JIS G 0321: Product Analysis and Its Tolerance For Wrought Steel

JAPANESE
INDUSTRIAL
STANDARD
Translated and Published by
Japanese Standards Association
JIS G 0321
:2010
(JISF)
Product analysis and its tolerance

for wrought steel
ICS 77.040.01;77.140.01
Reference number: JIS G 0321 : 2010 (E)
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Copyright Japanese Standards Association

Provided by IHS under license with JSA
No reproduction or networking permitted without license from IHS
PROTECTED BY COPYRIGHT
Not for Resale
7S
G 0321 : 2010
Date of Establishment: 1966-09-01

Date of Revision: 2010-10-20
Date of Public Notice in Official Gazette: 2010-10-20
Investigated by: Japanese Industrial Standards Committee
Standards Board
Technical Committee on Iron and Steel
JIS G 0321 :2010, First English edition published in 2011-03
Translated and published by: Japanese Standards Association

4-1-24, Akasaka, Minato-ku, Tokyo, 107-8440 JAPAN
JSA 2011
All rights reserved. Unless otherwise specified, no part of this publication may be reproduced or
utilized in any form or by any means, electronic or mechanical, including photocopying and
microfilm, without permission in writing from the publisher.
Printed in Japan
KAIAT

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In the event of any doubts arising as to the contents,

the original JIS is to be the final authority.
G 0321 : 2010
Contents
Scope ...................................................... 1
Normative references ...................................................... 1
Terms and definitions ............................................................................................... 1
4
4.1
4.2
Method of sampling for analysis ...................................................... 2

Method of sampling for analysis ...................................................... 2
Number of analytical samples ...................................................... 3
5
5.1
5.2
Analysis method 3
Chemical composition specified in each standard of wrought steel 3
Chemical composition not specified in each standard of wrought steel 3
Tolerances for product analysis ...................................................... 3
Re-sampling and re-analysis4
(i)

Not for Resale
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Page
G 0321 : 2010
Foreword
This translation has been made based on the original Japanese Industrial Standard
revised by the Minister of Economy, Trade and Industry, through deliberations at
the Japanese Industrial Standards Committee as the result of proposal of revision
of Japanese Industrial Standard submitted by The Japan Iron and Steel Federation
(JISF) with the draft being attached, based on the provision of Article 12 Clause 1
of the Industrial Standardization Law applicable to the case of revision by the provision
of Article 14.
Consequently JIS G 0321: 2005 has been replaced with this Standard.
This JIS document is protected by the Copyright Law.
(ii)
Not for Resale
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Attention is drawn to the possibility that some parts of this Standard may conflict
with a patent right, application for a patent after opening to the public, utility model
right or application for registration of utility model after opening to the public which
have technical properties. The relevant Minister and the Japanese Industrial Standards
Committee are not responsible for identifying the patent right, application for a patent
after opening to the public, utility model right or application for registration of utility
model after opening to the public which have the said technical properties.
JIS G 0321 : 2010
JAPANESE INDUSTRIAL STANDARD
Product analysis and its tolerance for

wrought steel
1 Scope
This Japanese Industrial Standard specifies the product analysis and its tolerance
for the killed steel products of rolled or forged carbon steel, alloy steel, stainless steel
and heat resisting steel (hereafter referred to as "wrought steel").
In addition, the application of this Standard shall be as stated in the individual product standards.
2
Norma ti ve references
The standards listed in table 1 contain provisions which, through reference in this
text, constitute provisions of this Standard. The most recent editions of the standards
(including amendments) indicated in the table shall be applied.
Terms and definitions
For the purpose of this Standard, the terms and definitions given in JIS G 0417
and JIS G 1201, and the following apply:
3.1
heat analysis
This analysis is generally carried out on analytical samples 1) taken during a series
of procedures in which the molten steel is poured into a mould from a ladle and then
solidified.
Note
3.2
1)
Where it is not feasible to obtain the analytical sample from the molten
steel, such as in vacuum arc remelting method (VAR), electro-slag remelting method (ESR), or other method, the analysis is carried out on analytical samples taken from steel ingot, steel slab, or steel material, and
the results are applied to the heat analysis.
product analysis
analysis carried out on analytical samples taken from wrought steel

NOTE:
3.3
The analytical values obtained by a product analysis can differ from

those obtained by a heat analysis due to segregation, and can also show
variation between different samples.
tolerances for product analysis
permissible deviation of the individual value of product analysis from the upper limit
value and/or the lower limit value of the heat analysis specified in a standard of wrought
steels

