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tcvn 6017 : 1995 ISO 9597 89(E)

Xi mng Ph|ng php th - Xc nh thi gian ng kt v n nh

Cements - Test methods - Determination of setting time and soundness
1. Phm vi p dng Tiu chun ny quy nh ph|ng php xc nh thi gian ng kt v n nh th tch ca xi mng. 2. Tiu chun trch dn TCVN 6016: 1995, Xi mng - Ph|ng php th - Xc nh bn. 3. Nguyn tc Thi gian ng kt |c xc nh bng cch quan st ln su ca mt kim loi h xi mng c do tiu chun cho n khi n t |c gi tr quy nh. n nh th tch, theo ph|ng php Le Chatelier, |c xc nh bi s n th tch ca h xi mng c do chun, thng qua dch chuyn t|ng i ca hai cng khun. H xi mng c do tiu chun l khi t kh nng cn thit cn li s ln ca mt kim chun. L|ng n|c cn thit cho mt loi h nh| vy |c xc nh bng ba ln st kim vi h c hm l|ng n|c khc nhau. 4. Phng th nghim v thit b 4.1. Phng th nghim

Phng th nghim ni ch to v th mu gi nhit 270C H 20C v m t|ng i khng thp hn 50%. 4.2. Thit b 4.2.1. Cn, c chnh xc n 1g; 4.2.2. ng ong c vch chia hoc buret, c kh nng o th tch chnh xc n 1% 4.2.3. My trn, ph hp vi cc yu cu ca ISO 679. 4.3. Vt liu 4.3.1. N|c ct hoc n|c kh ion |c s dng ch to, bo qun hoc luc mu
Ch thch: - C th dng loi n|c khc nh|ng phi m bo kt qu nh| nhau.

4.3.2.

Xi mng, n|c v thit b dng ch to v th mu |c gi nhit 270C H 20C v phi ghi li nhit trong bo co th nghim. 5. Th do chun 5.1. Dng c Dng dng c Vicat nh| hnh 1a) v 1b) vi kim to nh| hnh 1c). Kim to |c lm bng kim loi khng r v c dng mt tr thng, c chiu di hu ch l 50mm H 1mm v |ng knh l 10mm H 0,05mm. Khi l|ng ton phn ca phn chuyn ng l 300g H lg. Chuyn ng ca n phi tht thng ng v khng chu ma st ng k, v trc ca chng phi trng vi trc kim to.
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Vnh khu Vicat (xem hnh 1a) cha h phi |c lm bng cao su rn. Vnh khu c dng hnh nn ct, su 40mm H 0,2mm, |ng knh trong pha trn l 70mm H 5mm v y l 80mm H5mm. Vnh khu phi cng v phi c mt tm e phng bng thu tinh c kch th|c ln hn vnh khu v dy t nht 2,5mm.
Ch thch: Vnh khu bng kim loi hoc cht do hay vnh khu dng hnh tr u c th s dng min l phi m bo chiu su yu cu v kt qu thu |c phi ging nh| khi th bng vnh khu cao su cng hnh nn ct.

5.2. Tin hnh th 5.2.1. Trn h xi mng Cn 500g xi mng , chnh xc n 1g. Cn mt l|ng n|c l 125g ri vo trong ci trn (4.2.3) hoc dng ng ong c vch chia hay buret (4.2.2) o l|ng n|c vo ci trn. xi mng vo n|c mt cch cn thn trnh tht thot n|c hoc xi mng. Thi gian khng t hn 5 giy v khng nhiu hn l0giy. Ly thi im kt thc xi mng l thi im " khng ", t tnh thi gian lm tip theo. Khi ng, nguy my trn v cho chy vi tc thp trong 90 giy. Sau 90 giy, dng my trn khong 15 giy vt gn h xung quanh ci vo vng trn ca my bng mt dng c vt thch hp. Khi ng li my v cho chy tc thp thm 90 giy na. Tng thi gian chy my trn l 3 pht.
Ch thch: Mi ph|ng php trn khc, d bng tay hay my u c th |c s dng min l cho cng kt qu th nh| vi ph|ng php quy nh theo tiu chun ny.

