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1 Jirka, A.M.; Carter, M.J., Analytical Chemistry, 1975, 47(8), 1397 2 Federal Register, April 21, 1980, 45(78), 26811-26812. Thang o 0-15000mg/L
Tin trnh ph mu
1. ng nht 500mL 2. Bt thit b nung mu trong 2 pht DRB200. Cho gia trong my xay. nhit n 1500C.
Ch : i vi thang o 0-15000 mg/L, ng nht 100mL. mu xay ra cc 250mL. mu khuy t trong khi ht mu. iu ny gip tng chun xc v lp li. Ch : Xem hng dn s dng DRB200 chn chng trnh ci t sn theo nhit ph hp.
3. M np y ng thuc th COD theo thang o thch hp. Nng mu (mg/L) 0 n 150 0 n 1500 0 n 15000 Loi ng thuc th COD Thang thp Thang cao Thang cc cao
4. Gi ng nghing 45 . Dng pipet nh mc cho vo 2mL mu (hoc 0.2 mL i vi thang o 0 n 15000 mg/L)
Ch : i vi thang o t 0 n 15000 mg/L, s dng TenSette pipet ly 0.2 mL thay v 2 mL. c kt qu phn tch chun xc hn th phn tch ba mu c gi tr trung bnh. Ch : Thuc th b trn s nh hng n chun xc v gy hi n da hoc ph hy vt liu nu tip xc. Khng tip tc thc hin test vi ng b thuc th. Nu b trn, lp tc ra sch vi nc.
Ch : Thuc th nhy vi nh sng. Gi cc ng COD cha s dng trong hp cha hoc trong t lnh nu c. nh sng chiu ti ng trong qu trnh phn tch th s khng nh hng n kt qu.
Phng php 8000, COD dng cho my DR890, dch bi Hach Vit Nam
Ch : Mt s ha cht v dng c s dng trong quy trnh ny c th c hi cho sc khe v s an ton ca ngi s dng nu khng c s dng ng cch v c tai nn khng mong mun xy ra. Hy c ton b cc phn v bo m an ton v cnh bo ca ti liu ny. eo knh bo v v bo h. Nu c tip xc ha cht, ra sch khu vc b nh hng. Tun th theo cc hng dn mt cch cn thn.
7. Chun b mu trng bng cch lp li cc bc 3 n 6 thay mu bng pipet 2mL nc kh ion (0.2 mL i vi thang o 0-15000 mg/L)
Ch : m bo pipet sch Ch : Mt mu trng cn cho mt lt test cc mu. Thc hin mu v mu trng cho cng mt l thuc th ging nhau (Lot# c ghi trn nhn hp cha)
ng
Ch : Nhiu mu c th phn hy nhanh hn. Nu cn nh gi, c th ly mu c (trong khi ng cn nng) sau mi 15 pht cho n khi thy gi tr c khng i. Lm ngui mu n nhit phng c kt qu cui cng.
Phng php 8000, COD dng cho my DR890, dch bi Hach Vit Nam
11. S dng mt trong cc phng php phn tch sau xc nh COD: Phng php so mu 0-150 mg/L Phng php so mu 0-1500 mg/L Phng php so mu 0-15000 mg/L
1. Chn chng trnh phn tch COD ci t sn trong my, thang o thp. Nhn phm: PRGM Mn hnh s hin: PRGM ?
3. t adapter COD/TNT vo trong bung cha cell bng cch xoay adapter n khi khp v tr. Sau y n xung.
Ch : tng hiu qu phn tch, mt di bng khuch tn bao quanh ly cc l truyn nh sng trn adapter. Khng tho di bang ny ra.
Phng php 8000, COD dng cho my DR890, dch bi Hach Vit Nam
7. Nhn: ZERO Con tr s di chuyn bn tri sau mn hnh hin th: 0 mg/L COD
11. Nhn: READ Con tr s di chuyn bn tri sau mn hnh hin th kt qu: mg/L COD
Phng php 8000, COD dng cho my DR890, dch bi Hach Vit Nam
1. Chn chng trnh phn tch COD ci t sn trong my, thang o cao. Nhn phm: PRGM Mn hnh s hin: PRGM ?
3. t adapter COD/TNT vo trong bung cha cell bng cch xoay adapter n khi khp v tr. Sau y n xung.
