipment and planning software.
www.colloids.co.uk www.duo-uk.co.uk
Antimicrobials continue to play an important role in protecting plastics from damage by microbes, including bacteria, algae and fungi such as mould and mildew. However, the types of chemistries that are used for biocides compounded into plastics are undergoing major changes with the phase-out in Europe of the traditional workhorse biocide, OBPA (oxybisphenooxyarsine), due to concerns about the toxicity and ecotoxicity of arsine chemistry. Supply of OBPA to the EU market ended as on 31 January 2013 under the Biocidal Products Directive (BPD). Although there are several alternatives, none are equivalent to OBPA. Depending on the microorganism, the alternatives may not always be effective or may require different levels of active ingredient to be effective. Formulations using alternatives may need to be modied to ensure that they are stable and provide maximum cost efciency. Suppliers and their customers have been preparing for years for the potential need to replace OBPA, but it is still a major undertaking. Although OBPA supply is currently allowed in the United States, its use is coming up for a re-registration eligibility decision (RED) with the US Environmental Protection Agency (EPA) in 2014. This re-registration is being backed by OBPA supplier Troy Corporation. Its customers in all regions except Europe can continue to
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The phase-out of some wellestablished biocides means that compounders are turning to alternative antimicrobials both to protect plastics and to reduce hospital acquired infections. Jennifer Markarian reports
use OBPA without any service interruptions, says David Faherty, the companys vice president. However, the leading suppliers of OBPA, Akcros and Dow, are not supporting the RED. Akcros and Dow formed a strategic partnership on biocides in North America in November 2012. Under the agreement, Akcros is the exclusive channel partner for Dow Microbial Controls OBPA and isothiazolinones for the polymer markets in the US and Canada, promoting grades under the Intercide brand. Akcros plans to continue to supply OBPA as long as permitted into 2014 and as stock allows, says Dean Nichols, biocides
July 2013 | COMPOUNDING WORLD 17
Other important biocide properties include heat stability, UV stability, and interaction with other additives in a formulation. To achieve the performance and especially the price/performance of OBPA is quite challenging, says Dr Heinz Katzenmeier, head of innovation at Sanitized. While no single substance is ideal for all applications, properties can be optimized for a specific applications requirements.
Improving stability
Sanitized recently introduced two new products for PVC with improved stability in specific applications. Sanitized PL 12-32 has high water resistance and UV stability, making it suitable for outdoor applications. Sanitized PL 12-33 has high thermal stability to withstand high processing temperatures while retaining transparency; it is targeted for indoor applications, such as flooring and furnishings. Both formulations are designed to reduce initial discoloration and yellowing in use. Sanitizeds new PL 12-32 has high water resistance and UV stability for outdoor PVC applications product manager for Akcros. Several chemistries can be used as alternatives to OBPA in plastics. The primary options are the wellestablished isothiazolinones, which include n-octylisothiazolinone (OIT), dichloro n-octyl-isothiazolinone (DCOIT), and others, such as butylbenzisothiazolinone (BBIT). Other alternatives include Folpet, zinc pyrithione, silver and iodo-propynlbutyl carbamate (IPBC). Katzenmeier says that these combinations of active ingredients are fully able to replace OBPA in the relevant applications. Another new product, Sanitized PL 25-36, is a clear solution with no dispersed particles that is compatible with various polymer matrices, such as PU or PVC. The patent-pending product causes no turbidity and is designed for applications where high clarity is demanded, such as PVC curtains or indoor flooring. A field test at the University of Manchester is currently underway with PVC flooring containing PL 25-36 to demonstrate efficacy under real conditions, and results to date have exceeded expectations, says Katzenmeier. In addition to efficacy and stability, formulators must consider potential interactions with other additives, such as heat stabilizers, antioxidants, and light stabilizers, says Nichols. He adds that Akcros, which produces a wide variety of additives for PVC, has carried out extensive development work to solve interaction issues. One of these solutions is a new isothiazolinonefriendly stabilizer for flexible PVC. Initially these products are available in the EU, but similar products are being rolled out for the US market, says Nichols, who notes that Akcros is also developing stabilizers that are friendly to other biocides. Katzenmeier notes that Sanitized has built up an empirical database that is used to check for expected interactions between recommended antimicrobials and the stabilizer used by a customer. Sanitized has also started a publicly funded project with an academic institution that will scientifically investigate these complex interactions. Some bio-based plasticizers, such as soybean-oil derivatives, levulinic ketals, glycerol esters, and
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Evaluating alternatives
When choosing a biocide, formulators need to look at the spectrum of efficacy against various types of microbes and at the cost to dose at the level needed for efficacy. One measure is minimum inhibitory concentration (MIC), which shows inherent activity of the biocide against a particular microorganism. Another measure, not shown by MIC, is the availability of the active ingredient on the plastic surface, which depends on several factors, including the dosing level and the biocides migration rate through the finished plastic part. The migration rate is affected by the water solubility of a biocide. Although it is necessary for the active ingredient to migrate to the surface to be effective, if it migrates too quickly it can lose efficacy over time. Highly water-soluble actives may show visually impressive zones in agar plate tests, but are more prone to leach out of plastics more quickly than often desired, especially in exterior and high-moisture applications, notes Nichols. Conversely, low watersoluble actives, such as silver and DCOIT, dont show such zones in agar plate tests, which, Nichols warns, can lead to improper conclusions that they cannot be effective.
18 compounding world | July 2013
2.5 times higher throughputs Enhanced mixing quality and dispersion Energy savings up to 25%
isosorbid diesters, are more susceptible to microbial attack compared to conventional, phthalate-based plasticizers. Users who switch to natural plasticizers may require higher levels of biocide, or, in some cases, may need to introduce biocides to products that previously may have been only moderately or even unsusceptible to microbiological attack, comments Nichols. In addition, says Katzenmeier, the tendency of some bio-based plasticizers to cause discoloration is higher, and the whole system including plasticizer, stabilizer and antimicrobial additive must be fine-tuned to achieve good performance in terms of antimicrobial efficacy as well as low discoloration. It is generally understood in the industry that when a formulation is changed, the impact on all properties, including susceptibility to microbiological activity, must be considered, adds Nichols. Microbiological laboratory tests can be used to determine differences in susceptibility.