vo vnh khu ngay h vo khu |c t trn tm phng bng thu tinh c bi mt lp du. y hn khu m khng nn hay rung qu mnh. Dng dng c c cnh thng gt h tha theo kiu chuyn ng ca nh nhng, sao cho h y ngang khu v b mt phi phng trn. 5.2.3. Th ln Tr|c khi th gn kim to (hnh 1) vo dng c Vicat, h kim to cho chm tm v chnh kim ch v s khng" trn thang chia vch. Nhc kim to ln v tr chun b vn hnh. Ngay sau khi gt phng mt h, chuyn khu v tm sang dng c Vicat ti v tr ng tm d|i kim to. H kim to t t cho n khi n tip xc vi mt h. Gi v tr ny t 1 giy n 2 giy trnh tc ban u hoc gia tc ca b phn chuyn ng. Sau th nhanh b phn chuyn ng kim to ln thng ng vo trung tm h. Thi im th kim to t thi im s "khng" l 4 pht. c s trn thang vch khi kim to ngng ln, hoc c ti thi im 30 giy sau khi th kim to, t theo vic no xy ra sm hn. Ghi li s c, tr s biu th khong cch gia u kim to vi tm . ng thi ghi li l|ng n|c ca h tnh theo phn trm khi l|ng xi mng. Lau sch kim to ngay sau mi ln th ln. Lp li php th vi h c khi l|ng n|c khc nhau cho ti khi t |c mt khong cch gia kim to vi tm l 6mm H lmm. Ghi li hm l|ng n|c ca h ny, ly chnh xc n 0,5% v coi l l|ng n|c cho do chun. 6. Th thi gian ng kt 6.1. Dng c
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5.2.2.

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6.1.1.

tcvn 6017 : 1995

Dng phng hoc mt bung kch th|c v gi nhit 270C + 10C v m t|ng i khng nh hn 90%. 6.1.2. Dng dng c Vicat xc nh thi gian bt u v kt thc ng kt. Tho kim to v lp vo kim nh (hnh 1d), kim ny lm bng thp v c hnh tr thng so vi chiu di hu ch 50mm H 1mm v |ng knh l,13mmH0,05mm. Tng khi l|ng ca b phn chuyn ng l 300g H 1g. 6.2. Xc nh thi gian bt u ng kt Tr|c khi th cn hiu chnh dng c Vicat |c gn kim nh, bng cch h thp kim nh cho chm tm v chnh kim ch v s "khng" trn thang vch. Nng kim ln ti v tr sn sng vn hnh. h c do chun vo y khu Vicat v gt bng mt khu theo iu 5.2.1. v 5.2.2. t khu c h v tm vo phng d|ng h m (xem 6.1), sau thi gian thch hp chuyn khu sang dng c Vicat, v tr d|i kim. H kim t t cho ti khi chm vo h. Gi nguyn v tr ny trong vng 1 giy n 2 giy trnh vn tc ban u hoc gia tc c|ng bc ca b phn chuyn ng. Sau th nhanh b phn chuyn ng v n ln su vo trong h. c thang s khi kim khng cn xuyn na, hoc c vo lc sau 30 giy th kim, ty theo cch no xy ra sm hn. Ghi li cc tr s trn thang s, tr s ny biu th khong cch gia u kim v tm . ng thi ghi li thi gian tnh t im khng. Lp li php th trn cng mt mu ti nhng v tr cch nhau thch hp, ngha l khng nh hn 10mm k t ra khu hoc t ln tr|c n ln sau. Th nghim |c lp li sau nhng khong thi gian thch hp, th d cch nhau l0 pht. Gia cc ln th kim gi mu trong phng m. Lau sch kim Vicat ngay sau mi ln th kim. Ghi li thi gian o t im "khng" khi khong cch gia kim v t 4mm H lmm, v ly lm thi gian bt u ng kt, ly chnh xc n 5 pht. chnh xc c th |c m bo bng cch gim khong thi gian gia cc ln th kim gn ti im cui v quan st cc kt qu lin tip thy khng bin ng qu nhiu. 6.3. Xc nh thi gian kt thc ng kt Lt p khu s dng iu 6.2 ln trn tm ca n sao cho vic th kt thc ng kt |c tin hnh ngay trn mt ca mu m lc u tip xc tm . Lp kim c gn sn vng nh (xem hnh 1e) d quan st su nh khi kim cm xung. p dng qu trnh m t nh| trong iu 6.2. Khong thi gian gia cc ln th kim c th |c tng ln, th d l 30 pht. Ghi li thi gian o, chnh xc n 15 pht, t im khng vo lc kim ch ln 0,5 mm vo mu v coi l thi gian kt thc ng kt ca xi mng. chnh l thi gian m vng gn trn kim, ln u tin khng cn ghi du trn mu. Thi gian ny c th xc nh mt cch chnh xc bng cch gim thi gian gia cc ln th gn n im cui v quan st thy cc kt qu th k tip khng bin ng qu nhiu.
Ch thch: Cc my o thi gian ng kt t ng c bn sn u c th |c s dng min l my cho cng kt qu nh| khi dng dng c v quy trnh quy nh trong tiu chun ny. Nu dng my t ng, khng cn thit phi lt p mu.