Not for Resale
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analysis of chemical composition performed by the manufacturer according to a Japanese

Industrial Standard or other certain documented procedure, for determining the representative values of the molten steel
2
G 0321: 2010
NOTE:
For example, when the upper limit value of heat analysis of carbon (C)
specified in a standard of wrought steel is 0.25 %, and the tolerance for
product analysis on the plus side designated in a standard of wrought
steel in accordance with this Standard is +0.03 %, the permissible upper
limit value of product analysis is 0.28 %.
3.4 original analysis method

analysis method not specified in JIS, which falls under either of the following:
a)
An appropriate steel analysis method developed by steel manufacturers, steel users,

laboratories and so on, which is made public in the form of library, research paper and so on, and whose preciseness is verified by the certifying standard material and so on.
b)
An analytical method prepared by altering a part 2) of the procedures of the relevant JIS standard method so as to have a broader range of application, and which
satisfies the critical limit from a certified value, repeatability limit and within laboratory reproducibility limit specified in 7.2 or 7.3 of JIS G 1201.
Note
2)
Mass of sample weighed, aliquot ratio, the amount of extracted solvent,

or other matters.
3.5
sample product
product sampled from the test unit for inspection and/or test
4.1
Method of sampling for analysis

The method of sampling for analysis shall be as follows:
a)
The analytical sample for product analysis shall be taken from a position representing the average chemical composition of the cross-section of the original steel
billet.
If the method of sampling is not specified in the product standard or in the requirements given in the order of the product, the analytical sample may be directly
taken from the specimens or test pieces for the mechanical test, or a sample product.
b)
The analytical sample shall be free from scales, rust, paint, plating metal, decarburized layer and impurities. Further, the analytical sample shall not be used if
oxidized, rusted or soiled during storage.
When the sample is taken from chips produced in machining, the sampling procedure shall be in accordance with 4.4 of JIS G 0417.
c)
When the analytical sample is to be taken directly from a sample product, the
procedure in clause 10 of JIS G 0417 shall be applied. However, if this is impracticable, analytical samples shall be taken by a suitable method referring to 4.1 a)
and 4.1 b). In this case, the sampling method shall be subjected to the agreement
between the purchaser and the manufacturer.

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4 Method of sampling for analysis
3
G 0321: 2010
d)
When the analytical samples for the emission spectrometric analysis and fluorescent X-ray analysis of the product analysis are to be directly taken from a sample
product, the samples which comply with JIS G 1253 and JIS G 1256 shall be taken
in accordance with clause 10 of JIS G 0417. However, when the sample for instrumental analysis can not be taken in accordance with 4.1 a), the analysis shall
not be carried out.
Number of analytical samples

When the number of analytical samples is not specified in a standard of wrought
steel, one sample shall be taken from a unit of products manufactured from the same
heat.
4.2
5 Analysis method
Chemical composition specified in each standard of wrought steel
Analysis method shall be as follows. In the case of doubt arising as to the analytical value obtained by the instrumental analysis, a re-analysis may be performed by a
chemical analysis method.
5.1
JIS
JIS
JIS
JIS
JIS
JIS
JIS
G
G
G
G
G
G
G
1211, JIS G 1212, JIS G 1213, JIS G 1214, JIS G 1215-1, JIS G 1215-2,
1215-3, JIS G 1215-4, JIS G 1216, JIS G 1217, JIS G 1218, JIS G 1219,
1220, JIS G 1221, JIS G 1222, JIS G 1223, JIS G 1224, JIS G 1225,
1257, JIS G 1258-1, JIS G 1258-2, JIS G 1258-3, JIS G 1258-4,
1258-5, JIS G 1258-6, JIS G 1258-7, JIS G 1281
Chemical composition not specified in each standard of wrought steel

Apply methods in 5.1, and if the component or the content rate under question can
not be determined by methods in 5.1, an original analysis method agreed between the
manufacturer and the purchaser shall be applied.
5.2
6 Tolerances for product analysis

The tolerances for product analysis shall be as follows:
a)
The tolerances for product analysis are given in table 2 to table 5.