Lise Moloney, director of business development for healthcare at Sciessent, in a February 2012 article in Compounding World on Specifying silver antimicrobials for medical devices (http://bit.ly/sciessent). We continue to see interest in all the major device-related infection areas: central venous catheters and accessories to central lines (like connectors), urinary catheters, endotracheal tubes and wound dressings and closures, reports Moloney. I think the biggest use and greatest success of antimicrobials in FDA-cleared devices has been in central venous catheters, where the pathogenesis of catheter-related bloodstream infection is wellunderstood and accepted. The need to prevent microorganisms from colonizing the external and internal surfaces of the catheter is critical to preventing these infections. Data published in 2012, for example, found a 90% reduction in catheterrelated bloodstream infections using Agion-treated umbilical venous catheters in pre-term infants. There is also an increasing interest in antimicrobials for surfaces in patient-care areas. Adoption in these applications has been slower because it is harder to demonstrate the direct benefit of treating these types of surfaces and to achieve regulatory clearance for claims against human pathogens than it is with indwelling medical device, says Moloney. Purchasing groups and infection-control practitioners want to know what the benefit will be before they switch to an antimicrobial product.We will see greater demand and acceptance for these products as more data is generated to show a link between surfaces in the healthcare environment and patient outcomes, predicts Moloney. Other areas of growth for silver antimicrobials, outside of healthcare, include food and water products, she adds. BASF, which offers Irgaguard silver-ion antimicrobials for industrial applications, supplies fully compounded polymer systems containing medical-grade, silver-ion releasing HyGentic additives for medical
Silver solutions
Silver-based antimicrobials, primarily those that release silver ions, are effective against bacteria but require higher concentrations to be effective against fungi and algae, thus they are not seen as cost-effective alternatives to OBPA for traditional plastic protection. The use of silver-ion antimicrobials is, however, growing in medical applications. Awareness of hospital acquired infections (HAIs) has led to increased use of antimicrobials in medical devices and other surfaces in healthcare settings, such as masks, gowns, equipment and furnishings. Silver has a long history of efficacy against bacteria, and has been found to be effective against antibioticresistant organisms, such as MRSA. This was covered by
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applications. Grades include HyGentic SBC (styrene butadiene copolymer), HyGentic PA (glass-filled nylon) and HyGentic SA (acrylic modified polystyrene); custom formulations can also be developed in a wide range of plastic materials. BASF is currently developing products that provide added functionality beyond antimicrobial performance, says Stephen Zlock, business development manager for medical device materials at the company. For example, a polyurethane compound with both anti-thrombotic and antimicrobial performance for vascular access devices is in advanced development. PolyOnes WithStand antimicrobial additive solutions, available since 2010, are targeted for medical devices, medical packaging, and other healthcare applications. Last year, PolyOne launched Smartbatch HC additive concentrates, which combine WithStand antimicrobials and OnColor HC colorants for healthcare applications. Last year Clariant added Sanitized MedX silver antimicrobials, which can also be combined with pigments, to its line of Mevopur masterbatches for medical applications. Targeted applications include catheters, surgical instruments, and preservative-free pharmaceutical packaging. Plastics Color Corporation (PCC) recently introduced silver-ion based MicroBlok antimicrobial compounds targeted for medical device, medical packaging, appliance and other consumer markets. Fred Jhaveri, PCCs global technical manager, says that the additive inhibits the growth of bacteria which may cause stains, odours and product deterioration. supplies, healthcare environments, housewares and others. RTP Company uses various organic and inorganic antimicrobial additives in its masterbatches and ready-to-use compounds to meet the needs of specific application requirements. Earlier this year, Sabic launched nine new antimicrobial compounds featuring silver technology. The company says that they have been tested for log reduction values according to ISO 22196-2007. Five of the grades provide a high antimicrobial effect with log reduction values above 4, representing more than a 99.99% reduction in pathogens. The other four compounds have a lower antimicrobial effect with log reduction values below 4, representing a 99.0 to 99.99% reduction in pathogens. The new grades are based on the four Sabic resins that are most commonly used in medical devices: Lexan EXL copolymer, Lexan PC, Xenoy PC/PBT, plus PP resins with and without glass fibre reinforcement. The company says that its optimised antimicrobial compounds offer advantages over adding antimicrobial masterbatch to a base resin, including more uniform distribution of the active ingredient. It also says that its expertise in colour and effects means that it can provide precise control over clarity, a property that can be impacted by antimicrobials. Target applications include fluid and drug delivery systems, surgical instruments, monitoring and imaging devices and durable medical equipment such as
RTP is using NanoBioMatters BactiBlock, which combines silver-ion technology and a nanoclay carrier
Nano-technology options
NanoBioMatters BactiBlock additive is a silver-ion based technology in a nanoclay carrier. The antimicrobial has been used in Europe commercially since 2010 and received EPA registration for use in the US in 2011. The primary difference between BactiBlock and other silver-based solutions is the clay carrier, which has a synergistic effect and works as an efficient delivery system with long-term durability, says Paul Kennedy, business development manager for North America at NanoBioMatters. The ionic silver is linked to the clay surface, which creates a uniform distribution of the active species and prevents platelet agglomeration to ensure additive dispersion throughout the polymer matrix. Several BactiBlock grades are available for a range of polymers and applications. Last year, compounder RTP Company announced that it would use BactiBlock in antimicrobial compounds targeted for applications including furniture, athletic equipment, personal-care items, office
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Sabics new antimicrobial compounds can be used for medical equipment like healthcare scanners
hospital beds and operating tables. Other potential applications outside of healthcare include consumer electronics, automobile interiors, business equipment, or any other surface where there is a desire to reduce the potential transfer of pathogens. Americhem introduced nShield masterbatches in 2012 for inhibiting odourcausing bacteria growth in fibre and plastics for applications including synthetic turf and automotive interiors. Americhem says that the additive is non-migratory and resists discoloration for long-lasting aesthetic appeal. Troys Faherty says that the company has seen some migration away from silver and that it has introduced alternatives, with more in development. Troys Micropel 1000, for example, is designed to impart surface antibacterial properties and offer comparable performance to silver but in a more cost-efficient manner, says the company. Foster Corporation supplies custom formulations of medical-grade polymers containing either silver or polymeric-based antimicrobial compounds that reduce bacterial infection in catheters and sustained bodily fluid contact applications. Last year, Foster announced a partnership with Biosafe to develop and market Biosafes polymeric additive technology based on cationic quaternary ammonium salt, which is seen as a cost-effective alternative to silver additives for infection-resistant medical devices.
selecting and applying antimicrobial additives at the Compounding World Forum 2013, which is being held in Philadelphia, PA, USA on 10-11 December. In addition, Dr Larry Acquarulo, CEO of Foster Corporation, will give a paper at the event entitled Adding functionality and value to medical compounds with novel reinforcements, fillers and additives. For more information on the conference, visit http://bit.ly/CWF2013p. Dr Manish Nandi and Lynn Colucci-Mizenko of Sabic will discuss a multi-pronged approach to meeting HAI challenges with specialty engineered thermoplastics at the Medical Grade Polymers 2013 conference, which takes place in Boston/Woburn, MA, USA, on 17-18 September. For details, visit http://bit.ly/MGP13. Click on the links for more information:
More information
Lise Moloney, director of business development for healthcare at Sciessent, will present a paper on
www.akcros.com www.americhem.com www.basf.com www.biosafe.com www.clariant.com www.fostercomp.com www.nanobiomatters.com www.plasticscolor.com www.polyone.com www.rtpcompany.com www.sabic.com www.sanitized.com www.sciessent.com www.troycorp.com
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Online colour control is an emerging technology with the potential to improve the quality and productivity of compounding, reports Pat Toensmeier
ROC provides the ColorControl System, a remote unit with several components that collect pellets, transport them pneumatically to the unit for measurement, analyse them with an image-processing spectrophotometer in a test cycle of 2.5 minutes, and restores colour to spec in as little as 30 minutes, says Peter Dietrich, board member of the company. Colour correction in both systems is done with miniature feeders that dose the necessary amounts of colour to bring a compound in spec. Though the technologies differ, the companies cite similar advantages from the use of their equipment. The main benet is the time it takes to detect and begin correcting off-spec colour minutes compared with 2-3 hours using conventional procedures. Other advantages include precision analysis. Both systems have software that correct for process-related inuences on colour, whether thermochromatic, as with the Equispec OCS, or stress whitening and other cutting defects caused by pelletizing, as with ColorControl. The ability to rapidly detect and x colour problems means that less compound is lost to waste, reducing scrap and material cost. Fast detection and resolution
Teknor Color uses a special pre-production process to predict how well masterbatches will turn out
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A KraussMaffei Berstorff twin-screw compounder fitted with three Equitech colour spectrometers. Two are side-by-side in the die plate: a reflection probe (foreground) and a transmission probe. A second transmission probe is on the side of the die plate