7. Nhn: ZERO Con tr s di chuyn bn tri sau mn hnh hin th: 0 mg/L COD
Phng php 8000, COD dng cho my DR890, dch bi Hach Vit Nam
11. Nhn: READ Con tr s di chuyn bn tri sau mn hnh hin th kt qu: mg/L COD
Ch : Khi dng ng thuc th TNT thang o cc cao th nhn kt qu vi 10 Ch : c kt qu chun xc vi mu gn 1500 hay 15000 mg/L, lp li phn tch vi mu pha long.
Phng php 8000, COD dng cho my DR890, dch bi Hach Vit Nam Kim tra s chnh xc trong dy o 0 n 15000 mg/L vi dung dch chun 10000 mg/L COD. Chun b dung dch chun 10000mg/L bng cch ha tan 8500 mg (120 C, kh qua m) potassium acid phthalate (KHP) vo 1 lt nc kh ion. Ly 2.0mL ca dung dch ny lm mu, kt qu d kin thu c phi l 10000 mg/L COD.
Thuc th thay th
Mercury-free COD2 Reagents khng c cha thnh phn c hi c th s dng trong th nghim khng cn bo co. i vi ng dng trong kim sot quy trnh, thuc th COD2 s loi tr vic thi b thy ngn v tit kim chi ph x l cht thi nguy hi. Nhng thuc th ny hon ton thch ng vi cc quy trnh th nghim v cc ng cong chun c ci t sn trong my quang ph. Cn xc nh thnh phn chloride v ammonia cho kt qu chnh xc cao. Ghi ch: Nhng thuc th ny khng c USEPA chng nhn dng cho mc ch bo co. bit thm thng tin chi tit, xem COD Reagent Vial Information Brochure, Lit. No. 1356.
Cc cht cn tr
Chloride l cht cn tr u tin khi xc nh nng COD. Mi ng COD cha mercuric sulfate loi b cn tr do chloride theo mc trong bng 1 bn di. Mu c chloride cao phi c pha long gim nng chloride theo nh ct 2 trong bng. Nu pha long mu lm nng COD thp qu, kh o chnh xc th cho 0.5g mercuric sulfate (HgSO4) (Cat. No. 1915-20) vo mi ng COD trc khi cho mu vo. Phn b sung ny s lm tng nng chloride ti a cho php c nu trong ct 3.
Phng php 8000, COD dng cho my DR890, dch bi Hach Vit Nam Bng 1
Ct 3 Nng Cl ti a trong mu khi cho thm 0.50 HgSO4 (mg/L) 8000 4000 40,000
Tm tt phng php
Kt qu o mg/L COD c nh ngha l mg oxy c tiu th trn 1 lt mu di iu kin th nghim. Trong th nghim ny, mu c un trong 2 gi vi tc nhn oxy ha mnh l K 2 Cr2O7 . Cc cht hu c c th oxy ha c phn ng, kh ion dichromate ( Cr2O72) thnh ion chromic xanh (Cr3+). Khi s dng phng php so mu trong dy 0 n 150mg/L, tng lng Cr6+ cn li c xc nh. Khi s dng phng php so mu 0-1500 hay 0 n 15000 mg/L, tng lng Cr3+ sinh ra c xc nh. Thuc th COD c cha bc v ion thy ngn. Bc l cht xc tc v thy ngn c dng hn ch cht cn tr clorua.
Phng php 8000, COD dng cho my DR890, dch bi Hach Vit Nam
Dng c cn thit
Cc thuc th thay th
Cc thuc th ty chn
Phng php 8000, COD dng cho my DR890, dch bi Hach Vit Nam
Dng c ty chn
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