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BHG Doc No.

Peschl-003 Rev A
Bulk Handling Global Pty Ltd Solutions for storage and flow of solids . . . . Its all about flow.
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Bulk Handling Global Pty Ltd
Bulk solids and powder flow properties testing, silo and hopper design, discharge and conveying technology


Principles of shear testing


Paper by:-
Dr. Ivan Peschl IPT. Seminar MIT Boston 14
th
May 1999


























Peschl Bulk solids and powders flow property testing





BHG Doc No. Peschl-003 Rev A
Bulk Handling Global Pty Ltd Solutions for storage and flow of solids . . . . Its all about flow.
Email: info@bhglobal.com.au Website: www.bulksolidsflow.com
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Principals of shear testing for bulk solids.

The shear testing technique should measure the resistance of a soil/powder against plastic deformation
in relation to the pressure working in the shear plain.

An idealized shear test is shown in fig. 1. - An infinite plain representing the test sample. The upper
portion moves relative to the lower portion, creating a uniform shear plane in between the moving
spaces. Ideally, the shear testing device should reach this idealized situation as soon as possible. For
practical consideration, the shear tester should have limited dimensions.

The basis of shear testing of products has derived from soil mechanics. Of original design by
Casagrande, the shear testing device was rectangular because with limited knowledge at that time, soil
samples were easily prepared as rectangular as compared to other forms. The rectangular cell was
composed from a cell base, and a top-loading cover. The intention was a linear movement of the
loading cover against the cell base, and the soil-sample shears in-between the cell base and the
loading cover. For soil samples, this method of shear test by Casagrande delivered acceptable results.

As knowledge and experience was gained, the Casagrande tester was introduced to bulk solids
powders. However, unlike soil samples which have been consolidated for thousands of years, it was
found that the samples of industrial powders required to be consolidated in the shear cell, and the
rectangular format was found to be less than ideal. Industrial powders were found to be more or less
loose powders, as compared to soils.

Experimentation and process requirements lead to a device where powders can be more efficiently
filled and consolidated. Early pioneer J enike altered the square cell design of Casagrande, having a cell
base cell ring and a loading cover. Operation of the shear cell remained a linear movement. In this
revised design, the consolidation process occurred during the shearing process, until a stable shear
stress was established. By experimentation, some powders too small in particle size were unable to
reach a stable shear stress, making this design limited in effectiveness.

This lead to a need for shear tester design which would allow a longer shear strain until the shear
stresses reaches a stable value.

In order to reach a longer shear strain, Walker developed the ring shear tester. The Walker ring shear
tester was based on an inner and outer annulus, with the loading lid located in between the inner and
outer ring. The inner ring is introduced because the idea that the shear stress is dependent of the
radius. Approximate uniform shear stresses have been supposed in the ring formed sample. The
assumption of a linear function of the stresses versus the radius was more realistic compared to
previous shear tester designs. The linear function of stress would only be valid during the elastic
deformation of the sample.

However, for true testing of shear requirements, the function of plastic deformation is of more important
value rather than the values of elastic deformation.

In the Walker design shear cell, the shear plane was localized directly under the top cover, where the
shear stress is a combination of wall friction of top cover and internal friction of the powder. As the
shear plane occurs in this localized region, it is established that it is a limitation of the ring shear cell
tester. The Walker (annulus) shear cell design, does allow the measurement of the plastic deformation,
however, the measured shear stress during deformation, is equal at any radius of the sample.
Therefore, the introduction of the inner ring of the shear cell is not necessary.



Continued.


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Principals of shear testing for bulk solids. Continued.

Extensive development has lead to the Peschl full area rotational split ring shear cell - without an inner
ring. The Peschl rotational shear cell combines the advantages of J enike shear cell and Walker ring
shear cell. In the rotational shear cell, the shear plane is located in the middle of the sample tested
well away from the surfaces of the upper and lower cells, with the ability to apply unlimited shear strain
due to rotational movement. This shear tester approaches the most the idealized infinite powder sample
as shown in fig. 1.


Jenike shear tester.

The J enike shear tester consists from a cell bottom, cell ring and top loading cover as shown in fig. 2.
Shearing is introduced by translation of the top loading cover and cell ring against the cell base. The
shear force is externally introduced (rather than within the sample) by movement of the cell ring. As a
result of the linear ring movement, the internal pressure is higher on the trailing side of the upper cell,
and lower on the leading side. This leads to a consequential inclination of the top lid.

The shear force is partially introduced by movement of the cell ring. This effect has as result a non-
uniform development of the consolidation pressure and the shear stress over the cross section of the
shear cell.

