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Salvinija Petrulyte,

Renata Baltakyte
Static Water Absorption in Fabrics
of Different Pile Height
Kaunas University of Technology, Abstract
Faculty of Design and Technologies, The static water absorption, fabric thickness and surface density of woven structures were
Department of Textile Technology, investigated. Samples were woven for this experiment using low, medium and high pile of
Studentu 56, LT-51424 Kaunas, Lithuania 6, 9, and 12 mm, respectively. The fabrics were affected by various impacts/finishing like
E-mail: salvinija.petrylute@ktu.lt macerating, washing with detergent, washing with detergent and softener, and tumbling.
rebalta@yahoo.com
It was found that an increase in pile height in many cases causes an increase in water ab-
sorption for grey, macerated, washed with detergent, washed with detergent and softened
fabrics. The biggest differences in water absorption between fabrics with low, medium,
and high loops were determined for grey fabrics, i.e. from 142.9 to 300.8%. Increasing the
tumbling time to 90 - 120 min increased the static water absorption in fabrics with medium
and low loops. Treatment with detergent or with conditioner decreased the thickness of the
fabric compared with grey and macerated ones. The surface density of the variously treated
fabrics generally increased significantly with an increase in pile height.

Key words: static absorption, surface density, terry woven structures, fabric thickness.

to the loop pile facilitating water absorp- with respect to warp density, weft densi-
n Introduction tion, which is thanks to the developed ty, pile height, and the type of yarns used
Terry fabrics are produced using weft, surface. The pile height together with a for producing them. It was found that an
ground warp and pile warp yarns. Pile large density determines the products increase in weft density, warp density or
structure has a very important effect on full bulky handle [2]. The sorption- pile height causes an increase in static
the structure and usage properties of desorption process is very important to water absorption, but the pile height had
terry fabrics. Cotton and linen yarns are maintain the microclimate during tran- the most significant effect. The percent-
very desirable materials for terry fabrics sient conditions [3]. The behaviour of age of water absorption is the lowest for
because of their good water absorption textile in contact with liquid plays an im- open-end yarn, and the highest for two-
properties, bearing in mind that terry portant role in determining clothing per- ply ring carded yarn. The higher twist
materials are widely used for towels, formance and in maintaining body com- values used in the production of open-end
home textile products, sauna dressing- fort [4]. The thermal comfort of clothing yarns are thought to make water penetra-
gowns, headgears, slippers, childrens is associated with the thermal balance of tion inside open-end yarns more difficult.
clothes, hygiene products for babies, etc. the human body as well as with thermal It was concluded that the percentage of
Although the yarn material is an impor- responses to interactions with the textile water absorption decreases with increas-
tant parameter in determining the water and environment system [5]. In this case ing warp and weft densities as the terry
absorption properties of terry fabrics, the air permeability of terry textile also fabric structure becomes dense, whereas
pile characteristics also have an effect on plays a significant role [6, 7]. it increases with an increase in pile height
them. Unfortunately, the literature avail- because of the increased pile warp yarn
able on the water absorption properties of The heterogeneity of pore size, shape and surface area.
terry fabrics is limited. There is a lack of orientation affects the penetration of liq-
detailed studies on such questions as how uid into the yarn structure and, hence, its Regarding water vapour permeability,
the construction of terry fabric affects the liquid retention properties, as exhibited no correlation of this parameter with the
water absorption properties of the ma- by textured filament yarns [8]. In [2] it thickness of knitted fabric was noted [9].
terial, and the influence of the finishing was determined how the level of water There are various test methods used for
procedures of the fabrics on their sorp- sorption ability and handle depends on the evaluation of liquid absorption, such
tion properties. Current mathematical the kind of raw material used, the terry as the aqueous immersion test, the satura-
relationships to express the dependen- fabrics structure and finishing. Fabrics tion value test, the drop test, etc. [4, 10].
cies between the sorption characteristics with cotton, cotton-linen, and cotton- To assess the influence of different wash-
of fabrics and their structural properties hemp pile were investigated. The average ing techniques on denim properties and
were found wanting. water sorption ability of the fabrics after the washing procedure, during which the
washing increases by over 10%, but this textile is affected by a complex of differ-
Absorption properties are determined difference is not statistically significant. ent factors, the changes in thickness and
by the fabrics structure and geometrical The fabrics compression ability was cal- surface thickness were determined [11].
characteristics, such as porosity, thick- culated using the free sample thickness It was found that after simple softening,
ness, pile density, handle etc. as well as after washing and the thickness of the the thickness increased by 12.5%, where-
by finishing procedures like washing, washed sample after compression load- as after washing with chlorine solution, it
softening etc. ing with a force of 1 N/m2. increases by some 7%. Enzyme washing
conditioned fabric thinning and negligi-
Static water absorption defines the The effect of terry fabric parameters on ble changes. Enzyme washing removed
amount of water the terry fabric can ab- water absorption properties using various impurities and loose fibre, smoothening
sorb, which is an important property of fabric constructions without hydrophilic the surface, which caused the thinning.
any terry textile [1]. The high water ab- finishes was investigated in [1]. The wa- Softener precipitates on the yarns and
sorption ability of terry material is due ter absorption properties were analysed fibres, consequently the fabrics thick-