of colour problems improve productivity, which means that compounders complete runs faster and thus free machine time for more jobs, increasing revenue and profitability, and perhaps even the need to invest in a new line to expand capacity. Reducing the time required to compound materials lowers energy use and contributes to reductions in electricity and other process-related expenses. Both systems can also be used as diagnostic and process-control tools for compounding lines. The companies say that their equipment develops data about feeder stability, screw wear, temperature profiles, screw speed and other parameters. Colour measurement with both systems can, moreover, be done with one operator, which cuts back on labour expense. KraussMaffei Berstorff in the US promotes the Equispec OCS system to customers, and has installed demonstrators on some of its compounding lines. The system is about as accurate as you can get, says Martin Mack, vice president of research and development for the compounding machine maker. He says that interest in online colour measurement and control is growing among compounders. There is a learning curve involved with the system, as with any technology, he acknowledges. But once compounders understand the operation and are comfortable with it, they see the positive impact of online control. Online monitoring opens up every inconsistency in colour, no matter how slight, and sometimes surprises operators, he adds. Masterbatch compounders in particular find both systems extremely sensitive to variations, especially when transitioning from one colour, such as yellow, to another one, like blue. In a case such as this, both companies say that traces of yellow that would be undetectable to the eye can be measured with the
26 compounding world | July 2013
Equispec OCS or ROC ColorControl for as long as 30 minutes after a changeover. The systems also perform well when compounding recyclate, a material that can have a lot of inconsistency when loaded into a hopper. The closed-loop monitoring and control of the Equispec OCS detects colour shifts immediately in compounded recyclate and automatically corrects them to assure uniform pellets. The ROC ColorControl does this as well, though after colour measurement of pellets. Even polymerization lines use systems from both companies for colour control, including transparent resins such as polyethylene terephthalate, polystyrene and polycarbonate. With the transparent materials the benefit is in making certain no yellowing or other discolorations occur. The advantages are also economic. Dietrich points to one major resin producer that installed two ColorControl systems on its compounding lines in Europe. The company, which he declines to identify for reasons of confidentiality, substantially improved colour control, along with the productivity and profitability of operations. Two other European resin producers that use the system were able to increase compounding capacity 40-60% entirely through the productivity gains of the technology, he says. Clearly, there are compelling reasons to consider online colour control, though many compounders, notably those that specialize in masterbatches and other small runs, are currently unconvinced. One is John Wood, technical manager at Teknor Color in the US. Wood believes that online colour control is practical for large-run compounding, but doesnt think it suits the tight tolerances, specialty colours and small volumes that Teknor specializes in with its masterbatches. You would need larger production runs than we do for it to be effective, he
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says, adding that other concentrate houses probably think the same way. Wood says that Teknor uses conventional test methods to measure colour, as well as a special pre-production process the company developed that has been successful in predicting how well masterbatches will turn out. He declines to reveal details about the process, calling it a competitive advantage, but notes that its success rate is high. Furlan says Wood voices concerns he hears from others. Though online colour control technology has been around for a while, it is still not well understood by most compounders. His companys technology is suitable for all processes and colours, he insists, while continuous measurement has benefits in colour consistency and how well a process runs. The Equitech and ROC technologies produce the same result colour control but in markedly different ways. The Equispec OCS system calculates the black and white ratios in a compound (L*), then how much red and green (a*) and blue and yellow (b*) it contains, based on an optical signal transmitted to the spectrophotometer from the melt probe. The resulting numbers are used to determine if colour is in spec. The system compares these values with a pre-programmed colour formulation, expressing them in L*a*b*, L*c*h, Hunter Lab or XYZ units, and provides a trend plot and 2-D colour space plot. Furlan says the technology is accurate to less than one half of one unit. Most people are unable to distinguish between a colour drift of one and two units. The systems Millennium 3 UV-VIS spectrophotometer has a wavelength range of 380-780 nanometres The ROC ColorControl system measures pellet colour in 2.5-minutes cycles
(nm) for reflected colour, and 230-820 nm for transmission. It uses a xenon flash lamp that generates up to 250 pulses in 500 milliseconds. Colour data is stored in the PC-based computing system, which runs Equicolor for Windows software. Stored data lets users develop process archives and run trend histories. The computer has a 12.1-inch touchscreen, Ethernet port, and comes with OPC tags that allow communication to the process control system. Colour control is maintained by the use of special gravimetric feeders, which selectively add colours to a compound based on the closed-loop data to correct imbalances. Furlan says the closed-loop control is a huge benefit for its immediate feedback. He declines to discuss specifics about system price, but says the return on investment for most compounders could be as little as 4-6 months. ROCs colour control technology samples compounds in pellet form. The measuring unit is set up in a clean, air-conditioned location, which can be up to 300 metres (1,000 ft) from the compounding line owing to the length of its pneumatic transport line. The process begins with collection of a small amount of pellets. Samples are continuously collected over a programmed period of time, typically 1-20 minute. The pellets are automatically homogenized within the ContiSampling unit, after which 35 ml (about 1,000 pellets) are sent to the ColorControl unit in a special transport carrier. Each sample represents the average production for a specific period of sampling time. Because the ColorControl operates in a stable measurement environment, the pellets are the only variables. Since pellets and colour are solidified, no changes to colour development need to be calculated. At the ColorControl unit, pellets are unloaded onto a vibratory table, which spreads them out for analysis. When the vibration stops pellets are analysed by the image-processing spectrophotometer, in a process that takes 2.5 minutes. Before every measurement cycle the instrument is calibrated for white and black balance. Afterwards, the software analyses images. Every measured pellets colour is based on up to 1,500 pixels. Each pixel contains a full-spectrum colour wavelength ranging from 500-700 nm in 10-nm intervals. This data, expressed as CIELAB L-a-b values, is used to determine if the colour is in spec. Dietrich says that the self-calibrating software is programmed to filter out stress whitening on the edges of pellets and cutting defects from the pelletizer, along with the surface of the table. The repeatable measuring accuracy of strand- or underwater-cut pellets is high,
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formulation, Dietrich says. ROCs experience shows that 8-12 SPCs correct 90% of colour-control problems. The amount of colour used to bring a run back on spec, moreover, is small: 0.5-2 kg (1.1-4.4 lb) per hour for a line running 900-1,000 kg (1,980-2,200 lb) of compound hourly. Importantly, an operator monitors the effect of a correction in real time. Each ColorControl unit can be used on up to six compounding lines simultaneously. CEO Jens Dietrich stresses the economic benets of the ColorControl system. He cites major savings in manpower and electricity (since stop time is drastically reduced owing to fast colour measurement results), and signicant increases in productivity. Operators also acquire skills through use of the system that enable them to more precisely monitor, Equitechs reection probe accesses melt through a standard adapter opening and is used to analyse the colour of opaque resins with an average of less than 0.1 CIE-Lab points. This degree of precision cannot be achieved with most standard laboratory test processes, he adds. Once an operator receives the measurement results, he corrects off-spec colour by using the ColorDosage system, which comprises six small gravimetric extruders per production line, each containing singlepigment concentrates (SPC) with concentrations of 1-60%. The SPCs represented by the six feeders are usually black and white (for the L value), red and green (for the a value), and blue and yellow (for the b value). Other concentrates can be used depending on Click on the links for more information: adjust and control production. ROC has found that with the system, compounders achieve greater product acceptance rates by customers, due to fewer colourquality errors. ROC works with pelletizing systems maker Gala Industries and the University of Darmstadt in Germany in testing the technology. Dietrich says that 26 compounding lines running 100,000 tonnes/year currently use the system. Online colour control is an emerging technology for compounders. While it requires more promotion throughout the industry and a clear understanding by users of its benets, the competitive advantages and bottom-line protability the technology provides should be an easy sell. The technology may, in fact, become a requirement as compounders look to expand business by enhancing their capabilities.
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Tuesday, December 10, 2013 8:00 9:00 Registration and welcome coffee Opening announcements
C O N F E R E N C
December 10-11, 2013 Hilton Philadelphia City Avenue, Philadelphia, PA, USA
Applied Market Information and Compounding World magazine are pleased to announce the Compounding World Forum, taking place December 10-11, 2013 at the Hilton Philadelphia City Avenue, in Philadelphia, PA, USA. This new conference features a high-level program brought together by the editorial team of Compounding World, exploring and developing many of the magazines most popular themes in a live event. It will provide an excellent opportunity for discussion and networking between the international panel of speakers and delegates. The conference will cover business strategies and new materials technologies, as well as providing practical advice on getting the most from compounding lines. The primary focus will be on the production of technical compounds based on engineering thermoplastics, performance polyolefins and thermoplastic elastomers. Key end-use markets that will be addressed include the automotive, medical, electrical/electronic and consumer goods sectors. A wide range of polymer and additives technologies will be covered including electrically and thermally conductive compounds, antimicrobial formulations, fillers and reinforcements, flame retardants, bio-based materials, and anti-counterfeiting techniques. Strategic business and production issues will also be addressed, including growing a compounding business in a global marketplace, improving sustainability, clean compounding for medical markets, and responding to emerging regulations. In addition, leading experts will discuss how to get the very best from compounding lines with a wide range of practical tips and advice.
