Oxalic acid chit xut t sn phm OTC The Way d dng c vit bi Ning HTML ca Rhodium Trong qu trnh

thc hin tng hp nht nh, n tr nn cn thit c c axit oxalic t cc ngun OTC.Trong khi cch d nht lm iu ny l khng c nghi ng mua n tinh khit nh thuc ty g, khai thc trn dp l cn thit, hoc t bn giy tiu ha v hn hp kim / axit t qu trnh oxy ha mt tinh bt, hoc mt sn phm lm sch c cha grit tt, x phng , v rc thi khc. M t y l mt phng php sp xp hp l m axit oxalic tinh khit c th d dng ch bin t bt k ngun, vi ti thiu l thit b v khng c dung mi hu c.

Tuyn ng ny c li th ca s thay i rt ln trong kh nng ha tan gia natri v canxi mui axit oxalic phc hi n t rc thi khc, n c th c trn ln vi. Cc nguyn liu c cha axit l ln u tin basified vi soda hoc dung dch kim to ra natri oxalat, khuy u v gii quyt, sau chit thng qua mt b lc c ph loi b cc ht cn li. Mt gii php mnh m ca canxi clorua sau c b sung, kt ta canxi oxalate, v ni b i. Sau kt ta c ra sch v ha tan vi acid sulfuric long, v calcium sulfate kt ta b loi b. Cui cng, hn hp ny c un si cho n khi cc tinh th bt u hnh thnh, v sau p lnh, v ri qung m ca cc tinh th axit oxalic tinh khit s ri ra v c th c thu thp. Thc hi n / thc tp - Bt u vi mt th ca Zud Gi s zud l tt c cc axit oxalic (m chc l khng), v rng bn c mt 175 g c th, s c 1,3 mol axit oxalic trong (n l mt dihydrate), do , thm 3 nt rui (252 g) baking soda hoc dung dch kim (120 g), hoc 1,5 mol (429 g) ra soda vo zud trong 1 lt nc. Lc k trong mt ci bnh, v vo mt chai. Ti s dng mt ca hng ng la ly chai, hot ng ging nh ma thut. Hy ngi cho mt gi hoc lu hn, lc ny tt c cc ht nh mi mn s t nhiu gii quyt. Sau , rt nh nhng, gn ly ra khi cht lng thng qua mt b lc c ph vo mt ly (hay ni c ph). y chai vi 1 lt nc v swirl n xung quanh mt s chi tit, v khi n lng xung, gn ly phn nc mi thng qua cc b lc vo bnh cng c. 160 g khan canxi clorua (m-thot khi) c trn vi nc va ha tan n, v sau vo bnh. Cc chai vo

mt thng cha cht thi v ra sch.Ly c sau lc u v vo chai, v hn hp gii quyt. Sau , nc c chit ra, v 1 lt nc ngt vo chai, khuy ng, cho php nh c, v b i. Chu k git ny c lp i lp li cho n khi nc c v tt p v r rng sau khi cc ht gii quyt. Sau , thay v loi b nc, 160 ml axit sulfuric c thm vo mt cch cn thn. Hn hp ny c chit thng qua b lc vo mt ni trng, v un si cho n khi cc tinh th bt u hnh thnh. Sau n c lm lnh n nhit phng v qua mt b lc c ph thu thp cc tinh th. Cc tinh th c ra sch vi nc lnh v t chng vo kh, v ni t trong t to thnh mt ti th hai, c ch bin theo cch tng t nh ln u tin. Nc sau c th b loi b, v tt c cc thit b lm sch. Sau khi axit oxalic kh, n c th c cn nhc, v s lng c s v axit c s dng khai thc iu chnh cht thi ti thiu. - Bt u t hng lot phn ng tng hp kim Tt c cc axit oxalic l c trong mt hnh thc mui, v vy bc basification l khng cn thit. Khi lng phn ng tng hp c th cha mui format c gi tr, l gi tr mt th phc hi cng c, v vy khng nn c x l ngay lp tc. Nu khng, s dng cc th tc trn. - Bt u t kh lng axit nitric qu trnh oxy ha Khi basifying, hy chc chn a vo ti khon s lng axit c b sung vo khi lng, v iu chnh kim thm vo cho ph hp. Hy cn thn. L thuyt (COOH) 2 + 2 NaHCO3 Na 2 (COO) 2 + 2 CO 2 + 2 H 2 O (ha tan) Na 2 (COO) 2 + CaCl 2 Ca (COO) 2 + 2 NaCl (khng tan) Ca (COO) 2 + 2 H 2 SO 4 Ca (HSO 4) 2 + (COOH) 2 (ha tan) lun phin, Ca (COO) 2 + H 2 SO 4 CaSO 4 + (COOH) 2 Canxi clorua l hp cht canxi l tng s dng cho mc ch ny, nh hu ht cc mui canxi khc hoc l khng ha tan, hoc ch hi tan, nh vy l rt kh tch bit vi axit oxalic mong mun ta nu thm vo trong bt k d tha. CaCl 2 l rt d tan, v vy d tha c th c thm vo m khng s nhim ca sn phm cui cng.