60 Petrulyte S., Baltakyte R.; Static Water Absorption in Fabrics of Different Pile Height.
FIBRES & TEXTILES in Eastern Europe 2009, Vol. 17, No. 3 (74) pp. 60-65.
ness increases. The highest influence Macerating-draying
on the change of the surface thickness Washing with detergent-centrifuging-draying
was found using enzyme washing and Washing with detergent-softening-centrifuging-draying

I, II, III variants


silicone softening. After that the greatest

Grey fabric
Washing with detergent-softening-centrifuging-tumbling for:
reduction in thickness was observed, i.e. 30 min
from 0.42 mm to 0.27 - 0.28 mm. After 60 min
simple softening, the surface thickness 90 min
increased by 17%. The fabric thickness 120 min
[12] could be measured using the FAST 150 min
system.
Figure 1. Scheme of impacting/finishing procedures applied to the fabrics.
The surface density of any woven materi-
als with special reference to terry and pile Table 1. Construction of terry fabrics.
fabrics is an important structural property.
The relationship between the pile height, Fabric variant Pile height, mm Material and linear density of pile warp
surface density, and bending resistance or I 6
softness degree was established. Besides II 9 Bleached linen yarn, 50 tex
this, production parameters such as the III 12
type of softener, colouration method and
fabric structure were found to significant-
ly affect softness, which was particularly Table 2. Determination coefficients of other equations between the Sw, t and d parameters
pronounced for velvet fabric; its softness of the fabrics and tumbling duration.
was found to be better than that of un-cut Determination coefficient R2,
pile structures like terry materials. Since Parameter Fabrics variant
type of equation
the pile height of velvet fabrics is shorter I 0.8885, power; 0.8797, logarithmic
than that of loop pile fabric, the mate- Static water absorption, Sw II 0.7368, power; 0.7135, logarithmic
rials thickness in this case becomes less III 0.1942, linear; 0.1886, exponential
than that of the others [13]. I 0.500, linear; 0.4813, exponential
Fabrics thickness, t II 0.6113, linear; 0.6096, exponential
The aim of this research was to investi- III 0.8516, linear; 0.8500, exponential
gate the static water absorption together I 0.0239, exponential; 0.0236, linear
with the thickness and surface density of Surface density of fabric, d II 0.7192, power; 0.7184, logarithmic
various terry woven structures designed III 0.9662, exponential; 0.9601, linear
with pure linen pile as well as affected by
various impact/finishing procedures.
necessary to complete wetting, and then ter, they were hung for three minutes to
dried in air. Industrial finishing proc- remove excess water, and the weight of
n Experimental esses were performed by the joint-stock the wet samples (mw) was measured. An
company A Grup. In this research, the electronic balance was used in the weight
Object and method of investigation detergent NOG CHT R. Beitlich (Ger- measurements. The static water absorp-
The both sided pile formation principle many) was used for industrial washing tion Sw was calculated using the follow-
was used in the production of the terry at 60C, which was performed in a rope ing formula:
woven structures discussed in this study. bath BK (Russia). The tumbling process
There are three systems in terry fabric, Sw = (mw - md)/md 100
gives a fuller volume and nice handle to
namely weft yarn, ground warp yarn the fabric. For this purpose the samples The fabrics thickness t and surface
and pile warp yarn. The construction were washed with detergent, softened, density d was measured in accordance
of terry fabrics is presented in Table 1. centrifuged, and tumble-dried for dif- with ISO 5084:1996 [14] and LST ISO
The pile and ground warp density was ferent periods: from 30 to 150 min in a 3801:1998 [15], respectively.
250dm-1, and the weft density 200 dm-1. tumbler Aipress 15, model Frofix 7126
The ground warps were plied cotton (Germany). A Tubingal SMF CHT R.
yarns of 25 tex 2, whereas the ground silicone conditioner, Beitlich (Germany)
n Results and discussion
wefts were cotton yarns of 50 tex. Pile was used for softening. After tumbling To assess the influence of water, me-
loops were embedded using four picks. for 30 and 60 min, the fabrics were dried. chanics, heat, and chemical treatment on
The cotton-linen terry fabrics used in the If necessary the samples were dried after terry woven structures, the changes in
experimental work were woven by joint- tumbling for 90 min as well. static water absorption, fabric thickness
stock company A Grup (in Jonava, and surface density were analysed. The
Lithuania). The static water absorption was meas- characteristics of the terry fabrics were
ured according to method [1]. The sam- analysed with respect to pile height as
Figure 1 presents the scheme of im- ples were conditioned in laboratory well. The results of static water absorp-
pacting/finishing procedures applied to conditions, cut into pieces (10 10) and tion, thickness and surface density of the
the fabrics. For the wetting procedure then weighed (md). After that the sam- terry fabrics are presented in Figures 2
the specimens (300 500 mm) were ples were kept for one minute in distilled - 7 (see page 62). In order to describe the
placed into water for 2 - 3 s, which is water. After being removed from the wa- results, polynomial, linear, logarithmic,