As a rule, table 2 and table 3 shall be applicable for carbon steel, table 4 for alloy
steel (excluding stainless steel and heat resisting steel) and table 5 for stainless
steel and heat resisting steel. The application of tables shall be as specified in
the respective standards.
b)
The values obtained from the product analysis shall not exceed the prescribed
maximum value of chemical composition plus the upper limit value given in tables
2 to 5 or be lower than the prescribed minimum value minus the lower limit value
given in the said tables. However, the tolerance shall be obtained from the table
of tolerance based on the specified maximum value of chemical composition. If only
the minimum value is specified, the tolerance shall be obtained from the table of
tolerance based on the minimum value of the chemical composition.
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4
G 0321: 2010
c)
For the tolerance of one kind of wrought steel, all or a part of the tolerances in
one table shall be applied, and tolerances in 2 or more tables shall not be used in
mixture.
Re-sampling and re-analysis
When the result of analysis does not conform to this Standard, a re-sampling and
re-analysis may be performed upon agreement between the purchaser and the manufacturer.
Normative references
JIS G 0417 Steel and iron - Sampling and

preparation of samples for the determination of chemical composition
JIS G 1201 Iron and steel-General rules for
analytical methods
JIS G 1211 Iron and steel-Methods for determination of carbon content
JIS G 1212 Iron and steel-Methods for determination of silicon content
JIS G 1213 Iron and steel-Methods for determination of manganese content
JIS G 1214 Iron and steel-Methods for determination of phosphorus content
JIS G 1215-1 Iron and steel-Determination
of sulfur content-Part 1: Gravimetric
method after separation of iron
of sulfur content-Part 2: Gravimetric
method after chromatographic separation
of sulfur content-Part 3: Methylene blue
spectrophotometric method after separation of hydrosulfide
JIS G 1220 Iron and steel-Methods for determination of tungsten content

JIS G 1221 Iron and steel-Methods for determination of vanadium content
JIS G 1222 Iron and steel-Methods for determination of cobalt content
JIS G 1223 Iron and steel-Methods for determination of titanium content
JIS G 1224 Iron and steel-Methods for determination of aluminium content
JIS G 1225 Iron and steel-Methods for determination of arsenic content
JIS G 1226 Iron and steel-Method for determination of tin content
JIS G 1227 Iron and steel-Methods for determination of boron content
JIS G 1228 Iron and steel-Methods for determination of nitrogen content
JIS G 1229 Steel-Methods for determination of lead content
JIS G 1232 Methods for determination of zirconium in steel

of sulfur content-Part 4: Infrared absorption method after combustion in an induction furnace
JIS G 1233 Steel-Method for determination

of selenium content
JIS G 1216 Iron and steel-Methods for determination of nickel content
JIS G 1235 Methods for determination of

antimony in iron and steel
JIS G 1217 Iron and steel-Methods for determination of chromium content
JIS G 1236 Method for determination of tantalum in steel
JIS G 1218 Iron and steel-Methods for determination of molybdenum content
JIS G 1237 Iron and steel-Methods for determination of niobium content
JIS G 1219 Iron and steel-Methods for determination of copper content
JIS G 1253 Iron and steel-Method for spark

discharge atomic emission spectrometric
analysis

JIS G 1234 Methods for determination of tellurium in steel
Not for Resale
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Table 1
5
G 0321: 2010
Table 1
JIS G 1256 Iron and steel-Method for X-ray
fluorescence spectrometric analysis
JIS G 1257 Iron and steel-Methods for
atomic absorption spectrometric analysis
JIS G 1258-1 Iron and steel-ICP atomic
emission spectrometric method-Part 1:
Determination of silicon, manganese,
phosphorus, nickel, chromium, molybdenum, copper, vanadium, cobalt, titanium
and aluminium contents-Dissolution in
acids and fusion with potassium disulfate
Determination of manganese, nickel, chromium, molybdenum, copper, tungsten, vanadium, cobalt, titanium and niobium
contents-Dissolution in phosphoric and
sulfuric acids
Determination of silicon, manganese,
phosphorus, nickel, chromium, molybdenum, copper, vanadium, cobalt, titanium
and aluminium contents-Dissolution in
acids and fusion with sodium carbonate
Table 2
(concl uded)
Determination of niobium content-Dissolution in phosphoric and sulfuric acids or
dissolution in acids and fusion with potassium disulfate
Determination of boron content-Dissolution in phosphoric and sulfuric acids
Determination of boron content-Dissolution in acids and fusion with sodium carbonate
Determination of boron content-Distillation as trimethyl borate
JIS G 1281 Methods for chemical analysis of
nickel-chromium-iron alloys
Tolerances for product analysis of carbon steel (1)

