Chapter 1 Introduction 1

1.1 Product Introduction 1

1.1.1 Product Properties 1
1.1.2 Product Use 3
1.1.3 Status and Role in the National Economy 3
1.1.4 domestic and foreign production methods 4
1.1.5 Production Status at Home and Abroad 5
Chapter 2 Chemical Separation Technology 8
2.1 Overview of Chemical Separation Technology 8
2.2 Importance of chemical separation technology 8
2.3 Domestic and International Progress of Chemical Separation Technology 9
2.3.1. Diversity of chemical separation technologies 9
2.3.2. Complexity of chemical separation technology 10
2.3.3 Opportunities and Challenges for Separation Technology 10
2.3.4. Several characteristics of chemical separation technology development 11
Chapter 3 Binary Mixing Distillation 12
3.1 Principle of distillation 12
3.2 Types of Distillation Column Equipment 12
3.3 Progress of Plate Rectification Tower Technology 15
Chapter 4 Design and Calculation of Rectification Tower 15
4.1 Determination and description of design plan 15
4.1.1 Operating Pressure 15
4.1.2 Feeding conditions 15
4.1.3 Heating Method 15
4.1.4 Reflow ratio 15
4.1.5 Reflow method 15
4.1.6 Selecting a Plate Type 15
4.2 Process Calculation of Rectification Tower 16
4.2.1 Material Balance 16
4.2.2 Determination of operational reflux ratio and number of theoretical plate layers 16
4.2.3 Estimation of the efficiency of the entire tower and the determination of the number of
actual trays 19
4.3 Calculation of Tower Process Dimensions and Calculation of Related Physical Data 19
4.3.1 Calculation of the rectification section 20
4.3.2 Calculation of stripping section 21
4.4 tower size calculation 22
4.4.1 Board Spacing 22
4.4.2 Tower Space 22
4.4.3 Feed plate space 22
4.4.4 Additional Height at the Bottom 22
4.4.5 Spacing of manhole trays 22
4.4.6 Head Height 22
4.4.7 Skirt Height 22
4.4.8 The total height of the tower 23
4.5 Calculation of the major process dimensions of the trays 23
4.5.1 Calculation of Rectification Section 23
4.5.2 Calculation of stripping section 25
4.6 Fluid Mechanics Check of Sieve Plates 28
4.6.1 Hydrodynamic verification of rectifying section 28
4.6.2 Hydrodynamic checking of stripping section 29
4.7 Plate Load Performance Chart 31
4.7.1 Tray loading performance chart for rectifying section 31
4.7.2 Tray loading performance chart for stripping section 34
Chapter 5 Calculation and Selection of Auxiliary Equipment 38
5.1 Calculation and Selection of Condensers 38
5.1.1 Determine Design Plan 38
5.1.2 Determination of Physical Properties 38
5.1.3 Estimating heat transfer area 39
5.1.4 Condenser Selection 39
5.2 Reboiler Calculation and Selection 39
5.2.1 Determining the Design Plan 39
5.2.2 Determining Physical Properties 39
5.2.3 Estimating Heat Transfer Area 40
5.2.4 reboiler selection 40
Chapter 6 Process Flow Chart of Rectification Unit 41
References 42
Acknowledgement................................................................................................................43