FIBRES & TEXTILES in Eastern Europe 2009, Vol. 17, No. 3 (74) 61
I variant II variant III variant I variant II variant III variant

394.1
550.0

337.2
400.0

338.6 .
2
y = 0.005x - 0.6719x + 488.49

306.7
300.8 .
500.0

Static water absorption, %


310.3
275.1
R2 = 0.3100
Static water absoption, %

292.4
300.0 450.0 2
y = -0.0134x + 3.1949x + 249.51

216.0 .
213.5 .
R2 = 0.8267
172.8 .

400.0
2
y = -0.0083x + 2.6667x + 252.8
200.0
142.9 .

2
R = 0.9142
350.0

300.0
100.0
30 60 90 120 150
1 2 3 4 Tumbling period, min
Treatment

Figure 2. Static water absorption of terry fabrics with respect to Figure 3. Static water absorption of terry fabrics with respect to
treatment: 1 - without finishing (grey fabric); 2 - macerating, 3 - the tumbling time.
washing with detergent; 4 - washing with detergent and conditioner.

I variant II variant III variant I variant II variant III variant


6.154
6.168

6.500 4.000 2
y = -0.000008x + 0.0037x + 3.5344
5.616 .
5.667

2
5.552

R = 0.8652
3.800
5.055.

5.500
4.730 .
4.769 .

3.600
Thickness, mm
Thickness, mm

4.500 3.400
y = 0.00002x2 - 0.0022x + 3.5196
3.777
3.352

2
R = 0.7676
3.257
2.919

3.200
3.500
3.000
y = 0.00004x 2 - 0.0042x + 3.1356
R2 = 0.6359
2.500 2.800
1 2 3 4 30 60 90 120 150
Treatment Tumbling period, min

Figure 4. Fabric thickness with respect to treatment: 1 - without Figure 5. Fabric thickness with respect to the tumbling time.
finishing (grey fabric); 2 - macerating, 3 - washing with detergent;
4 - washing with detergent and conditioner.

I variant II variant III variant I variant II variant III variant

700.0 750.0
658.5

2
636.8 .

y = 0.0038x - 0.0192x + 636.4


R2 = 0.9996
635.1

602.9 .

700.0
618.4

650.0
606.1

602.7

Surface density, g/m 2


Surface density, g/m 2

600.0 650.0 2
y = 0.0026x - 0.8057x + 645.26
552.6 .
540.1

2
R = 0.7612
522.0 .

550.0 600.0
516.1

2
y = -0.0043x + 0.7427x + 514.22
2
474.6 .