Unit: %
Elements
Si
Mn
Maximum value of prescribed

chemical composition
Tolerance
Lower limit
Upper limit
0.15 or under
0.02
0.03
Over 0.15 up to and incl. 0040
0.03
0.04
Over 0040 up to and incl. 0.80
0.03
0.05
Over 0.80
0.03
0.06
0.30 or under
0.02
0.03
Over 0.30 up to and incl. 0.60
0.05
0.05
0.60 or under
0.03
0.03
0.04
0.04
0.05
0.05
0.060 or under
0.010
0.060 or under
0.010
When the minimum value is

specified.
0.02
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Cu

Not for Resale
6
G 0321: 2010
Table 3
Tolerances for product analysis of carbon steel (2)

Unit: %
Elements

Tolerance on sectional area given below

65000 mm 2
or under
Over
65000 mm 2
up to and incl.
130000 mm2
Over
130000 mm 2
up to and incl.
260000 mm 2
Over
260000 mm 2
up to and incl.
520000 mm 2
Lower Upper Lower Upper Lower Upper Lower Upper

limit limit limit
limit limit limit
limit
limit
C
Si
Mn
0.25 or under
0.02
0.02
0.03
0.03
0.04
0.04
0.05
0.05
0.03
0.03
0.04
0.04
0.05
0.05
0.06
0.06
Over 0.55
0.04
0.04
0.05
0.05
0.06
0.06
0.07
0.07
0.35 or under
0.02
0.02
0.02
0.02
0.03
0.03
0.04
0.04
0.05
0.05
0.90 or under
0.03
0.03
0.04
0.04
0.06
0.06
0.07
0.07
0.06
0.06
0.06
0.06
0.07
0.07
0.08
0.08
0.050 or under
0.008
0.010
0.010
0.015
0.060 or under
0.008
0.010
0.010
0.015
0.03
Cu

specified.
0.02
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Not for Resale
G 0321: 2010
Table 4
Tolerances for product analysis of alloy steel

Unit: %
Elements

Tolerance on sectional area given below

65000 mm 2
or under
Over
65000 mm 2
up to and incl.
130000 mm 2
Over
130000 mm2
up to and incl.
260000 mm2
Over
260000 mm 2
up to and incl.
520000 mm 2
Lower Upper Lower Upper Lower Upper Lower Upper

limit limit limit
limit
limit
limit limit limit
C
Si
Mn
0.30 or under
0.01
0.01
0.02
0.02
0.03
0.03
0.04
0.04
0.02
0.02
0.03
0.03
0.04
0.04
0.05
0.05
Over 0.75
0.03
0.03
0.04
0.04
0.05
0.05
0.06
0.06
0.35 or under
0.02
0.02
0.02
0.02
0.03
0.03
0.04
0.04
0.05
0.05
0.06
0.06
0.06
0.06
0.07
0.07
0.90 or under
0.03
0.03
0.04
0.04
0.05
0.05
0.06
0.06
0.04
0.04
0.05
0.05
0.06
0.06
0.07
0.07
0.050 or under
0.005
0.010
0.010
0.010
0.060 or under
0.005
0.010
0.010
0.010
Cu
1.00 or under
0.03
0.03
0.05
0.05
1.00 or under
0.03
0.03
0.03
0.03
0.03
0.03
0.03
0.03
Ni
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Cr
Mo
Al
0.05
0.05
0.05
0.05
0.05
0.05
0.05
0.05
0.07
0.07
0.07
0.07
0.07
0.07
0.07
0.07
0.10
0.10
0.10
0.10
0.10
0.10
0.10
0.10
0.90 or under
0.03
0.03
0.04
0.04
0.04
0.04
0.05
0.05
0.05
0.05
0.06
0.06
0.06
0.06
0.07
0.07
0.10
0.10
0.10
0.10
0.12
0.12
0.14
0.14
0.20 or under
0.01
0.01
0.01
0.01
0.02
0.02
0.03
0.03
Over 0.20 up to and incl. 0040
0.02
0.02
0.03
0.03
0.03
0.03
0.04
0.04
Over 0040 up to and incl. 1.15
0.03
0.03
0.04
0.04
0.05
0.05
0.06
0.06
0.10 or under
0.01
0.01
0.01
0.01
0.01
0.01
0.01
0.01
0.02
0.02
0.02
0.02
0.02
0.02
0.02
0.02
0.03
0.03
0.03
0.03
0.03
0.03
0.03
0.03

specified.
0.01
0.01
0.01
0.01
1.00 or under
0.04
0.04
0.05
0.05
0.05
0.05
0.06
0.06
0.08
0.08
0.09
0.09
0.10
0.10
0.12
0.12
1.50 or under
0.10
0.10
0.10
0.10
0.10
0.10
0.10
0.10

