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Assurance Guide
SILICONE STRUCTURAL
GLAZING MANUAL
2001 Dow Corning Corporation
Guidelines for European Technical Approval (EOTA ) for Structural Glazing (ETAG 002 part 1
Sept. 1998) (Europe)
CEN Draft European Standards CEN/TC129/WG16 - PrEN 13022 (parts 1 - 4) October 1997 (Europe)
Bundesanzeiger 92a - Bekanntmachung der Leitlinie fr die europische technische Zulassung fr
geklebte Glaskonstruktionen, Vom 15. Dezember 1998, ISSN 0720-6100 (Germany)
Ift Rosenheim Leitfaden fur den Ubereinstimmngsnachwies fur Structural Glazing (Germany)
Vitrages extrieurs colls faisant lobjet dun avis technique - Conditions gnrales de conception /
fabrication et mise en uvre. (Cahiers du CSTB 3130, Livraison 399 - mai 1999) (France)
BSI: BS 6262 Code of practice for Glazing for Buildings Part 6: Special Applications (U.K.)
STS 56 - Vitrage Extrieur Coll and Cahiers de lINV (Belgium)
Standard Guides for Structural Sealant Glazing. ASTM C1401-98 (United States)
Structural Silicone Sealant for Building. GB 16776 - 1997 (China)
Users are advised to check with their local Building Authority to verify the Standards and requirements
for Structural Glazing prior to commencement of the work. Please consult your local DOW CORNING
Construction Office for assistance and further information.
Setting Procedure . . . . . . . . . . . . . . . . . . . . . . 11
Project Review . . . . . . . . . . . . . . . . . . . . . 3
Product Recommendations . . . . . . . . . . . . . . . 3
Drawing Review . . . . . . . . . . . . . . . . . . . . . . . . 3
Adhesion Testing . . . . . . . . . . . . . . . . . . . . . . . 4
Compatibility Testing . . . . . . . . . . . . . . . . . . . . 4
Non-Stain Testing . . . . . . . . . . . . . . . . . . . . . . 4
Other Test Requirements . . . . . . . . . . . . . . . . 5
Structural Adhesion Limited Warranty . . . . . . 5
Product Quality . . . . . . . . . . . . . . . . . . . . 6
One-Part Structural Silicone . . . . . . . . . . . . . . 6
Shelf Life and Storage Conditions . . . . . . . 6
Skin-Over Time/Elastomeric Test . . . . . . . . 6
Multi-Component Structural Silicone . . . . . . . 6
Shelf Life and Storage Conditions . . . . . . . 6
Pump Procedures . . . . . . . . . . . . . . . . . . . . 6
Quality Control Testing . . . . . . . . . . . . . . . . 7
Glass or Butterfly Test . . . . . . . . . . . . . . . . . 7
Snap Time . . . . . . . . . . . . . . . . . . . . . . . . . . 8
Mixing Ratio Measurement . . . . . . . . . . . . 8
Adhesion Testing . . . . . . . . . . . . . . . . . . 14
Peel Adhesion testing . . . . . . . . . . . . . . . . . . . 14
H-Piece Adhesion testing . . . . . . . . . . . . . . . . 15
Quality Control Guidelines . . . . . . . . . . . . . . 16
Quality Control Log Sheet . . . . . . . . . . . . . . . 16
Project Timetable . . . . . . . . . . . . . . . . . . . . . . 18
3.
4.
Sealant Adhesion
1.
Product Quality
5.
Documentation
Project Review
Dow Corning
Dow Corning
797 Weatherproofing
Sealant
2. Dow Corning 3793 Insulating Glass Sealant a one-part silicone sealant used in the factory
as a secondary sealant in insulated glass unit
production.
2. Dow Corning 3556 Cleaner for SSG recommended specifically for cleaning of
anodized aluminium surfaces only.