Because of translation movement, the shear strain is limited to few millimeters, whereby the ring moves
over the cell base. For some elastic powders, the allowed shear strain is already reached before the
plastic shear stress is established. As the J enike shear cell relies on a linear operation of the cells to
achieve shear, the function of pressure applied to the sample area is varying due to uneven
displacement of sample particles during the linear movement. These issues place a limitation on the
intension to measure the true shear stress as function of pressure.


Ring shear tester and similar designs.

Following the Walker development of the ring shear tester, various reputable institutes have designed
shear testers with minor differences in size or design. These variations have some common
characteristics in design where the cell base and the loading top cover is ring formed. The top cover,
which is provided with vertical wings, presses on the surface of the powder in the ring formed space as
shown in fig. 3.

A number of influences from these designs are described as follows:

a. Variation of consolidation pressure in the tangential direction is introduced by wings on
the top cover.

b. Variation of pressure in the radial direction is introduced trough the ring-orifices on the
outer and inner radius of the cell. The powder tends to leak through the ring formed
orifice between the cell wall and the loading cover. Consequently, pressure drops to
zero at the place of orifices because of loss of material during the shearing.

c. The shear plane is directly under the loading ring. Because of this, the shear plane
consists of areas where wall friction is measured and areas where internal friction is
measured. Consequently, a mixture between wall friction and internal friction will be
measured depending on the geometry of construction and the powder properties.

Continued.


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Ring shear tester and similar designs. Continued.

d. Difference of shear stress occurs at the place of the wings - passive on the pressure
side and active on opposite side. Consequently, the sample tends to compress on the
side of high passive pressure and expand on the side of the low active pressure also
we receive a variation of compaction in the shear cell and as result a non-uniform shear
stress.

e. Difficulties during the course of measurement of wall friction. Problems: The wall
sample has to be machined to a ring form and has to be fixed to the bottom. The
measurement of friction is accompanied with measurement of forces along the
sidewalls of the cell. The result is a measurement of to high wall friction.


f. Measurement of Time Consolidation is difficult with alternative ring shear testers.
Ideally, time consolidation should be measured without the removal of shear cell
covers. The first movement of upper cells should be during measurement of shear
stress after time consolidation. This is not ensured because of following reasons:


A guided loading cover originally designed by Walker, required the lifting of the
load cover during the ongoing measuring process. This also increases the duration
of testing time.

Using a free load-cover, the positioning and concentricity of cover and cell is
difficult to establish, and requires re-setting to allow clearance and freedom of the
cell torque arm. By this process the shear plain is partially disturbed and the
measured time consolidation shear stress is generally lower.

g. Ultimately, the design of a ring shear cell tester should include features that allow the
shear stress as a linear function of the radius of the shear cell. Experimentation shows
that these values are only achieved after elastic deformation limits are reached, and
plastic deformation is established to the further shear process. By this plastic
deformation, the plastic shear stress is constant across the entire volume of the shear
cell from the outer radius of the shear cell right to the middle of the shear cell. That
means that the inner ring of a ring shear cell is not necessary.


Peschl rotational split level shear cell.

Peschl has developed a rotational shear cell whereby the shear plain occurs in the middle of the
sample, exactly between the end of the cell base and the beginning of the rotational ring. The location
of the shear plane is located in this region, due to the design of the surfaces of the upper and lower cell
surfaces which entraps the particles and shear occurs directly within the body of the sample. The
increased holding friction prevents the sample from shearing on the surfaces of the upper and lower
cells. The shear plane occurs in the split level between bottom and the loading cover.

Consequently, the Peschl shear tester, shown in fig. 4, is a true full area shear tester which directly
measures the internal friction of powder against powder, without disturbing effects. The Peschl split cell
shear tester allows sufficient shear strain to reach the stable value of the shear stress by plastic
deformation. Thus peak initial shear stress is accurately measured, and used in determining the Mohrs
values.

Continued.


BHG Doc No. Peschl-003 Rev A
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Peschl rotational split level shear cell. Continued.