R = 0.4243
500.0 550.0

500.0
450.0
30 60 90 120 150
1 2 3 4
Treatment Tumbling period, min

Figure 6. Surface density of the fabrics with respect to treatment: Figure 7. Surface density of the fabrics with respect to the tumbling
1 - without finishing (grey fabric); 2 - macerating, 3 - washing with time.
detergent; 4 - washing with detergent and conditioner.

power, and exponential types of regres- It was found that an increase in pile Figure 2 the biggest differences in wa-
sion, were analysed. In Figures 3, 5 & 7 height causes an increase in water ab- ter absorption between I, II, and III vari-
the equations with the highest determina- sorption for grey, macerated, washed ant were determined for grey fabrics:
tion coefficients are shown. Some other with detergent and softened fabrics (the 2.1 times (comparing variants I and III)
types of regressions and coefficients of difference between macerated sample and 1.7 times (comparing variants II and
determination are presented in Table 2 variants I and II is the only one not sta- III), i.e. from 142.9 to 300.8%. Mean-
(see page 61). tistically significant), which is due to while the smallest differences were ob-
an increase in the surface density of the tained for fabrics washed with detergent:
Figure 8 shows microscopic surface fabrics. This tendency confirms data 23.1% (comparing variants III and I) and
views of the terry structures investigated. presented in Figure 6. As is seen from 10.4% (comparing variants III and II). As

62 FIBRES & TEXTILES in Eastern Europe 2009, Vol. 17, No. 3 (74)
is seen from Figure 6 grey fabrics with tensively treated fabrics. The loop pile
a pile height of 12 mm, compared with in grey fabric is stiff and of regular ge- a)
the 6 and 9 mm, demonstrate the biggest ometry; the loops are perpendicular to
differences in surface density compared the fabrics base. The water impact dur-
with analogous macerated fabrics or with ing the macerating procedure or more
fabrics washed with detergent or washed intensive finishing operations changed
with detergent and softened ones. Hence the pile structure of the fabric, resulting
our data are in agreement with those ob- in it being more filled with loops. Soften-
tained by other researchers [1]: the in- ing conditioned the loss of stiffness of
crease in the weight of dry pure cotton the loops throughout, in which the terry
terry fabrics of higher pile is suggested fabrics became soft and bulky. Such a
as a reason for the increase in water ab- structure could provide an easier uptake b)
sorption ability. Besides, these authors of water.
stated that the pile height had the most
pronounced effect on static water absorp- Increasing the tumbling time to 90 -
tion compared with other characteristics 120 min increased the static water ab-
investigated. sorption in variants with medium and low
loops. The polynomial relationships with
Macerating is a very passive procedure the highest determination coefficients,
compared with industrial finishing op- R2 = 0.9142 and R2 = 0.8267, were deter-
erations as it only includes the impact of mined for water absorption with respect
water. Yet such an impact increased the to the tumbling time for fabrics of vari- c)
static water absorption by 49.4 - 25.0% ants I and II, respectively (see Figure 3).
for fabrics with low and medium loops Such coefficients indicate a very good
compared with grey ones, respectively. match between the experimental data and
The difference between macerated vari- polynomial curves. Other kinds of re-
ants III and I-II is less compared with the gression also distinguish sufficiently high
analogous difference in grey fabrics. determination coefficients for variants
Iand II; whereas for the fabric with high
Intensive industrial treatments like wash- loops, the relation between the experi-
ing with detergent or washing with de- mental data and mathematical expression
tergent and softener changes the fabrics is weak throughout (see Table 2). It was d)
structure much more because during the found that during the tumbling period
whole washing cycle, the fabric is affect- investigated, the water absorption of the
ed by a complex of factors like the wash-
fabrics increased from 337.1 512.5%.
ing solution, heat, abrasion, compressive
Tumbling for 30 min increased the ab-
deformation, etc. The important changes
sorption ability of the fabrics compared
in the fabrics structure lead to intensive
with the samples affected by washing
transformation of its physical and me-
and softening procedures (except variant
chanical properties as well as usage pe-
II, for which the increase is statistically
culiarities, such as the fabrics handle.
insignificant). Meanwhile, increasing the
Softening solution acts as an additional
tumbling time to 90 min determined the e)
factor for the fabrics which were sof-
tened after the washing procedure. It was increase in water absorption of the fabrics
determined that the difference in water investigated by 17.7 - 39.6% compared
absorption is 1.9 and 1.8 times for fabrics with samples washed with detergent and
washed with detergent and even 2.2 and those softened. The increase in water
2.0 times for those washed with detergent absorption with respect to the tumbling
and softened compared with grey ones of time could be explained by substantial
I and II variants, respectively. Besides changes in the fabrics structure after
this the water absorption reached highest such intensive and numerous finishing
values in fabrics washed with detergent procedures: washing with detergent-sof-
Figure 8. Microscopic views of terry fab-
and softened, i.e. 310.3% (I variant) - tening-centrifuging-tumbling. Warp pile rics of variant I: a) grey, b) macerated, c)
394.1% (III variant) compared with all yarns became very bulky and fluffy in the washed with detergent, d) tumbled for 60
tumbled fabrics. A certain amount of fly min, e) tumbled for 90 min.
other variants presented in Figure 2. The
water absorption of fabric washed with slipped from the yarns and got trapped in
detergent and softened with a loop pile the fabric, increasing the ability of wa- By increasing the tumbling duration to
of 12 mm is 31.0% higher compared with ter uptake. Very significant increases in 150 min, compared with the duration
grey fabric; however, the difference was water absorption were determined com- of 120 min, the increases in water ab-
95.1-117.1% for fabrics II and I. To our paring fabrics tumbled for 90 - 120 min sorption were not conditioned (except
mind, fibre swelling and the decrease in and grey ones, for example, the water ab- for a slight increase for fabrics with
pore size could be the main reasons for sorption increased 1.5 - 3.3 times in the high loops). Furthermore, it is neces-
the increase in water absorption of in- above-mentioned samples. sary to bear in the mind that prolonged