Product Recommendations
After reviewing project drawings and
specifications, and having performed the
necessary laboratory testing, DOW CORNING
will assist in the selection of the correct Dow
Corning silicone sealants.
Adhesion Testing
Structural Bite (m) =
Weight of glass (kg) 9.81 ms-2
bite
e
Compatibility Testing
Incompatible glazing accessories (gaskets, spacers,
backer materials, setting blocks, etc.), can lead to
sealant discoloration and/or loss of adhesion to
the substrate. To ensure compatibility, DOW
CORNING tests the compatibility of project
specific accessory materials with its silicone
sealants. Results of the compatibility test will be
forwarded in writing. Testing takes approximately
four weeks from receipt of samples.
Non-Stain Testing
Pump Procedures
insufficient mixing
properly mixed
1. Apply sealant to
creased white paper
2. Press together
3. Well-mixed sealant
Snap Time
Non-Porous Substrates
Masking
10
Appearance
Clear liquid
18 months
Storage Temperature
Discard Indication
25 C
Product turns
milky white
Setting Procedure
11
Site Glazing
12
13
Adhesion Tests
Peel Adhesion Testing
This is a simple screening test that can be done
on a flat test surface, as shown in the diagram to
the right.
25 mm
Bond breaker
25 mm
NOT
ALLOWED
14
2.
15
date:
morning
afternoon
packaging change
temperature (C)
metal (2)
type:
lot number
x
x
x
x
x
x
x
x
(x)
(x)
(x)
(x)
glass
(x)
type:
(x)
x
x
x
x
(x)
(x)
(x)
(x)
adhesion testing on
H-pieces (5) (6)
sample n1: after ... days
type of rupture
tensile stress (MPa)
x
x
x
x
x
x
(x)
(x)
(x)
(x)
(x)
(x)
(x)
(x)
(x)
(x)
(x)
(x)
(1A)
(2)
For insulating units there is no metal support but a second glass plate
(3)
The purpose of these tests are to check the homogeneity of the mixture. See test descriptions text of this guidebook.
(4)
All 2-component mixing equipment comes equipped with 2 sampling tubes where small quantities of base and
catalyst can be taken for verification of the correct mixing ratio..
(5)
The H-pieces are test-pieces of silicone (12*12*50 mm) between 2 supports. See reference drawing in text of
the guidebook.
The shape of the test-pieces can be provided by wooden blocks which have been treated with a soap solution to avoid
adhesion of the silicone or by means of Norton tape from which the adhesive tape has not been removed. Be sure that in the
case of one-component sealants, the spacers are not air- and vapour tight otherwise they will prevent the curing of the
silicone.
For every half day of production, 3 test-pieces have to be made. The test pieces have to be stored in the same conditions as
the produced units. After 24 hours e.g. the first test-piece can be tested according to the procedure described below.
For testing the test pieces to rupture a sophisticated machine is not required. The roman scale as represented below will
allow the silicone applicator to test sealant adhesion and mechanical properties with a low cost equipment.
The strength applied to the silicone joint is equal to the weight W on the roman scale plate times the ratio b/a.
Before the produced units can be transported to the site or in the case of structural bonding on site with DC 895 the time to
wait before the temporary mechanical fixings can be removed, the H-piece test sample needs to have a cohesive (this means
rupture in the mass of silicone and not at the adhesion interface) tensile stress at rupture of minimum
0.7 MPa. This corresponds to a strength of 12 * 50 * 0.7 = 420 N to be applied to the test piece. This strength corresponds
to a load of 42 kg.
If the roman scale is designed for having a ratio b/a of 10, a weight W of 4.2 kg is necessary on the scale to generate the
required stress in the silicone. This strength will be submitted to the joint for max. 10 seconds and no adhesive or cohesive
rupture may be observed.
If this is the case, continue to rupture by adding half a kilo at a time on the scale. The strength must be recorded in the
logbook and also the type of rupture. The rupture needs to be 100 % cohesive in all the cases.
