Professional Documents
Culture Documents
INTRODUCTION
Part A: Emulsion Test
Emulsion tester is used in the evaluation of inverted emulsion drilling fluids, cement
and fracturing fluid. This test indicates the stability and types of emulsion whether water-inoil or oil-in-water. Time stability and resistance to electrolyte contamination of these systems
can be predicted from a measurement of relative emulsion stability.
Electrical Stability (ES) test is a test that applied to oil-base and synthetic-base muds
that indicates the stability of the emulsion and oil-wetting capacity of the sample. The
electrical stability is determined by applying a steadily increasing sinusoidal alternating
voltage across a pair of parallel flat plate electrodes submerged in the oil base drilling fluid.
Maximum voltage that the mud will sustain across the gap before conducting current is
displayed as the ES voltage.
The composition of the oil base drilling fluid controls the absolute magnitude of (ES).
Several conditions influence the Electrical Stability of a given drilling fluid such as resistivity
of the continuous phase, conductivity of the non-continuous phase, properties of suspended
solids, temperature, droplet size, type of emulsifier used, dielectric properties of the fluids and
shear history of the sample. It is advised to take several readings of ES of the samples to
establish a trend. This series of (ES) measurements will reflect a more accurate condition of
the drilling fluid on which drilling fluid treatments can be based.
Knowledge of the liquid and solids content of a drilling mud is essential for good
control of the mud properties. Such information will often explain poor performance of the
mud and indicate whether the mud can best be conditioned by the addition of water or
whether treatment with chemical thinner or the removal of the contaminant is required.
Similarly, proper control of an oil emulsion mud depends upon knowledge of the oil content.
For muds containing only water and solids, the quantity of each can be determined
from the mud density and from the evaporation of a weighed sample of mud. Oil and water
content can also be obtained by measuring the liquid fraction. The latter method is only
applicable to oil emulsion muds.
The retort kit working principle is based on the heating, vaporisation and
condensation. The mud is heated up to 500C until all the liquid is vaporized. The vapour then
flow into the condenser and condensed back to liquid form.
OBJECTIVES
THEORY
Liquid drilling fluid is often called drilling mud. The main functions of drilling fluids
include providing hydrostatic pressure to prevent formation fluids from entering into the well
bore, keeping the drill bit cool and clean during drilling, carrying out drill cuttings, and
suspending the drill cuttings while drilling is paused and when the drilling assembly is
brought in and out of the hole. The drilling fluid used for a particular job is selected to
avoid formation damage and to limit corrosion.
Drilling fluid composition consists of liquid (oill and water) and solid. Solids content
is fundamental to proper control of mud properties such as rheology, density and filter cake
building properties. Amouts of solids need to be controlled to avoid drilling problem such as
pipe sticking. The volume of solids is found by substraction from 100%. Liquid and solid
content of a drilling mud is essential for good control of the mud properties. Some will
explain poor performance of the mud and indicate whether the mud can be conditioned by
addition of water or whether treatment with chemical thinner or the removal of contaminant
required. The proper control of oil emulsion mud depends of the oil content.
Muds that containing only water and solids their quantity of each can be determined
from the mud density and from the evaporation of a weighed sample of mud. Oil and water
content can also be obtained by measuring the liquid fraction. Latter method is only available
to oil emulsion muds. The mud is heated up to 500 C until all the liquid is vaporized. The
vapour then flow into the condenser and condensed back to liquid form.
The emulsion test is a method to determine the presence of lipids using wet chemistry.
It is used in the evaluation of inverted emulsion drilling fluids, cement and fracturing fluid.
This test indicates the stability and types of emulsion whether it is water-in-oil or oil-in-water.
The time stability and resistance to electrolyte contamination of these systems can be
predicted from a measurement of relative emulsion stability.
Electical Stability (ES) test is a test that applied to oil-base and water-base muds that
indicates the stability of the emulsion and oil-wetting capacity of the sample. It is determined
by applying a steadily sinussoidal alternating voltage across a pair of parallel flat plate
electrodes submerged in the oil base drilling fluid. Maximum voltage that the mud will sustain
across the gap before conducting current is diplayed as the ES voltage. There is a few
conditions influence the Electrical Stability of a drilling fluid such as resistivity of the
continuous phase, conductivity of the non-continuous phase, conductivity of the noncontinuous phase, properties suspended solids, temperature, droplet size, type of emulsifier
used, dielectric properties of the fluids and shear history of the sample. Series of (ES)
measurements will reflect a more accurate condition of the drilling fluid on which drilling
fluid treatments can be based.
PROCEDURES
General Start-Up
1
Mud was prepared by put it into the mud cup until reach the upper indicator of the
cup.
Then, the mud was mixed by using the mixer about 3-5 minutes.