FIBRES & TEXTILES in Eastern Europe 2009, Vol. 17, No. 3 (74) 63
Table 3. Relative and absolute errors of experimental data for the Sw, t and d parameters The differences in surface density of grey
of terry fabrics. fabric of variant III were 143.8 g/m2 and
102.3 g/m2 compared with those of I and
Impact/ Fabrics Relative error Absolute error
finishing variant
II, respectively. After treatments like
Sw, % t, % d, % Sw, % t, mm d, g/m2
macerating, washing with detergent and
I 3.1 4.3 1.6 4.4 0.219 7.7 washing with detergent and conditioner,
Grey fabric
(without finishing)
II 6.2 1.5 2.0 10.8 0.095 10.2 these differences remained but did not
III 5.4 3.9 3.8 16.2 0.223 23.5 exceed the above-mentioned values.
I 3.7 3.7 2.2 9.2 0.208 11.4
Macerating II 3.8 3.9 2.5 8.2 0.240 15.4 The polynomial relationships with the
III 3.9 2.7 1.6 11.4 0.152 10.5 highest determination coefficients,
R2 = 0.7612 and R2 = 0.9996, were de-
I 5.5 4.7 1.9 15.1 0.176 10.0
Washing with termined between the surface density and
II 4.5 6.1 1.6 13.6 0.206 9.5
detergent tumbling duration for fabrics II and III.
III 3.7 6.2 2.2 12.5 0.294 14.4
Other kinds of equations investigated (ex-
I 2.6 3.8 2.6 8.2 0.124 14.2 ponential, linear) also demonstrate high
Washing with
detergent and II 2.5 2.9 1.7 8.5 0.084 10.0 determination coefficients. However,
conditioner
III 3.1 2.1 2.7 12.0 0.100 17.0 only the polynomial regression showed a
I 5.0 4.3 1.5 16.7 0.134 7.8 slight match with experimental data for
Tumbling in 30
II 3.9 5.4 1.8 13.3 0.189 11.0 variant I (see Figure 7 - page62).
min
III 1.7 2.5 2.2 7.9 0.090 14.1
The experimental results were statistical-
I 4.5 5.6 4.4 16.1 0.160 24.2
Tumbling in 60 ly evaluated at a confidence level of 95%.
II 5.2 2.8 1.5 18.7 0.096 9.1
min Full statistical analysis was performed
III 6.3 1.9 8.2 31.4 0.071 53.6 and the standard deviation, coefficient of
I 2.0 3.5 1.8 8.5 0.110 9.7 variation, absolute error, and relative er-
Tumbling in 90
min
II 2.7 2.4 1.2 12.2 0.086 6.9 ror were calculated. Relative errors and
III 4.2 1.5 3.1 19.3 0.059 20.9 absolute errors of the experimental data
I 0.7 4.1 0.5 3.5 0.132 2.4 are presented in Table 3. Statistical anal-
Tumbling in 120
II 2.6 1.8 2.3 11.5 0.064 13.3 ysis of the experimental data showed that
min
III 2.8 2.2 1.7 12.3 0.086 11.8
the coefficients of variation for the static
water absorption of terry fabrics and
I 2.1 3.2 1.8 9.5 0.104 9.7
Tumbling in 150 the surface density of the fabrics gener-
II 5.9 1.3 7.1 25.2 0.048 41.3
min ally did not exceed 5.0%, except for iso-
III 4.4 1.2 3.3 22.4 0.047 24.0 lated instances in which they are higher,
whereas the coefficient of variation of
tumbling could over dry the textile, and ter the fabric had been analysed follow- the fabrics thickness varied from 2.1 to
therefore the recommendation to extend ing the tumbled periods (see Figure 5 see 11.8%. The relative errors of all param-
the tumbling procedure to no longer than page 62). The data showed that generally eters investigated varied within the range
120min could be substantiated. the thickness is bigger with a higher pile, of 0.5% to 5.0%, except in some cases
confirming the effect of terry fabric con- where the values gowent up to 8.2 %.