Analyzing changes in the global compounding industry Mr. Andy Beevers, Publisher/Editor, Compounding World magazine, APPLIED MARKET INFORMATION Ltd., United Kingdom Growing a profitable formulating and compounding business in a dynamic, global economy Mr. Roger Avakian, Vice President, Scientific Development, POLYONE CORPORATION, United States Implementing clean compounding to meet the needs of the medical market Mr. Paul Burke, Vice President of Manufacturing, TEKNOR APEX, United States
10:40-11:10 Coffee break sponsored by: 11:10 11:40 Metal replacement: Finding practical solutions with technical compounds Mr. Jeffrey McCoy, Manager, Marketing & Business Development, A. SCHULMAN INC., United States Responding to changing regulations in America and beyond Ms. Melissa Hockstad, Vice President - Science, Technology & Regulatory Affairs, SPI: THE PLASTICS INDUSTRY TRADE ASSOCIATION, United States
SESSION 2 ADDING VALUE TO TECHNICAL COMPOUNDS 12:10 Combating piracy with innovative anti-counterfeiting additives for thermoplastics Mr. Stuart Swain, Director of Sales and Marketing, CHROMA CORPORATION, United States
12:40-2:10 Lunch sponsored by: 2:10 2:40 3:10 Selection and application of antimicrobial additives in thermoplastic compounds Ms. Lise Moloney, Director Business Development, Healthcare, SCIESSENT, United States Pushing the limits of polypropylene developing the worlds first all-plastic, mono-material automotive tailgate Mr. Anis Tebib, Marketing Manager Automotive, STYRON, Germany Flame retardancy of engineering plastics Dr. Martin Klatt, Senior Manager Research, BASF SE, Germany
CONFERENCE HOTLINE Contact: Ms. Kelly Cressman, Conference Coordinator Tel: +1 610 478 0800 Fax: +1 610 478 0900 Email: kc@amiplastics-na.com
FIVE GOOD REASONS WHY YOU SHOULD ATTEND: 1. Hear leading experts discuss key trends in technical compounding 2. Discover new additive and materials technologies 3. Learn practical tips for getting the most from compounding lines 4. Gain insights into global market trends and business strategies 5. Network with other professionals in the compounding industry
3:40-4:10 Coffee break SESSION 3 IMPROVING SUSTAINABILITY 4:10 4:40 5:10 A profitable path to sustainable compounding Mr. Jack Leahy, Vice President of Manufacturing, TECHMER PM LLC, United States Engineered wood fibers for a new generation of biocomposites Mr. Christophe Chambonnet, Global Manager, Woodforce, SONAE INDUSTRIA (WOODFORCE), Canada Compounding of bio-based plastics and natural fibers Mr. Dean Elliott, Lab Manager, ENTEK EXTRUDERS, United States
P R O G R A M
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CONFERENCE VENUE Located on the East Coast of the United States, Philadelphia has a major international airport and is just hours away from New York and Washington DC. The city sights include historic buildings, museums, shopping malls and beautiful parks. Philadelphia offers its visitors a multicultural experience with many different types of dining and entertainment. SPONSORSHIP & EXHIBITION SPACE With an exhibition running alongside the conference as well as a range of sponsorship opportunities, there are ample ways to make sure your company stands out at the conference. All options have proven to be successful marketing tools and will effectively increase brand awareness. The table top package includes one complimentary delegate space and allows companies to display their products and services to a highly targeted audience. Sponsorships will guarantee your company logo will be included on all conference promotions and the event website. To book your table top or secure your sponsorship for the Compounding World Forum 2013 please contact the Conference Coordinator. ORGANISED BY: APPLIED MARKET INFORMATION LLC Applied Market Information LLC is the North American operation of Applied Market Information Ltd., Europes leading supplier of plastics consultancy and information services to the global plastics industry. AMI LLC can offer the full range of AMI services and products to North American clients.Together with our well-established European-based operations this means AMI is well placed to provide a truly global research capability to our clients. Based in Reading PA, Applied Market Information LLC can supply all of AMIs European directories and CDs and is developing a whole new range of products for the North American market. Its range of specialized services cover individual consulting services, multi-client reports, conferences and publishing. To find out more about AMIs conference program or any of our other services and products visit our web site at: www.amiplastics-na.com or call the AMI LLC office at: +1 610 478 0800 or email: consult@amiplastics-na.com COMPOUNDING WORLD MAGAZINE Compounding World is the monthly digital magazine for the global plastics compounding industry. Published by AMI, it is available free-of-charge online and via free apps for iPads, iPhones and Android-based devices. www.compoundingworld.com
SESSION 4 ADDING ELECTRICAL AND THERMAL CONDUCTIVITY 9:10 9:40 Adding electrical and thermal conductivity to plastics compounds Ing. Christine Van Bellingen, Product Manager, Carbon Black & Graphite for Polymers, TIMCAL GRAPHITE & CARBON, Belgium Advanced functional fillers for thermally conductive compounds: Key technology for cost reduction in electronic thermal management Mr. Armin Kayser, Director of Business Development, ESK CERAMICS GmbH & Co KG, Germany
SESSION 5 REINFORCEMENTS AND FILLERS 10:10 Adding functionality and value to medical compounds with novel reinforcements, fillers and additives Dr. Larry Acquarulo, CEO, FOSTER CORPORATION, United States
10:40-11:10 Coffee break 11:10 11:40 Integration of design, materials and manufacturing in long fiber thermoplastic composites Dr. Raj Mathur, V.P. Technology & Business Development, PLASTICOMP INC., United States New mineral opportunities in polymers Dr. Saied Kochesfahani, Development Manager, Polymers, IMERYS, United States
SESSION 6 GETTING THE MOST FROM YOUR COMPOUNDING PLANT 12:10 Tips for optimizing twin-screw extrusion Mr. Bert Elliott, Engineering Manager, LEISTRITZ EXTRUDER CORP., United States
12:40-2:10 Lunch 2:10 2:40 3:10 3:40 4:00 Optimizing screw configurations for twin-screw compounding extruders Mr. Adam Dreiblatt, Director, Process Technology, CPM CENTURY EXTRUSION, United States System engineering: The global rise of turn-key compounding lines Mr. Matt Sieverding, General Manager, KRAUSSMAFFEI BERSTORFF NA, United States Taming hard-to-handle ingredients, and increasing loading levels Dr. Paul Andersen, Director, Process Technology, COPERION CORPORATION, United States Afternoon wrap up and questions Conference ends Conference bag sponsored by:
AMI reserves the right to alter the program without notice. The latest program including any new speakers or changes to schedules can be viewed on our website www.amiplastics-na.com
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Ron Beck, R&D manager at Americhem, looks at how colour works, how it is perceived, and the implications for specifying, controlling and measuring colour in plastics
Figure 1: Three examples of light energy with their spectral power distribution: Illuminant A (Incandescent) has a colour temperature at 2,856 K; Illuminant D65 (Daylight) has a colour temperature at 6,500 K; and Illuminant F2 (Fluorescent) has a colour temperature at 4,200 K
www.compoundingworld.com July 2013 | COMPOUNDING WORLD 35
using the same pigment. This is because the two materials have completely different refractive indexes. Diffuse reection, on the other hand, dictates how an object selectively absorbs (or hides) some colour. Start with a white pigmented lm and gradually add colour. For a while the lm will not change in appearance, effectively absorbing the colour. The moment in which the colour begins to be visible is known as the percolaFigure 2: When a green pigment is added to an object it will only reect the green colour, while other colours are absorbed Well begin by looking at the four elements of colour: light, object, human eye (observer), and human brain. Light: Light is a continuum of electromagnetic energy and can be broken into two categories. The rst is source, a device serving to illuminate, while the second is illuminant, a theoretical source of visible light with documented attributes that are used as a basis for comparing colours. Illuminants can represent average incandescent light, direct sunlight, daylight, and more. For example, Illuminant D65 is the standard daylight illuminant that represents average illumination conditions throughout the world. The D stands for daylight and 65 is the temperature, which happens to be 6,500 degrees Kelvin. Illuminant D65, and its counterparts, are represented by a set of tables that can be used to simulate conditions and to view objects, and colour, in controlled lighting. Further, Illuminant F2 represents average illumination conditions for cool white uorescent light (See Figure 1). Object: Now, well move on to what objects do to light. For starters, all objects interact with light in the same ways: G Specular reection refractive index, which is responsible for gloss; G Diffuse reection scattering of light, which is responsible for opacity and hiding; Figure 3: Colour perception is an extremely complex process involving the interaction of the eye, optic nerves and brain G Absorption of light mainly responsible for colour; G Transmission how light passes through the object. Every material reacts with light in these ways. But its to what extent light reects, diffuses, absorbs and transmits with the object that gives it its appearance. Light absorption has a great impact on the colour of a plastic object. For example, when a green pigment is added to an object it will only reect the green colour and all other colours are absorbed by the object (Figure 2). Specular reection is to what extent the light scatters. Imagine you have an object made of polypropylene and an object made of polyester and you use the exact same pigment in both. You will likely nd that the two objects are completely different colours, despite
36 COMPOUNDING WORLD | July 2013 www.compoundingworld.com
tion point. For polymer engineers, this is an important moment. Slight changes in the objects make-up or the pigment can change the percolation point, creating a teetertotter effect when a product is produced. One time the colour is there, the next time it isnt. This is caused by the scattering of light. Light absorption is what truly provides visible colour, which is what is reected back from an object when it is exposed to a light source therefore, the type of light source directly impacts the appearance of the object. Human Eye: Perception of colour is the result of an extremely complex process. While we still do not fully understand how it works, we do know that it involves the interaction of three separate areas: the eye, the optic nerves and the brain. There are two kinds of light-sensitive cells in the eye rods and cones. Rods control sensitivity to light and are responsible for night vision. They are so sensitive that during daylight they turn off. This is why you might feel blind when you enter a movie theatre from a brightly lit street. When the light level falls below their overload threshold, they slowly regain their sensitivity, a process that takes about 30 minutes to complete. Where rods are colour blind, cones step in and are responsible for distinguishing colour. Approximately 7 million cones are packed into the area of the retina called the fovea. They are not nearly as sensitive to light as rods, but are able to distinguish between colour wavelengths.
NEW IN 2013
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Order online or by telephone, fax or email. Contact Matt Wherlock, Tel: +44 (0)117 924 9442 Fax: +44 (0)117 9892128 email: mjw@amiplastics.com All prices are correct at the time of publication but may be subject to change. Please check the Plastics Information Direct website for current prices and shipping charges.
