Professional Documents
Culture Documents
be
PROCESS TECHNOLOGY
Can a
Vacuum is widely applied in the chemical and food processing industry, because it permits to perform processes that
cannot otherwise be done under atmospheric conditions.
he most well-known sub-atmospheric application is vacuum distilation, where vacuum is used to lower the boiling point of a solvent or
other chemical compound in order to perform a separation or purification of a high-boiling-point or thermal sensitive product with minimal input
of heat. Vacuum processing is the solution for the increasing high-purity requirements for a growing number of materials in a large variety of
applications. The costs of rejected, off-specification product and the rising energy costs are the main incentives to apply vacuum
as a process aid.
Other vacuum applications in the chemical industry are vacuum filtration, vacuum drying, vacuum evaporation, evaporative cooling, degassing, etc.
Common vacuum applications in the food industry are given in Table 1.
Frequently, food and chemical plants find it less costly to obtain vacuum by means of steam jet ejectors. Especially the chemical industry
makes largely use of steam jet ejec-tors to generate the vacuum required in many distillation processes. Table 2 gives an over-view of
some advantages and disadvantages of steam jet ejectors.
Steam jet ejectors (usually multi-stage) are especially used for wet processes that require vacuum levels ranging from 15 mbar down to 0.1 mbar
vacuum absolute. Water ring
pumps are not capable to generate such a deep vacuum. Moreover, when steam jet ejectors are used to produce the required vacuum for distillation,
evaporation or drying processes, the same steam ejectors can act as condenser for the water or solvent vapours drawn from these processes along with the
air. A cold wall vapour condenser upstream of the steam jet ejector may not be required, except where a
photo: Nitech
Fig. 1: fluctuation of pressure and velocity of the steam/gas-stream over its traject through the steam jet ejector.
very high degree of efficiency is required or where recuperation of solvents is requested. In contrast to steamjet ejectors, water ring pumps may
never act as a condenser in applications where high amounts of solvent or water vapours have to be condensed. In such a situ-ation, always a
barometric or shell-and-tube condenser has to be installed upstream of that water ring pump.
engineeringnet.be
PROCESS TECHNOLOGY
Application
Vacuum Absolute
Function
(mbar)
50 - 100
Sous-vide cooking
milk
50 - 250
Evisceration (poultry, fish, etc.)
100
- 150
300
- 600
50
Vacuum drying
20 - 50 (begin)
1
-3
Fractional distillation of vegetable oil
10
Fractional distillation of essential oils
10
Freezing drying
20
- 50
UHT treatment - vacuum flash cooling of
1 - 4 (end)
De-aeration of water
50
Bottling of beer, soft drinks, mineral and
50 - 60
sparkling water
100
Table 1: vacuum applications in the food industry (Note: with vacuum absolute, we allude to the cacuum pressure measure relative to absolute perfect zero vacuum) .
engineeringnet.be
PROCESS TECHNOLOGY
stage
steam
jet
ejector
with two
baromet
ric
intercon
densers
and one
baromet
ric
aftercon
denser.
compress
ed to a
higher
discharge
pressure.
Fig. 1
demonstr
ates how
the
pressure
and
velocity
of the
steam/
gasstream
fluctuates
over its
traject
through
the steam
jet
ejector.
Fig. 2:
three-
Basic
compo
nents
of a
steam
jet
ejector
A single
stage
steam
ejector can
produce
only a
limited
vacuum
(cfr. Table
2). Multistage
steam
ejectors
(Fig. 2) are
used when
an
application
requires a
pressure
lower than
what
singlestage ejectors can
develop, as
the
first can
develop a
greater
suction
pressure.
With more
stages
added to
the system,
the
pressure of
the first
stage
becomes
lesser and
lesser,
generating
a deeper
vacuum.
The ejector
which the
entrained
gases enter
first, is
called the
first stage
and
subsequent
stages
are
numbered
in
successio
n.
It is
desirable
to connect
a
condenser
to the
discharge
of each
steam jet
ejector to
bring all
steam and
condensabl
e gases to
the liquid
state,
reducing
the load to
the suc-
ceeding
ejector
stage and
thus
imposing
on
subseque
nt stages
the work
of
compressi
ng only
those
gases that
are noncondensa
ble. The
condenser
s so employed
are
known as
intercond
ensers. A
condenser
connected
to the
diffuser
discharge of
the final
stage is
known as
an
aftercond
enser, that
is used to
prevent
the
discharge
of motive
steam and
condensa
ble
process
vapours
into
atmosphe
re.
An
interconde
nser
operates at
pressures
less than
atmospheri
c (under
vacuum).
It is
therefore
necessary
to provide
means for
draining
the mixture
of
condensing
water and
condensed
steam/cond
ensable
vapours
from a
barometric
interconde
nser, or the
condensed
steam/cond
ensable
vapours
only from
a shelland-tube
intercondenser.
The noncondensabl
e vapours
are
withdrawn
from the
top of each
interconde
nser by the
vacuum of
the
subsequent
steam
ejector.
The after-
Steam-jet
Max.