Not for Resale
8.
G 0321: 2010
Table 5
Tolerances for product analysis of stainless steel and

heat resisting steel
Unit: %

0.030 or under
0.01
Upper limit
0.005
0.01
0.02
0.02
0.03
0.03
0.05
0.10
0.10
1.00 or under
Mn
Lower limit
-
Si
Tolerance
1.00 or under
0.04
0.03
0.04
0.040 or under
0.005
0.040 or under
0.005
Ni
Cr
Mo
Cu
1.00 or under
0.03
0.07
0.07
0.10
0.10
0.15
0.15
0.20
0.20
0.25
0.25
0.30
0.30
0.10
0.10
0.15
0.15
0.20
0.20
0.25
0.25
0.03
0.03
0.05
0.05
0.10
0.10
0.50 or under
0.03
0.05
0.05
0.10
0.10
0.10
0.10
Ti

specified.
0.05
Nb+Ta

specified.
0.05
Al
0.10 or over up to and incl. 0.30
0.05
0.05
0.02
0.02

Not for Resale
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monthly by the Japanese Standards Association, and also provided to subscribers of JIS (English edition) in Monthly Information.
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JAPANESE

Product analysis and its tolerance

Copyright Japanese Standards Association

Date of Establishment: 1966-09-01

JIS G 0321 :2010, First English edition published in 2011-03

Translated and published by: Japanese Standards Association

Copyright Japanese Standards Association

In the event of any doubts arising as to the contents,

Normative references ...................................................... 1

Terms and definitions ............................................................................................... 1

Method of sampling for analysis ...................................................... 2

Tolerances for product analysis ...................................................... 3

Re-sampling and re-analysis4

Copyright Japanese Standards Association

JIS G 0321 : 2010

JAPANESE INDUSTRIAL STANDARD

Product analysis and its tolerance for

Terms and definitions

analysis carried out on analytical samples taken from wrought steel

The analytical values obtained by a product analysis can differ from

tolerances for product analysis

Copyright Japanese Standards Association

analysis of chemical composition performed by the manufacturer according to a Japanese

3.4 original analysis method

An appropriate steel analysis method developed by steel manufacturers, steel users,

Mass of sample weighed, aliquot ratio, the amount of extracted solvent,

Method of sampling for analysis

Copyright Japanese Standards Association

4 Method of sampling for analysis

Number of analytical samples

Chemical composition not specified in each standard of wrought steel

6 Tolerances for product analysis

The tolerances for product analysis are given in table 2 to table 5.

Copyright Japanese Standards Association

Re-sampling and re-analysis

JIS G 0417 Steel and iron - Sampling and

JIS G 1220 Iron and steel-Methods for determination of tungsten content

JIS G 1215-4 Iron and steel-Determination

JIS G 1233 Steel-Method for determination

JIS G 1216 Iron and steel-Methods for determination of nickel content

JIS G 1235 Methods for determination of

JIS G 1217 Iron and steel-Methods for determination of chromium content

JIS G 1236 Method for determination of tantalum in steel

JIS G 1218 Iron and steel-Methods for determination of molybdenum content

JIS G 1237 Iron and steel-Methods for determination of niobium content

JIS G 1219 Iron and steel-Methods for determination of copper content

JIS G 1253 Iron and steel-Method for spark

Copyright Japanese Standards Association

JIS G 1234 Methods for determination of tellurium in steel

Tolerances for product analysis of carbon steel (1)

Maximum value of prescribed

Over 0.15 up to and incl. 0040

Over 0040 up to and incl. 0.80

Over 0.30 up to and incl. 0.60

Over 0.60 up to and incl. 1.15

Over 1.15 up to and incl. 1.65

When the minimum value is

Copyright Japanese Standards Association

Tolerances for product analysis of carbon steel (2)

Maximum value of prescribed

Tolerance on sectional area given below

Lower Upper Lower Upper Lower Upper Lower Upper

Over 0.25 up to and incl. 0.55