In fig.5 is the development of the shear stress and density versus shear strain as function of the radius
for significant stages shown.

a. In begin of the shearing, fig. a, by strain between 0 and K1, is elastic deformation in
which period the shear stress. T is in linear relation to the radius R.

b. The next stage, fig b shows that by further shearing, the shear stress is lower in value
at the minor radius, to the maximum T1.

c. By further shearing, the maximum shear stress T1, is achieved in the middle region of
the shear cell at the strain K2. With additional shearing, the shear stress stays constant
over the entire surface of the shear cell.

d. By discontinuing shearing, and unload the shear stress by allowing the shear cell to
move free, the shear cell rotates backwards as the shear stresses at strain K3 are not
in equilibrium. The shear cell rotates backwards until the shear stresses across the
radius are in equilibrium. This deformation can only happen by elastic deformation.
Consequently, the shear stresses in the middle of the shear cell are not altered, and
remain at T1values. By shearing under decreased consolidation pressure, the shear
stress reduce in value according to the yield locus and reach a value of T2.

e. During the next stages of shearing K4-K5, the sample deforms elastically, whereby two
processes are simultaneously changing the shear stress and the density. By stopping
the shearing at K3, the sample compacts as the particles find the line of least
resistance in the inter-particular spaces, which leads to higher consolidated density.
When we start to shear again, we shear at the higher density and consequently with
higher shear stress T2. In the graphic for development of shear stress versus the strain
the value T2, is represented as a peek at strain K5

f. By continuing the shearing, the density decreases because of the shearing action. At
is reduced density, lower shear stress T3 the plastic shear stress K6 corresponds
to the consolidation pressure.


Conclusion.

Shearing is always a process of altering density by varying consolidation pressure, as well as altering
shear from static to dynamic conditions. The maximized/peek shear stress development can also be
attained by constant consolidation pressure due to plastic and non plastic deformation, as well as
fluctuations in density created by dynamic and static movement of particles.

The maximized/peek shear stress is attributed to, and attained purely by the normal shear process. The
recording of these values is easily attained, and of importance to measuring true material properties.
Hence, techniques such as altering sample preparation, varying consolidation load midstream of a test,
or altering the movement path of cells have a major impact on results. The Peschl rotational shear
tester avoids all these pitfalls currently experienced by previous design shear testing equipment.





Continued.


BHG Doc No. Peschl-003 Rev A
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Fig 1. Idealized shear test

a. Infinite shear plain.
b. Constant volume - Mohr diagram for plastic deformation. Shear stress on the top of the
Mohr circle.
c. Compacting volume Shear stress right from the top of the Mohr circle.
d. Expanding sample Shear stress left of the top of the Mohr circle
e. Idealized shear test Angle of expansion vector =AL is equal to the internal angle of
friction =F.









Continued.


BHG Doc No. Peschl-003 Rev A
Bulk Handling Global Pty Ltd Solutions for storage and flow of solids . . . . Its all about flow.
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Fig 2. J enike shear tester



S Vertical pressure in the shear plane
N Shear force
S1P Passive High pressure on the ring wall
S2P Active Low pressure on the ring wall
T Shear stress
TPP High shear stress on the passive pressure side
TPA Low shear stress on the active pressure side















Continued.


BHG Doc No. Peschl-003 Rev A
Bulk Handling Global Pty Ltd Solutions for storage and flow of solids . . . . Its all about flow.
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Fig 3. Ring shear tester



Fig 3A General view of the ring shear tester
Sn consolidation load
T shear force - moment




Fig 3B View on the top cover with wings and cell base ring shear tester



Continued.

BHG Doc No. Peschl-003 Rev A
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Fig 3B. Forces and pressures over the cross section of a ring shear tester


A. Vertical pressure distribution because of wings on the top loading lid
B. Horizontal active and passive pressures on the wings
C. Non uniform distribution of the shear stress because of non uniform vertical consolidation
pressure, as well as non uniform horizontal stress as a result of the wings













Continued.


BHG Doc No. Peschl-003 Rev A
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Fig 4. Peschl shear tester consists of a base cell ring and top consolidation cover
S Consolidation pressure
S1 - Major main stress
S2 Minor main stress
T Shear stress

A. Uniform distribution of vertical consolidation pressure over the entire cross section of the
shear cell
B. Shear plane in between the cell base and cell ring
C. Uniform distribution of the shear stress over the entire cross section of the shear cell




Continued.
BHG Doc No. Peschl-003 Rev A
Bulk Handling Global Pty Ltd Solutions for storage and flow of solids . . . . Its all about flow.
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Fig 4A Peschl shear tester

A. Raw materials shear cell
B. Standard shear cell
C. Pharmaceutical shear cell





A B C


















Continued.


BHG Doc No. Peschl-003 Rev A
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Fig 5. Development of shear stress during a shear stress




Fig 6 Development of shear stress during a shear test measured with a scientific shear cell


1. Few starting tests by increasing the shear stress
2. Development of the shear stress by continuation of the shear process
3. Backwards of the strain as a result of establishing equilibrium of the shear
stresses over the cross section of the shear cell

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