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It is generally accepted that there are three types of cone receptors with each responding to a different range of wavelengths: one is sensitive to the blue region of the visible spectrum, another is sensitive to wavelengths in the green region and the third responds to wavelengths in the red region. Designers are familiar with these colour spectrums as the RGB colour model, which can be used to create an array of other colours. Between the light sensing abilities of rods and the colour distinguishing abilities of cones, the perception of colour begins. Human Brain: All visual data processing is done in an area of the brain known as the visual cortex located at the rear of the skull. Here, all of the signals coming through the optic nerve bundle are sorted and organized. The rst thing it looks for are edges, or discernible differences in colour or brightness. Once it has detected edges, it organizes the edges into patterns. Then, it searches its memory banks to see if any of these patterns are identiable. This is how you can determine if you are looking at a red apple or your Aunt Helen who you havent seen in 15 years. Unlike a shape, a colour cannot be dened. It has no pattern with edges that can be catalogued and later recognized. While the brain has difculty remembering precise colours, it is excellent at comparing colours. If you examine two colours side-by-side, the brain can easily tell whether they are identical. If they are not identical, the brain again has a problem with accurately quantifying the degree of the difference. The brain analyses the signals it receives from the eye, searches for edges, and then considers each
Figure 4: How Many Colours Do You See? Answer: There are only three colours white, green and pink. There seem to be two different shades of pink, but they are really the same. This shows how surroundings can greatly impact appearance
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and metamerism. The latter is a phenomenon in which two objects have a given relationship under one set of viewing conditions and a different relationship under another. This happens because the two objects are spectrally different. Preventing metamerism is dependent on making sure the two examples have the same spectral curve. Figures 5 and 6 illustrate and explain metamerism.
Measuring colour
Figure 5: An example of metamerism There are two ways to measure colour. One is by a visual examination, relying on the human eye. The other is via instruments and equipment. Samples must be pre-qualied to: represent the batch; be free from contamination; be in the same form as the target; and be reproducible within acceptable limits of repeatability. Then, a single sample is chosen as the standard by which all others will be judged. Visual examination: Because visual colour measurement depends on consistent judgment, the observer would need to provide repeatable judgments. Examination by instrument: First and foremost, you must understand the instrument, how it works and its specications. Choose an instrument that gives you the best mix of functions to meet your design needs: Figure 6: Why metamerism happens G Spectral data, including absolute coordinates and metamerism; G Geometry; individually. It is the brains ability to detect edges that makes visual examinations of product designs so valuable. Our optical system can discern specs, streaks and blotches that no spectrophotometer could ever detect. The spectrophotometer would simply average the specs into the overall colour. It also allows us to evaluate surface textures and recognizes specular reections. With all of these factors considered light, object, the human eye and the human brain do all people see colour the same? We most denitely do not. We all have different spectral response curves even with normal colour vision. Then there are also other factors, such as individual colour deciencies and colour blindness that make our perceptions of colour vast and unique person-to-person. What we see is not all about colour. Its all about appearance. Colour, gloss, scattering, light sources, surroundings and temperature all impact appearance. For example, Figure 4 shows the impact of surrounding colours. For one to understand how the human observer sees and evaluates colour, one must have a clear understanding of the light source, how the object modies light, and how the human observer responds to light
40 COMPOUNDING WORLD | July 2013
G Precision and accuracy; G Software, including the ability to complete the necessary calculations, as well as the user interface; It is also important to remember that no instrument can replace the importance of the human eye. An instrument may indicate a fractional difference in colour that may not be discernible to the observer, so allow for some margin of difference to avoid unnecessarily scrapping an entire lot for a difference no one would ever notice.
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and non-contact sensing, the system can be used with textured, uneven, and multi-dimensional materials. It can measure reflected light for solid and semi-solid products, and transmitted light for clear plastics and films. The NC-1 is capable of controlling up to five colour sensors per controller, extending measurements across wide line applications.
www.konicaminolta.com
July 2013 | compounding world 43
EXHIBITING AT K 2013?
Promote your presence at the global plastics show using our global plastics magazines The great thing about the K show in Dsseldorf is that it attracts visitors from every corner of the world. Make sure that these international attendees know where to nd your booth among the 3,000 other exhibitors at this years show by advertising in our targeted magazines. These have a truly global readerships, both online and through our apps for the iPad/iPhone and Android devices (full details in our media packs use the relevant links). Take your pick from these 17 dedicated issues:
August: K 2013 rst look September: K 2013 preview October: K 2013 show issue November: News from K 2013 December: K 2013 review Click here to download the full media pack August: K 2013 rst look September: K 2013 preview October: K 2013 show issue November/December: K 2013 review Click here to download the full media pack July/August: K 2013 rst look September: K 2013 preview October: K 2013 show issue November/December: K 2013 review Click here to download the full media pack July/August: K 2013 rst look September: K 2013 preview October: K 2013 show issue November/December: K 2013 review Click here to download the full media pack
We will be exhibiting at K ourselves, with a well-positioned booth in the North Entrance, plus our highly-experienced and technically-qualied editors will be back in Dsseldorf to report direct from the show. Our special K issues are always very popular, so reserve your advertisement space now by contacting Claire Bishop on +44 20 8686 8139 or at claire@amimagazines.com www.amimagazines.com
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bookshelf
RECOMMENDED READING
Our selection of the latest titles and essential reference works for the compounding industry
PLASTICS ADDITIVES AND TESTING
2013, by Subramanian, 120.00 or 100.00 or $160.00 Brand New. A thorough overview of additive types, testing techniques and quality control. More info/Buy here
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PLASTICIZERS DATABOOK
2013, by Wypych, 215.00 or 180.00 or $285.00 Brand New. Property, performance, health and environmental data on 375 generic and commercial plasticizers. More info/Buy here
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ENERGY MANAGEMENT IN PLASTICS PROCESSING: STRATEGIES, TARGETS, TECHNIQUES AND TOOLS, 2ND EDITION
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NATURAL POLYMERS, BIOPOLYMERS, BIOMATERIALS AND THEIR COMPOSITES, BLENDS AND IPNS
2012, by Thomas, Ninan, Mohan & Francis, 115.00 or 95.00 or $150.00 A wide-ranging exploration of materials and applications. More info/Buy here
Visit www.pidbooks.com for hundreds of recent titles, easy online ordering, special offers and clearance bargains!
Order online or by telephone, fax or email. Contact Matt Wherlock, Tel: +44 (0)117 924 9442 Fax: +44 (0)117 9892128 email: mjw@amiplastics.com All prices are correct at the time of publication but may be subject to change. Please check the Plastics Information Direct website for current prices and shipping charges.
Peter Mapleston reviews recent developments in screen-changers and melt ltration systems from 12 leading suppliers in Europe, America and Asia
task, Kapfer explains. Passage through a pack of screens will provide elongational ow of the polymer melt, and such ow will deform and eventually break up the elongated particles or viscosity inhomogenities into individual droplets. These droplets are then mixed into the polymer melt stream. Screen pack changers have to cater not only for ever-increasing capacity requirements, but also for increases in polymer melt viscosity, says Kapfer. Larger screening areas are needed to accommodate higher line capacities in polymer plants. Increasing only
Coperions high capacity screen candle systems (above) are developed using computerbased ow simulation tools (below)
Nordson Xaloy offers SPC Extended Area systems with cylindrical screens to handle very high throughputs
screen-changer diameters will lead to significantly diverging and converging flow, with serious implications for flow stagnation; the screen area needs to be extended in the flow direction and elongated screen candles are used. Larger screening area has also been accomplished by routing the flow now from outside to inside of the individual screen candles. Today, screen pack changers with screening areas as high as 21,000 mm are in use, Kapfer notes. Such large areas can be achieved with a dual bar design with two screen holder cavities each. Another supplier of filtration equipment for large compounding operations, Nordson Xaloy, says that it has supplied several big producers with its SPC1200EA and SPC1500EA units for lines with outputs from 3 to 30 tonnes/hour. The design is based on a heavy one-piece body, with candles to provide the necessary extended filter area. Cylindrical screens create a low pressure drop, resulting in higher throughputs and longer on-line time between screen-changes, says accounts manager Walter Pieters. He also notes that fast screen changes between the production of different batches can yield important cost savings on such big lines.