7. Th n nh th tch 7.1. Dng c

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7.1.1.

tcvn 6017 : 1995

Dn dng c Le Chatelier (xem hnh 2) c khun bng ng n hi c cng o. Khun phi c n hi sao cho d|i tc ng ca mt khi l|ng nng 300g (nh| hnh 2c) th khong cch gia hai u cng khun tng ln 17,5mm H 2,5mm m khng bin dng c nh. Mi khun u c mt cp phng bng knh v a y. Mi tm a phi ln hn khun. a y phi nng t nht l 75g; vi a mng c th t thm vt nh ln trn p ng yu cu ny. 7.1.2. Dng thng n|c c dng c un nng, v c kh nng cha ngp |c cc mu Le Chatelier v nng |c nhit ca n|c t 270C H 20C n si trong thi gian 30 pht H 5 pht. 7.1.3. Dng mt bung m kch th|c, nhit 270C +10C v m t|ng i khng nh hn 98%. 7.2. Tin hnh th Tin hnh th trn hai mu ca cng mt m h xi mng. Ch to h xi mng c do chun. t mt khun Le Chatelier (7.1.1) bi mt lp du mng ln tm cng qut lp du v y ngay m khng lc hoc rung, ch dng tay v mt dng c cnh thng gt bng mt va nu cn. Trong lc y khun trnh lm khun b m tnh c, chng hn do b n nh ca ngn tay, do buc hoc khi cn dng mt dy cao su thch hp. y khun li bng a qut du, nu cn th thm khi l|ng iu chnh, ngay sau t ton b dng c vo bung m. Gi trong 24 gi H 0,5 gi nhit 270c H 10C vi m t|ng i khng nh hn 98%.
Ch thch: Khun mu nm gia cc tm knh, cng c th |c t ngp trong n|c trong 24 gi H 5 gi nhit 270C H 10C nu nh| cho kt qu th nh| nhau.

Vo cui thi gian 24 gi H 0,5 gi, o khong cch A gia cc im chp ca cng khun, chnh xc n 0,5mm. Gi khun ngp trong n|c, un n|c dn dn n si, sut trong 30 pht H 5 pht v duy tr b n|c nhit si trong 3 gi H 5 pht.
Ch thch: Nu n sau mt thi gian si ngn hn vn ging nh| sau 3 gi si th thi gian ngn hn cng s dng |c.

Vo thi im kt thc vic un si, o khong cch B gia hai im chp ca cng khun, chnh xc n 0,5mm. khun ngui n 270C H 20C. o khong cch C gia cc u chp ca cng khun, chnh xc n 0,5mm. mi mu, ghi li cc gi tr o A v C v tnh ton hiu C - A. Tnh gi tr trung bnh ca hai hiu C - A, chnh xc n 0,5mm. Thuyt minh Mc ch chnh ca th nghim n nh th tch l nh gi kh nng n th tch mun c th xy ra do hin t|ng hydrat ho ca canxi oxit v/hoc magie oxit t do. V mc ch ny phi bo co hiu trung bnh C - A.
Ch thch: Nu cc iu kin th nghim dn n sai lch khng ng k gia cc s o B v C th hiu s B C nn bo co v iu gim bt |c thi gian cn thit khi th.

7.3.

7.4.

Th nghim li
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7.5.

Nu xi mng mi khng p ng yu cu th n nh th c th th li sau khi ct gi. lm |c iu , ri xi mng thnh mt lp dy 7cm v bo qun 7 ngy trong mi tr|ng nhit 270C H 20C v m t|ng i khng nh hn 50%. Sau th li xi mng theo ng qui trnh th iu 7.2. n nh th tch lnh. Nu mun cng c th th n nh th tch lnh. Trong tr|ng hp ny, chun b mu v t vo trong n|c 270C H 20C theo iu 7.2. Sau o ngay khong cch A gia u chp ca cng khun, chnh xc n 0,5mm. Sau 7 ngy H 2 gi o khong cch D vi chnh xc trn. Nu cn xc nh thi im khi hin t|ng n th tch lnh xy ra th c th chn khong thi gian th nghim ngn hn. n nh th tch lnh |c tnh bng hiu D - A.

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