Advantages
Disadvantages
type
absolute
vacuum
(mbar)
1-stage
66
- High achievable vacuum
- Consumption of large amounts
of steam as
2-stage
5-15
- High suction capacities and gas
flow
pressurized motive fluid
3-stage
1-1.5
- Controlable over a wide range
of vacuum
- High energy consumption
4-stage
0.1-0.3
and flow rates
- Low thermal efficiency
particles
- Steam must be dry or should
have less than
corrosive conditions
the ejector vacuum to break or
fluctuate, and
- Simple design
can erode the nozzle and
diffusers.
vapour
operation
densate (waste water)
- Long life-span
- No heat emission
24
PUMPS & PROCESS MAGAZINE n
69 - maart 2011
engineeringnet.be
PROCESS TECHNOLOGY
condenser
operates at
atmospheric
pressure
and is
provided
with a vent
to finally
allow air
and noncondensab
le gases to
escape in
the
atmospher
e.
Barom
etric
conden
sers
A
barometric
condenser
(also called
direct
contact
condenser) is a
vertical
vessel
where
withdrawn
process
vapours are
cooled and
condensed
by direct
contact
with
downward
flowing
cold water
injected
into the
top of the
vessel.
Since the
ope-rating
pressure
of the
condenser is subatmospher
ic (under
vacuum),
collected
condensat
e
(effluent
cooling
water and
condensed
steam/
vapours)
must be
continuous
ly
removed.
That
condensate
is
normally
dropped
into a
recei-ver
tank that is
often
vented to
atmospher
e or a low
pressure
vent
system.
This
creates a
situation
where the
condensate
is under
vacuum in
the
condenser
and is
trying to
move
toward the
receiver
tank that is
under
positive
pressure. To
overcome
this
pressure
differential,
the
condenser
must be
located
higher than
the receiver
tank (the
bottom of
the
condenser
should be at
least 10.4
meters
above the
ground) to
create a tall
barometric
leg (10.4 m
long pipe)
in which a
static
column of
liquid
balances
the
atmospheric
pressure.
The
condensate
must flow
by gravity
through this
long sealed
vertical tail
pipe into
e to gas
accumul
ation.
Fig. 3: if
tail pipe
must
change in
direction, it
should
form at
least a
45 angle
from the
horizonta
l plane;
the
horizonta
l piping
(right
drawing)
is
vulnerabl
a hotwell
(drainage
basin
provided
with an
overflow
or pump)
or a sealed
condensate
tank
(provided
with fluidlevel
control
and
condensate
pump).
The
barometri
c leg
allows the
effluent
coolant
and
condensed
vapours in
the
barometric
condenser
to exit no
matter
what its
vacuum is,
finally
preventing
the
condenser
from
flooding
under
normal
operation.
In the
receiver
tank, the
tail pipe
must be
submerge
d enough
(not less
than 28
cm). If
this seal is
broken,
air will be
drawn into
the
tailpipe,
increasing
the risk for
flooding
the
condenser
and hence
affecting
the
performanc
e of the
downstream
vacuum
source and
the
upstream
vacuum
pro-cess.
The
drainage
lines or
tailpipes
should be
prefe-rably
installed
vertically.
Horizontal
drain leg
runs are
not
recommen
ded,
because
they are
susceptible
to gas
pockets.
The
mixture of
cooling
water plus
con-densed
steam/cond
ensable
vapours
always
contain air
or other
noncondensabl
e gases
which
cling to
upper pipe
surfaces.
All types
of
pipe contain
a certain
amount of
internal
roughness
and,
because of
this, gases
tend to start
clinging and
building up
in the
smallest
crevice. In
addition,
every
flanged
joint has a
slight crack
where a
gasket is
located,
thus
permitting
another
place for
gases to
collect. As
these gases
accumulat
e, they
form tiny
bubbles,
growing
into larger
ones that
eventually
become
big enough
to partially
or completely
block off
piping at
that point.
In that
case, the
condensate
cannot flow
downwards
and soon its
level rises,
flooding the
conden-ser.
If piping
changes
direction, it
must form
at least a
45 angle
from the
horizontal
(Fig. 3).
With this
amount of
sloping,
gases will
either slide
back up the
pipe or
continue
downward
with the
thrust of the
flowing
water. The
45
bend may only installed at no less than 5 pipe diameters away from the
condenser outlet flange. Where there is insufficient height to construct
a proper barometric leg, a low-level, condensate-removal system can
be added. This consists of a receiver equipped with a level controller
and a condensate pump. As a condensate pump removes condensate at
a constant rate, a mechanical level controller opens and closes a valve,
to control the flow of cooling water to the condenser. However, if
either pump or controller fails, there is a risk of flooding the vacuum
system. Direct-contact condensers are easily to design, relatively
inexpensive, and make multi-stage steam jet ejector designs less
vulnerable to damage or fouling resulting from carryover of entrained
solids. The major disadvantage of direct contact condensers is the large
quantity of water that passes through once and goes to disposal,
increasing the cost of wastewater and the environmental impact.
Shell-and-tube condensers
Literature references
Birgenheier D.B., Butzbach T.L., Bolt D.E., Bhatnagar R.K., Ojala R.E., Aglitz
J. (1993), Designing steam-jet vacuum systems, Chemical Engineering, 100
(7), 116-121.
Eckles, A.J. & Benz, P.H. (1992), The basics of vacuum processing,
Chemical engineering, 101 (1), 78-86.
Ojala, R. (1992), Keep ejectors online, Chemical Engineering, 101 (5), 114120.