As is seen from Figure 4 (see page 62), struction. If we compare grey fabrics and
the fabrics thickness did not change af- those tumbled for 30 min, the decrease n Conclusion
ter the macerating procedure compared in fabric thickness could be explained
The pile height of terry woven fabrics
with grey fabrics, except the variant by the changes in loop pile structure: the
had a significant effect on their static wa-
with low loops, but here the difference loops are rigid and range perpendicularly
ter absorption. The biggest differences in
is slight. Treatment with detergent and/ to the base of the fabric in grey textile;
static water absorption between variants
or conditioner decreased the thickness the loops are bulky and in some cases of investigated were determined for grey
of the fabric by 15.8 to 52.7% compared spiral or snarl configuration in tumbled fabrics. This was due to the increase in
with the grey ones. The authors in [2] fabrics. Until the tumbling procedure, the surface density of the fabric.
stated that the shrinkage of treads occur i.e. analysing macerated, washed with
during washing, followed by pile flatten- detergent, washed with detergent and Some changes in the static water absorp-
ing, which consequently decreases the conditioned samples, the thickness of the tion were determined even after a passive
fabrics thickness. Our results confirmed fabric continuously decreased for all var- procedure like the macerating one. Com-
this opinion. Of course, such changes in iants, except in some cases. The remains pared to the grey samples, an increase in
fabric thickness may valuably influence of small particles and amounts of fly are water absorption of up to 1.8-2.2 times
the handle of the textile. removed during washing by decreasing was found for terry fabrics washed with
the fabrics thickness. detergent, for those washed with deter-
The tendency of a fabrics thickness to As was hoped, the surface density of the gent and softened ones with low (6 mm)
increase during tumbling is noticeable, fabrics generally increased with an in- and medium (9 mm) loops. The increases
but in many cases the changes were crease in pile height for variously treated for washed and softened fabrics were
found to be statistically insignificant af- fabrics (see Figure 6 and 7 - page 62). 310.3 - 394.1% compared with grey

64 FIBRES & TEXTILES in Eastern Europe 2009, Vol. 17, No. 3 (74)
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The differences in surface density of grey proach on the Performance of Towels
fabric with high loops was 143.8 g/m2 Part I. Bending Resistance or Softness
and 102.3 g/m2 compared with the fab- Analysis, Fibres & Textiles in Eastern Eu-
ric designed with low and medium ones, rope, Vol. 14, No. 1 (55), 2006, pp. 39-46.
respectively. 14. Textiles Determination of Thickness
of Textiles and Textile Products. ISO
References 5084:1996.
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Fabrics, Fibres & Textiles in Eastern Eu-
rope, Vol. 14, No. 2 (56), 2006, pp. 59-63. Received 28.10.2008 Reviewed 10.02.2009

FIBRES & TEXTILES in Eastern Europe 2009, Vol. 17, No. 3 (74) 65

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