ADG Solutions, which is the exclusive North American importer of Fimic equipment, says it now offers filter screens with a size of only 200 microns, and should have a 150-micron screen available later this year. Company president Sandy Guthrie says that this ultra-fine filtration enhances product quality, while the large surface area of the screen compared to that of other screen-changers facilitates polymer flow and ensures a high level of productivity. Another new option is the model SCF-700 screenchanger, which extends the applicability of the Fimic system to recycling operations requiring throughput rates from around 2,700 to over 4,500 kg/hour. The Fimic screen-changer can handle scrap with up to 3% loadings of contaminants without a slowdown or stoppage of the process, and even contaminants close to 2.5 cm in diameter do not pose a problem, according to Guthrie. Purgings average less than 1.13 kg per cleaning cycle and there is minimal discharge of good material along with contaminants, he says. The self-cleaning cycles are subject to automatic PLC control. In each cycle, as molten polymer enters the screen-changer, contaminant accumulates on the screen-plate until back pressure reaches a preset level. This actuates a rotating blade which sweeps the screen and purges the contaminant through a central discharge port. Typically the screen does not need to be touched or changed more often than every week or two, depending on the material being processed. Guthrie cites a recently commissioned installation recycling highly contaminated material with very low melt index. He says the Fimic system is efficiently handling highly contaminated HDPE with a fractional melt index of 0.012 to 0.015 something that apparently other filtration systems were unable to do. Contaminants include dirt, wood, and pieces of aluminium. Austrian company Ettlinger says that operators employ its ERF melt filtration system to efficiently process recycled plastics whose contamination levels reach 18%, a task that it says used to be accomplished using more elaborate means. The filters are available in two variants, with throughput volumes ranging from 1,000 to 2,200 kg/hour depending on the type of material, level of contamination, and filter mesh. Melt passes through a rotating filter drum, and the particles trapped in the melt are removed by an angled
Fimic offers filter screens with a size of 200 microns to increase product uniformity and cleanliness
48
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New Strand & Underwater Pelletizers Sharpening Service Die & Equipment Rebuilds OEM Spare Parts
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Experience the speed and versatility of our new Continuous Hybrid Screen Changer. Instant screen movement Uniform extrusion pressure control Filters a wide range of polymers including PCR, PET & HDPE Compact, energy efficient package
Ettlingers ERF system features a rotating filter drum where trapped particles trapped are removed by an angled scraper
scraper across the entire width of the drum and fed to a high-speed delivery worm. The pressure applied by the scraper and the filter processing speed are regulated in accordance with the melt pressure. The self-cleaning action of the drum as it rotates provides for a large, open filter area that Ettlinger claims exceeds the performance of any disk-type filter. Only minimal quantities of plastic melt are required to remove the particles, and the higher the contamination level, the more efficient the system becomes. Processing a mixture with 18% aluminium flakes, for example, uses 10-12% of the melt. The large filter area also minimizes pressure fluctuations to +/- 2 bar at the exit point of the system, thus eliminating the need for a downstream melt pump in some extrusion systems. Eight filter screens are available, with sizes ranging from 80 to 1,000 microns, and can be used to filter all non-mineral-based contaminants. Kreyenborg describes an application in a recycling plant with strand pelletizing, which is benefiting from the use of one of its V-type screen-changers with integrated self-cleaning function of the screens. Strand breaks are things of the past when using the V-type, Kreyenborg claims, owing to its constant melt pressure. The customer mainly processes film remnants from PS and PP that contain a high level of contamination. The system was installed over three years ago, but despite the high mechanical demands on the screenchanger, there are no signs of fatigue after more than 51,000 back-flush cycles. One cycle comprises the flushing of all four screen cavities, of which there are always at least three in production. An overhaul due to rework or wear of the seals is not necessary when using a piston screen-changer because there is no leakage, says Kreyenborg. The screen-changer makes more than one hundred back-flush cycles with the same screen pack. Then the screens are changed as a precaution to avoid fatigue of the mesh, and to prevent the bypass of dirt particles around the boundary edge of the screen packs.
Kreyenborg says that strand breaks are things of the past at a recycling plant that is now using its V-type screen-changer
consumption and lower material removal, yielding a much higher return on capital investment. The KC (Key Continuous), originally developed for TPEs and also hot melts, employs an external hydraulic screen puller to move a proprietary screen across the melt channel. The KCN (Key Continuous, Non-actuated) is based, like several machines from other suppliers, on the design principle of the original Autoscreen developed by Dr Peter Kalman in the UK. It is simple to use and uses widely available RDW filter belts, but the operating window is quite narrow. It does not work on TPEs and hot melts. In developing the KCH (Key Continuous Hybrid)
50
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the goal was to combine the best properties of the KC machine, the external puller and instant operation, with the best properties of the KCN, the better flow channel and RDW screen use, into one machine, says Whaley. Our target was the growing TPE/TPO market and its need for continuous filters that offer constant and uniform control of extrusion pressure. The KCH uses a dedicated PLC to monitor extrusion pressure and quickly react by moving the screen to keep the extrusion pressure constant and uniform. With the same machine and the same screen, the KCH has demonstrated the ability to process polymers from TPEs as low as 25 Shore A scale through to acrylics with hardness up to 125 Rockwell R, all with leak-free, uniform pressure operation. In compounding, uniform extrusion pressure is paramount to quality mixing as well as rate control in the extruder, Whaley says. Because the KCH can move the screen very slowly across the melt stream, there is no pressure disruption throughout the entire production run. The unit also can be adapted to match the configuration of a twin-screw extruder to maximize the flow area. With the twin-screw configuration, the flow path is minimized, making the 8-o cross-section transition through the screen-changer such that the dwell time between screw tips and die is very short. Also highlighting the advantages of screen changes that can keep the compounding process constant is Melt Filtration Products. Its new AutoScreen Max is designed to provide compounders with uninterrupted extrusion during screen changes. It incorporates AutoScreens Extrusion Pressure Control (EPC) system that automatically maintains a selected melt pressure
delta. This feature keeps the melt pressure entering the pelletizing die within a selectable pressure range, regardless of changes in material bulk density or contamination levels. The result is a continuous, stable and uninterrupted compounding process. The AutoScreen Max has a small footprint and requires no hydraulics or pneumatics, plus there are no breaker plates or screen packs to replace.
Parkinson Technologies says that its Key Filters KCH continuous belt filter offers several advantages for compounders
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PUMP, PELLETIZING & FILTRATION SYSTEMS
Maag Pump Systems AG Aspstrasse 12 8154 Oberglatt Switzerland T +41 44 278 8200 welcome@maag.com www.maag.com
enable material colour and grade changes to take place as fast as possible. However, in order to take account of these additional requirements, Gneuss has developed special versions, with the design individually tailored so that inlet and outlet configurations are exactly matched to the extruder and the die, he says. For example, the inlet of the screen-changer can be designed effectively as an extension of the extruder The pre-flood system on Berhalters Becoscreen screen-changer redirects the flow of material into the awaiting cassette removed for cleaning on the other. The material flow is directly through the screen-changer, without division of the melt into multiple channels. This way, Berhalter says, there are no dead spots. Berhalter claims the Becoscreen is the only system on the market that can bring a 100% clean filter medium into the melt stream at each change. The function of our continuous screen-changer is not restricted, the company says. This is made possible by a pre-flood system, which redirects the flow of material into the awaiting cassette. The Becoscreen is said to work completely maintenance-free and leak-free, and can be used for almost all polymers. Econ will present a screen-changer with what it says is a brand new sealing technology at K2013. Again, it is not giving many details away prior to the show, but does say that high availability of the screen area (at least 75% is always in the melt flow, while 25 % is being back-flushed) leads to less back pressure and reduced energy consumption. The pistons are leak-proof, even with low viscosity materials, while blockages are prevented even with highly viscous material due to the prevention of abrasion and deposits. Blockages resulting from thermal expansion are also prevented. Dead volume is minimal, so quick material changes are possible. Econ also claims that the risk of spattering hot melt has been reduced, improving safety. screw barrel with the screws running inside it and the outlet side can be directly integrated with the strand die. In this way, the volume of material inside the screenchanger is minimised and colour / material or material grade changes can be carried out extremely quickly. For extreme cases where the types of materials processed mean that there is no alternative to periodically cleaning inside the screen-changer manually, Gneuss has devised a version in which all parts in contact with the melt can easily be removed for cleaning (for example in a pyrolysis cleaning furnace). It is even possible to supply the screen-changer with a second set of clean parts so that these can be ready for swapping, Prangnell notes.