If these two conditions are not fulfilled, the units have not cured sufficiently to transport them to the site. Wait e.g. anoth er
24 hours and test the second test piece in the same way ....etc.. Be ware that the time necessary to cure will strongly depend
on the temperature and for one-component silicones also on the relative humidity of the air.
(6) In case of impossibility to make H-pieces and to have a roman scale and there are no limits to the delivery time and/or
storage room, one can replace the 3 H-pieces per half a day of production and/or packaging change by 3 peel tests per
different substrate. After cleaning the substrate (and priming if necessary), a bead of silicone of approximately 10 mm
wide and 3 mm thick is applied. Afterwards a metal wire is pressed in the bead after which a second bead of silicone is
applied. After curing an incision is made with a cutter at the adhesion surface right in between the silicone and the metal,
of about 10 mm deep. By tearing with hand the type of tear should be checked. If the tear continues at the adhesion
surface an adhesive type of rupture is obtained which is not good. If the tear continues in the bulk of the silicone a cohesive
failure is obtained. At all times a 100% cohesive failure should be obtained!
This test does not allow the determination of the speed of curing because of the lack of recording a force at rupture.
Therefore when glueing in the factory one needs to keep the sealed units 7 days in the factory for a two component and 3
weeks for the one component if only performing a peel test and not a test on H-pieces. In the same way, by glueing on site,
one has to wait 21 days before removing the temporary mechanical fixings.
17
1 week
4 weeks
adhesion testing
compatibility testing
The test results will be communicated by letter,
confirming material suitability or identifying
potential problems.
3. Bonding and production documents
your time
as required
at project completion
(on request)
18
Project Checklist
Dear Customer:
The DOW CORNING Structural Glazing Checklist is designed to provide our Technical Service Engineers with a full
understanding of the details of your project. Completion of ALL SECTIONS of this 4-page Checklist initiates our technical
support of the project, producing a documentation review, adhesion and compatibility testing, and final warranty.
A. Project Identification
A.1.
A.2.
A.3.
B. Project Partners
B.1.
B.2.
B.3.
B.4.
B.5.
C.2.
For 2-sided system, are the horizontal or vertical joints structurally glazed?
Are the non-structurally glazed sides unfastened or mechanically fastened?
Are the two structurally glazed sides shorter, longer, or equal in length to the non-glazed sides?
C.3.
C.4.
C.5.
Are all units vertical or are there sloping elements? Angle (degrees) from horizontal: ___________________
C.6.
page 1 of 4
Project Checklist
D. Joint Dimensioning
D.1.
Structural Silicone between glass/frame is 1-component (DC 895), 2-component (DC993) or others ___________
between glass/glass is 2-component (DC3362) or 1-component (DC3793)
D.2.
Maximum wind pressure for geography of project (obtained from architect or authorities):
________ Pa or kN/m2
D.3.
________ kN/m2
E. Vision Glass
E.1.
Width _______m, height _______m, thickness ______mm of the single glass with the largest short-side
dimension panel for this project
E.2.
Width _______m, height _______m of the insulation glass with the largest short-side dimensionpanel
for this project
E.3.
Thickness _______mm of outer glass, spacer distance ______mm, thickness ________mm of inner glass panel
E.4.
Insulation glass panel with the smallest surface area: Width _______m, heigth _______m
E.5.
E.6.
E.7.
E.8.
E.9.
Yes
No
F. Spandrel Glass
F.1.
Width _______m, height _______m, thickness ______mm of the single glass panel with the largest shortside dimension for this project
F.2.
Width _______m, height _______m of the insulation glass panel with the largest short-side dimension for
this project
F.3.
Thickness _______mm of outer glass, spacer distance ______mm, thickness ________mm of inner glass panel
F.4.
Insulation glass panel with the smallest surface area: Width _______m, heigth _______m
F.5.
F.6.
F.7.
