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Effects of applied pressure and melt and die temperatures on the microstructure of squeeze
cast LM13 alloy were examined. The results showed that application of pressure during
solidication decreased the grain size and SDAS of the primary phase and modied the
27 July 2008
eutectic silicon particles. With application of an external pressure of about 100 MPa, the
average SDAS and the average aspect ratio of eutectic silicon particles were reduced from
47 m and 5 to about 34 m and 1.5, respectively. SDAS of the primary phase and the
average aspect ratio of eutectic silicon particles decreased slightly with a drop in the melt
Keywords:
or die temperatures, reaching to 32 m and 1.25, respectively, for the best conditions.
Squeeze casting
Solidication
Pressure
Microstructure
Modication
1.
Introduction
Corresponding author.
E-mail address: behzn@cc.iut.ac.ir (B. Niroumand).
0924-0136/$ see front matter 2008 Elsevier B.V. All rights reserved.
doi:10.1016/j.jmatprotec.2008.08.035
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2.
3.1.
Effect of pressure
Fixed
parameters
Variable
parameter
Pressure, P (MPa)
Tm = 730
P = 0, 20, 53,
106, 171, 211
Melt temperature, Tm ( C)
Td = 200
P = 171
Die temperature, Td ( C)
Td = 200
P = 171
Tm = 630,
680, 730, 780
Td = 150, 200,
250, 300
Tm = 730
Experimental procedure
3.
Cu
Mg
0.71.5
1.3
0.81.5
1.2
Si
1013
12.3
Fe
Mn
Ni
Zn
Pb
Sn
Ti
<1
0.4
<0.5
0.02
<1.5
1.4
<0.5
<0.03
<0.1
<0.03
<0.1
<0.05
<0.2
0.01
Al
Reminder
Reminder
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Fig. 1 Effect of external pressure on the microstructure of squeeze cast LM13 alloy: (a) 0 (atmospheric pressure), (b) 20 MPa,
(c) 53 MPa, (d) 106 MPa, (e) 171 MPa, (f) 211 MPa (Tm = 730 C and Td = 200 C).
3.1.2.
Fig. 2 Effect of external pressure on the morphology of eutectic silicon particles of squeeze cast LM13 alloy: (a) 0
(atmospheric pressure), (b) 20 MPa, (c) 53 MPa, (d) 106 MPa, (e) 171 MPa, (f) 211 MPa (Tm = 730 C and Td = 200 C).
j o u r n a l o f m a t e r i a l s p r o c e s s i n g t e c h n o l o g y 2 0 9 ( 2 0 0 9 ) 37903797
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Fig. 5 Effect of melt temperature on the microstructure of squeeze cast LM13 alloy: (a) 630 C, (b) 680 C, (c) 730 C, (d) 780 C
(P = 171 MPa and Td = 200 C).
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Fig. 6 Effect of melt temperature on the morphology of eutectic silicon particles of squeeze cast LM13 alloy: (a) 630 C, (b)
680 C, (c) 730 C, (d) 780 C (P = 171 MPa and Td = 200 C).
3.2.
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Fig. 9 Effect of die preheating temperature on the microstructure of squeeze cast LM13 alloy: (a) 150 C, (b) 200 C, (c) 250 C,
(d) 300 C (P = 171 MPa and Tm = 730 C).
Fig. 10 Effect of die preheating temperature on the morphology of eutectic silicon particles of squeeze cast LM13 alloy: (a)
150 C, (b) 200 C, (c) 250 C, (d) 300 C (P = 171 MPa and Tm = 730 C).
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3.3.
Effect of die temperature on the microstructure was investigated using die preheating temperatures of 150, 200, 250 and
300 C, where the melt temperature and the external pressure were 730 C and 171 MPa, respectively. Figs. 9 and 10
demonstrate the microstructure of these samples. Effects
of mold temperature on the SDAS of primary phase and
the average aspect ratio of eutectic silicon particles are represented in Figs. 11 and 12 respectively. The effects are
similar but more pronounced than those of the melt temperature in the range examined. The average SDAS of primary
phase has increased from 32 to 40 m and the average
aspect ratio of eutectic silicon particles has increased from
about 1.45 to 2.2 with increasing the mold temperature from
150 to 300 C. More elongated silicon particles are visible in
Fig. 10d where the die temperature was 300 C. The effect
4.
Conclusion
1. Applied pressure decreases the grain size and SDAS of primary phase. SDAS was dropped from about 47 m for
atmospheric pressure to about 34 m for an external pressure of about 100 MPa.
2. Applied pressure modies and reduces the average aspect
ratio of the eutectic silicon particles. The average aspect
ratio of the eutectic silicon particles was dropped from 5 for
atmospheric pressure to about 1.5 for an external pressure
of about 100 MPa. It has also made the morphology of the
eutectic silicon particles more uniform.
3. Effects of applied pressure on the SDAS of primary
phase and the aspect ratio of eutectic silicon particles
become negligible for external pressures of more than
about 100 MPa. It is postulated that 100 MPa is the external
pressure at which a complete contact between the metal
and die surface is realized.
4. No signicant change in the morphology of primary
phase was observed with melt temperature. However the
SDAS of primary phase and the average aspect ratio of
eutectic silicon particles decreased slightly with a drop
in melt temperature rendering more desirable microstructures.
5. The effect of die preheating temperature is similar but
more pronounced than those of melt temperature in the
range examined.
6. The effects of casting parameters on the microstructure of
LM13 alloy can be justied based on the effects of applied
pressure on the thermal grain renement or modication
of the microstructure. These include change in the melting point of the alloy, possibility of occurrence of a prompt
large under cooling in the melt and improved heat transfer
across the die-metal interface.
Acknowledgment
Fig. 12 Effect of die preheating temperature on the
average aspect ratio of the eutectic silicon particles of
squeeze cast LM13 alloy (P = 171 MPa and Tm = 730 C).
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references
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