Chinaplas unveilings
Chinaplas in May was the scene for several new product introductions. Exhibiting on home soil was leading Chinese screen-changer producer Anji. It announced two new product lines for compounding lines: a drum screen-changer with a very high filtration area, and a single-plate unit with back-flush. The first of these features what company representative Cao Wang calls a unique design of flow channels to achieve a greatly increased filtration area in the range of 1,800-5,650 cm2 in a compact design. Two drum-type filters with large filtration areas ensure continuous production during screen changing. A built-in static mixer improves product stability, while a superior sealing system is claimed to eliminate polymer
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Maag has developed filtration units with arched filters to maximize the surface area
The new single-plate screen-changer with back-flush is an improved version of an existing Anji unit. A special sealing system design is said to enable automatic compensation on the sealing gap during screen changing to eliminate polymer leakage. Wang says that Anji, which holds around 20 Chinese patents on screen-changers, has compounding customers all over the world, although not surprisingly China is still its most important market. Our customers are demanding even higher efficiency and production quality, says Wang. Trends we see in screen-changers include larger filtration area, more automatic operation, and minimum polymer flow fluctuation during the screen changing process, and also self-cleaning capability. Normally, our customers will take screen-changers with automatic control system and a larger filtration area to reduce the labour cost and increase productivity. Also at Chinaplas was Maag, with a system combining a SSC 076 screen-changer and an Extrex 45-5GP gear pump. Maag describes its screen-changers and melt pumps as work horses optimized for the application requirements for which they are built. SSC continuous single-piston screen-changers have two screen cavities and operate without any mechanical seals. The SSC 076 has a screen diameter of 76 mm, Click on the links for more information: and a filter area of 45 cm2. It can handle throughputs of up to 300 kg/h. Other SSC models have filter areas of up to 572 cm2, for maximum throughput of 4.7 tonnes/hour. Earlier this year, Maag announced that it had supplied an innovative screen-changer filter design for the worlds largest PET production line based on Uhde Inventa-Fischers MTR Melt-to-Resin process, which is located in the Middle East. Maag developed tailor-made filtration units with arched filters to maximize the filtration surface area while maintaining a compact footprint. The patentpending design guarantees a very low melt residence time, especially for high viscosity resin applications.
www.coperion.com www.xaloy.com www.fimic.it www.adgs.net www.ettlinger.com www.kreyenborg.com www.parkinsontechnologies.com www.meltfiltrationproducts.com www.berhalter.ch www.econ.eu www.gneuss.com www.anjiplast.com www.maag.com
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AMIs Directory
New 2013
AMIs Directory
Injection moulders
3E SP. Z O.O.
Type: Custom, Proprietary Products Polymers processed: PS, ABS, LDPE, HDPE, PP, PMMA, PC, ASA. Polymer throughput: Less than 50 tonnes Markets served: Automotive, Electrical, Alarm Cases. Services offered: Pad Printing, Silk Screen Printing Number of machines: 4 Minimum lock: 120 Maximum lock: 268 Minimum shot: 5 Maximum shot: 600
ACE LUXE
Type: Custom, Proprietary Products Polymers processed: ABS, PC, Elastomers. Polymer throughput: Between 1001 - 1500 tonnes Markets served: Telectron Services offered: Assembly Number of machines: 13 Minimum lock: 270 Maximum lock: 850 Maximum shot: 2500
3E SP. Z O.O.
ul. Okrna 1B 19-300 Ek Tel: 087 620 1630 Fax: 087 620 1630 E-mail: a.sznelinska@3E.net.pl Website: www.3E.net.pl Contact: Mr. Z. Hodyk, Plant Manager Parent company: Privately Owned Processes operated: Injection moulding
Type: Custom Polymers processed: PS, LDPE, PP Polymer throughput: Less than 50 tonnes Markets served: Household, Clothes Hangers. Services offered: Hot Foil Stamping Number of machines: 10 Maximum lock: 20 Minimum shot: 30 Maximum shot: 200
Type: Custom, Proprietary Products Polymers processed: PS, ABS, PP, PA, PC, PET Polymer throughput: Between 101 - 250 tonnes Markets served: Electrical, Electrical Connectors Services offered: Assembly Number of machines: 11 Minimum lock: 60 Maximum lock: 160 Maximum shot: 200
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Over the past decade polymer consumption has grown on average by 4% per year in Poland Make sure you know all about this dynamic industry
Companies included: Injection moulders Blow moulders Rotational moulders PE lm extruders Sheet extruders Cable extruders Pipe extruders Prole extruders Tube and hose extruders Compounders and masterbatch producers
6th edition
AMIs Directory
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POLYMER F O A M 2013
International conference on blowing agents and foaming technology for polymer materials
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Global demand for TPEs continues to grow, fuelled by material enhancements, design innovation and regulatory opportunities. Chris Smith reports
Coming from a background in custom compounding, Teknor Apex works in a wide range of application areas and its TPE division supplies all major end-use markets. Salkahar says the company currently sees the most promising growth prospects in the transport, medical and consumer sectors. A key factor in the growth in TPE applications has been substitution of thermoset rubbers. To take one example, our Sarlink TPEs are well established as replacements for EPDM rubber in sealing applications, but more of this replacement business remains to be captured, says Sakhalkar. While substitution of traditional rubbers will continue to present opportunites for TPEs, he also sees substitution of thermoplastics as a developing trend. Much of the future growth will involve TPEs replacing other thermoplastics or even making possible altogether new applications, as in some of the soft-touch products, he says. Teknor Apex also sees considerLeft: The Vapur closure is moulded in Thermolast K TFBNB, a 45 Shore A grade
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Main image: Kraiburgs Thermolast K TPE is used to produce the closure for US-based Vapurs Anti-Bottle water bottle
service. Earlier this year, the company announced it is working with Shell to incorporate the latters Risella X synthetic process oil into its TPEs. Produced from natural gas, the chemical structure of Risella X is said to differ from mineral oil-based alternatives and the process oil is claimed to display improved compatibility with the TPE matrix. At the moment we are in an early phase creating samples, says Goldman, who adds that the chemistry is expected to be particularly beneficial in the formulation of non-polar TPEs. We expect a positive influence on the hardness and haptics of our products. TPE suppliers put a great deal of effort into developing products for specific applications, but they also benefit from changes beyond their direct control. Goldman cites the example of the move in the automotive industry from toughened to laminated glazing, which is more susceptible to damage during encapsulaAbove: Phillips used a GLS TPE formulated to meet demanding fatty food contact regulations for the seals in its Avent breast milk storage containers able opportunity in high performance TPEs delivering the performance currently expected of TPVs. Sakhalkar says the company will introduce a number of new SBC grades to its Sarlink TPV product line over the coming months. These will include grades for automotive applications such as glass encapsulation, corner mouldings, airbag covers and mats. Environmental issues are also likely to play a growing part in TPE selection in the future, according to Sakhalkar. We are engaged in developing TPEs based on renewable resources. The challenge is to produce compounds that provide cost-performance profiles comparable to standard TPEs. We expect to reach that goal, he says. tion. The companys high flow grades allow mould pressures to be kept low to avoid unacceptable breakage rates, he says. While Hexpol TPE sees the European market going through a period of consolidation over the next few years, this is compensated for by activity elsewhere in the world, according to European sales coordinator Sven M Drewen. Asia-Pacific, the US and South and Central America are all forecasting good growth, he says. With an increasingly sophisticated consumer market in Asia, demand is rising for TPE compounds that provide the right combination of functional performance attributes as well as soft-touch aesthetics, says Drewen. While there is some evidence of re-shoring in certain sectors, we feel Chinas economy will continue to be a global driver. Hexpols history is in the rubber industry, so its decision to invest in TPEs through the acquisition of first Elasto (formerly Vita Thermoplastic Polymers) and then Mller Kunststofftechnik could be viewed as acceptance that the days of traditional rubbers are numbered. However, Drewen says the company sees the two materials as essentially complementary. We were very aware of the rubber versus TPE debate. However, we quickly realised with the Elasto acquisition, and further when Mller Kunststoffe joined our family, that TPEs are used in a diverse variety of applications that would never be made from rubber, particularly in the consumer, packaging and medical sectors. Likewise there are many applications where TPE
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Regional attractions
While the growth expectations for the major world regions differs, Kraiburg-TPE head of corporate marketing Lars Goldman says each has a specific attraction to the company, which supplies into almost all end use markets. All three regions have their driving forces and are of similar interest, he says. In Europe the demands for Right: The Happy Ears earplugs are moulded in a Mediprene TPE developed for medical industry requirements by Hexpol TPEs Elasto division
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quality 2-K component parts will still increase and in the other regions the demand for TPE will grow in general. Both customer demands are very interesting for us. Goldman says there is a clear requirement from customers for materials with higher levels of mechanical performance and temperature or oil resistance. While demand for these special grades may currently be relatively small, it is an area Kraiburg believes it is well positioned to
Drewen says rst generation polyolen TPEs were able to replace rubber at service temperatures between -50C and 130C and in non-oily and non-fatty environments, then second generation products lifted the limits to 200C and to oily and fatty environments. But the mechanical properties will never reach the level of thermoset rubber so there will be always a need for a smart part design if you want to make use of the benets of TPEs, he says. We continue to work on the advancement of properties, be it temperature resistance, compression set or new processing techniques. But growth is also being driven by trends in product design and end-use application performance, he says. Drewen cites the increased use of TPEs in packaging caps and closures applications, where manufacturers are looking to innovate by including soft-touch areas to their packaging, as just one of many examples of this design innovation trend. new attributes to designers. TPE use in entirely new applications remains a strong driver for growth. As designers in consumer and packaging industries look to differentiate themselves in the market place they look to TPEs to enable new solutions, from haptic and appearance to functional performance, says Page. Novel TPE formulations continue to expand the boundaries of possibilities. New smart materials are being developed including shape memory TPEs that are able to x a deformation semi-permanently, and retake their original shape after exposure to hot water, he says. And the performance of vibration damping and barrier materials has been expanded with low compression set TPE products that increase the number and type of applications they can be selected for. Click on the links for more information: Above: High ow TPEs can minimise glass breakage during encapsulation of laminated automotive glazing elements
Regulatory impact
Regulatory change can also act as a driver for TPE growth. TPEs are being selected to replace traditional materials in packaging and healthcare applications for improved regulatory compliance, patient and consumer safety and design exibility, says Charles Page, global marketing director with PolyOnes GLS Thermoplastic Elastomers business. For example, GLS was able to fulll Philips Consumer Lifestyles requirements for its breast pump application, including compliance with the US Food and Drug Administrations rigorous 21 CFR 177.2600 standard governing the use of TPE materials intended for repeated contact with fatty foods, he says. Page says that TPEs also continue to rise to the performance requirements of industries such as the automotive industry, where higher efciency levels have driven up temperatures under the hood, and to deliver
PHOTO: BMW
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flame retardants
www.addivant.com
compatibilisers stabilisers
www.wacker.com
nucleation
Samples quantities are available now, although Teijin says it will not have commercial quantities until 2015. The additive is said to already comply with current Japanese and European harmful substance regulations.