F.8.
F.9.
Yes
No
Project Checklist
G. List of Samples for Laboratory Testing
Please provide samples representative of the lot to be used on the project
G.1.
6 pieces, 15 cm long 1
G.2.
Coated, Enamelled, or
previously untested glass:
3 pieces, 20 cm x 15 cm
(only at our request normally)
G.3.
1 piece, 10 - 20 cm long
(of each material)
G.4.
3 pieces each
1: Exception: projects made in France or elsewhere in Europe under the control of an official French company
(Veritas, Socotec, etc) must submit 18 extra profiles that are 7.5 cm in length.
Vertical & horizontal cross-section of the structural seals of vision and spandrel units.
H.2.
page 3 of 4
Project Checklist
Description of Test Samples
Please complete the following list for each shipment of samples:
PROJECT NAME / CITY / COUNTRY _______________________________________________________________
DC993
DC3793
DC3362
DC797
DC897
For substrates requiring adhesion testing, please indicate on the samples the suface to be tested.
Profile:
_____
Anodised Aluminium
(company performing anodisation:
Colour _____________
)
_____
Polyester-coated Aluminium
Colour _____________
_____
Stainless Steel
Colour _____________
___________________
Vision Glass:
Manufacturer:
________________________________________________
________________________________________________
________________________________________________
1
(outside)
4
(inside)
enamelled
PU coating
PU film
Yes
No
Manufacturer:
________________________________________________
________________________________________________
________________________________________________
1
(outside)
4
(inside)
enamelled
PU coating
PU film
Yes
No
Accessory Materials: Please list the Manufacturer, Brand Name, and type of material to be used:
1. Spacer _____________________________________ / _______________________ / __________________________
2. Backer rod _________________________________ / _______________________ / __________________________
3. Preformed rubber or plastic
profiles or gaskets ___________________________ / _______________________ / __________________________
4. Setting blocks ______________________________ / _______________________ / __________________________
5. Other material ______________________________ / _______________________ / __________________________
Dow Corning is a registered trademark of DOW CORNING Corporation.
Printed in Belgium
page 4 of 4
Ref.: 62-0978B-01
Spandrel Glass:
AUSTRIA, GERMANY,
SWITZERLAND & EASTERN
EUROPE
DOW CORNING GmbH
Rheingaustr. 34
65201 Wiesbaden
GERMANY
Tel: INT + 49 (0)611 - 237 906
Fax: INT + 49 (0)611 - 237 603
SPAIN & PORTUGAL
DOW CORNING Ibrica S.A.
Avda Diagonal 613 - 5
08028 Barcelona
SPAIN
Tel: INT + 34 (0)93 - 405 12 15
Fax: INT + 34 (0)93 - 405 38 94
www.dowcorning.com
The information contained herein is offered in good faith based on Dow Cornings research and is believed to be accurate. However, because conditions and
methods of use of our products are beyond our control, this information shall not be used in substitution for customers tests to ensure that Dow Cornings
products are fully satisfactory for your specific applications. Dow Cornings sole warranty is that the product will meet its current sales specifications. Your
exclusive remedy for breach of such warranty is limited to refund of purchase price or replacement of any product shown to be other than as warranted. DOW
CORNING SPECIFICALLY DISCLAIMS ANY OTHER EXPRESS OR IMPLIED WARRANTY OF FITNESS FOR A PARTICULAR PURPOSE OR
MERCHANTABILITY. UNLESS DOW CORNING PROVIDES YOU WITH A SPECIFIC, DULY SIGNED ENDORSEMENT OF FITNESS FOR USE, DOW
CORNING DISCLAIMS LIABILITY FOR ANY INCIDENTAL OR CONSEQUENTIAL DAMAGES. SUGGESTIONS OF USE SHALL NOT BE TAKEN AS
INDUCEMENTS TO INFRINGE ANY PATENT.
ELG.: 62-0979C-01