The new masterbatch is designated LD-0392NU and uses proprietary Ferro technology, which is claimed to enhance the cellular
structure and the thermal and mechanical compression behaviour of low density polyethylene foams.
www.ferro.com
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July 2013 | compounding world 63
polyamide compounds
www.basf.com
clarifiers
According to Thierry Laurent, who heads up Roquettes plant-based chemicals business unit, polypropylene producers in Europe will welcome its decision to re-enter the clarifier business as it presents them with an alternative source of supply. Roquette has in the past supplied first and second generation clarifier products and until 2004 had a distribution agreement with Ciba, which supplied Roquette-manufactured products under the IrgaClear name. Milliken, meanwhile, has
announced that it has filed lawsuits against a number of Asian producers that it claims are infringing its patents relating to third generation DMBS clarifiers. The company says that while some of its manufacturing patents have recently expired it still holds IP covering specific areas, including certain blends. While Milliken has made it clear it will take steps to enforce its Millad 3998 intellectual property, the company has also told
NX8000 fourth generation nonitol-based clarifier, which maintains solubility at lower processing temperatures and is less dependent on polymer orientation. Millikens market manager for plastic additives for the EMEA region (Europe, Middle East and Africa) Sami T K Palanisami says that more than 200 PP grades are available worldwide already using the NX8000 product and the company estimates the product already accounts for 70% of the clarified PP market.
www.roquette.com
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Stephanie Berchem Conference Coordinator sb@amiplastics-na.com Ph: +1 610 478 0800 Fx: +1 610 478 0900
laser marking
www.rtpcompany.com
Infinity Compounding launched its new line of Inhibit antimicrobial concentrates and compounds at the MD&M East show last month. The new grades are based on silver functionalized clay and are claimed to prevent the growth of bacteria, fungus and other microorganisms in a variety of applications. The silver/clay platelets are designed to release their antimicrobial effect to the surface of a moulded or extruded part at a controlled rate for several years. Current tests of the products efficacy against staphylococcolour or surface appearance. Concentrates up to 25% nominal additive loading are available in many engineering resins, including PP, PE, ABS, PC, PC/ABS, PA, PBT, POM, PEI, PES and PEEK. With the ability to add antimicrobial functionality to any structural, lubricated, electrically active or coloured custom compound, we are able to help our customers achieve a fully functional antimicrobial product, says Tim Carroll, the companys vice president. Infinitys new Inhibit antimicrobial formulations are effective against staphylococcus aureus
www.tosaf.com
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cus aureus indicate very strong antimicrobial activity at loadings as low as 1% by weight with no effect on
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PLASTICS IN PHOTOVOLTAICS
2 0 1 3
International conference on backsheets, encapsulants and other polymer materials in photovoltaic systems
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Amanda Schaeffer Conference Coordinator as@amiplastics-na.com Ph: +1 610 478 0800 Fx: +1 610 478 0900
Polyolen Additives
PolyolefinAdditives2013
International conference on compounding of polyolefins focusing on PP and PE materials and applications
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The sixth Polyolen Additives conference is being organised by AMI in Dsseldorf, Germany on 10-12 September. The programme covers the latest developments in a variety of additives for improving the properties, durability and appearance of PE and PP.
AMIs next conference on Medical Grade Polymers takes place in Woburn/ Boston, Massachusetts, USA, on 17-18 September. Download the brochure, which has the full programme with its impressive selection of expert speakers.
AMI is running the eighth international Fire Resistance in Plastics conference on 12-14 November in Cologne, Germany. The high-level programme covers the latest technology developments, market trends and regulatory changes.
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The fth Flexible Packaging Middle East conference is being held in Abu Dhabi, UAE on 9-11 December. Download the brochure to see the full programme, which features expert speakers covering the latest materials and processing technologies.
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AMIs eighth international conference on Thin Wall Packaging takes place on 3-5 December in Cologne, Germany. The programme includes speakers from throughout the supply chain for thermoformed and injection moulded packaging.
The international conference on business strategies and new technologies for compounders
Images courtesy of: Faech Plast As, Micvac, saentis Packaging AG and silgan Plastic Food Containers
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To see our full line-up of more than 25 plastics industry events over the next 12 months, please visit www.amiconferences.com
COMPOUNDING
ADVANCED RECYCLING
NATURAL FIBERS
DIRECT EXTRUSION
LAB SYSTEM
www.icmasg.it
This brochure focuses on Enteks extrusion solutions for compounding. It covers the companys E-Max twin-screw extruders, its ability to offer complete turn-key systems, and its comprehensive spare parts service.
If you would like your brochure to be included on this page, please contact Claire Bishop. claire@amimagazines.com. Tel: +44 (0)20 8686 8139
Product line:
Product strengths:
Forthcoming features
The next issues of Compounding World magazine will have special reports on the following subjects: August PVC plasticizers Functional llers First look at K 2013 September Pigments and colorants Materials testing and analysis K 2013 show preview
Editorial submissions should be sent to Andy Beevers: abe@amiplastics.com For information on advertising in these issues, please contact Claire Bishop: claire@amimagazines.com Tel: +44 (0)20 8686 8139
Injection World July/Aug The July/August edition of Injection World has special features on: durable applications for bioplastics; the latest automation systems; optimising hot runners; developments in claried PP; and getting ready for K 2013. Click here to view
Injection World June The June issue of Injection World is packed with information on the latest trends in caps and closures, in-mould labelling and polymer distribution. In addition, it has useful tips on hot-runner control, cold-runner design and colour measurement techniques. Click here to view
Pipe and Prole July/August This issue of Pipe and Prole Extrusion examines the latest developments in recycling technology, window proles, testing procedures for pipes, and control and instrumentation systems. It also has useful links to prepare for your visit to K 2013 Click here to view
Film and Sheet June The June issue of Film and Sheet Extrusion is lled with features on the following: barrier materials for boosting shelf life; recent developments in bioplastics; sustainability trends in thermoforming; and the latest control and instrumentation systems. Click here to view
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AMI conferences
10-12 September 16-18 September 17-18 September 12-14 November 19-21 November 10-11 December 28-30 January 18-20 February 24-26 February 11-13 March 18-20 March Polyolefin Additives Agricultural Film, Madrid, Spain Medical Grade Polymers Fire Resistance in Plastics, Cologne, Germany Polymer Foam, Hamburg, Germany Compounding World Forum, Philadelphia, PA, USA Thermoplastic Concentrates, Coral Springs, FL, USA Grass Yarn & Tufters Forum, Barcelona, Spain PVC Formulation, Dsseldorf, Germany Cables, Cologne, Germany Green Polymer Chemistry, Cologne, Germany
2014
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