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J. Bon, P. J. Bon, A. J. Ortega, W. Nalepa, and R. Koo, Petrolab Australia Pty. Ltd.
This paper was prepared for presentation at the SPE/IATMI Asia Pacific Oil & Gas Conference and Exhibition held in Jakarta, Indonesia, 17-19 October 2017.
This paper was selected for presentation by an SPE program committee following review of information contained in an abstract submitted by the author(s). Contents
of the paper have not been reviewed by the Society of Petroleum Engineers and are subject to correction by the author(s). The material does not necessarily reflect
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consent of the Society of Petroleum Engineers is prohibited. Permission to reproduce in print is restricted to an abstract of not more than 300 words; illustrations may
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Abstract
PVT samples captured by openhole formation testers in wells drilled with Oil Based Mud (OBM) will
often suffer some degree of measurable contamination1-5. The contamination is even further pronounced for
gas condensate reservoir fluid systems. Often many years will pass before production or the opportunity
to re-sample the reservoir fluid and these contaminated samples are all there is to work with until that
time. Improved understanding of the effect that OBM will have on these fluids will lead to improved
characterization of the native reservoir fluid.
The primary objective of this work was to design a new experimental laboratory method to contaminate
a clean reservoir fluid PVT sample with OBM and capture the live single-phase fluid again under dynamic
conditions.
This experimental set-up will enable a laboratory to prepare samples representing PVT samples captured
by Wireline Formation Testers (WFT) from an OBM drilled well, as well as the clean reservoir fluid to work
with for comparison. It is envisaged that such an experimental setup will be able to be used to generate data
to then study the effect of OBM contamination of PVT samples and ultimately improve the ability to correct
PVT data on contaminated samples to obtain representative PVT properties.
In order to test the experimental test method, base oil from an OBM was used to contaminate a gas
condensate PVT sample with Condensate Gas Ratio (CGR) of 25 stb/MMscf. The data obtained from results
from both contaminated and uncontaminated sub-samples were then used to investigate the effect of OBM
on PVT properties.
Sufficient sample was obtained in order to measure dew point, Z-factor, CGR and composition of
the resulting contaminated samples to compare to the same properties from the original uncontaminated
reservoir fluid sample.
In this paper we present the following:
• A new experimental set-up was designed to create contaminated PVT samples from a clean sample
under dynamic conditions – flowing within a porous media at reservoir conditions.
• With the experimental set-up we were able to obtain samples and data for comparison of a clean
and OBM contaminated sample
2 SPE-186256-MS
• Results indicate that under the right conditions, a condensing-vaporising partial miscibility
dynamic is established between the gas condensate reservoir fluid and base oil.
Introduction
Several methods exist for obtaining PVT samples from an oil or gas reservoir6-8. Wireline samples captured
in openhole conditions while logging with Wireline Formation Testers (WFT) have become increasingly
popular in recent times, this development mainly comes from vast improvements made to formation
testers in the 1990s9. These tools use inbuilt analytical equipment to measure fluid properties downhole to
determine the quality of the reservoir fluid immediately prior to sampling2,5,10-12.
Drilling with OBM has also become increasingly popular in recent years due to shortening drilling time,
therefore saving costs13. Furthermore, OBM can have positive effects by avoiding near wellbore damage
due to Water Based Muds, for example fines migration or swelling of clays14.
Offshore and remote onshore exploration, with high drilling costs have benefitted from both using OBM
to reduce drilling time, and obtaining WFT samples while logging providing PVT quality representative
reservoir fluid samples without well testing. However, PVT samples captured by WFT will suffer from
contamination by the mud filtrate from OBM as the fluids are, at least partially, miscibile5,13,15.
A few studies have been conducted to determine the effect on the composition and PVT properties of
reservoir fluids contaminated by OBM in order to obtain best practices for cleanup of the reservoir fluid
and correction of the PVT properties such that accurate PVT data can be obtained, and the interaction of
the two fluids better understood. These studies were performed either through computerized modeling15,
contamination of the stock tank hydrocarbon liquid from a reservoir fluid1, or contamination at live
conditions in a PVT cell16.
We have observed through laboratory analysis of contaminated PVT samples, and either mud filtrate
or base oil, that the OBM components do not necessarily dissolve evenly into the reservoir fluid. This
is observed when mathematically removing the OBM components from a contaminated reservoir fluid
composition that certain components may need to be over subtracted while others still appear to carry
contamination while seeking the line of best fit through the fingerprint data. This effectively leads us to
conclude that partial miscibility has occurred, with certain components dissolving preferentially more than
others.
If the situation is similar to that of a near miscible flood on small scale, then there is a possibility that
not only are certain OBM components preferentially dissolving into the reservoir fluid, but that certain
components of the reservoir fluid may be preferentially dissolving into the mud filtrate. Part of this work
was to seek experimentally if C12+ components from the reservoir fluid could be lost to the filtrate in the
near wellbore region.
An in-house test method was designed to contaminate an uncontaminated PVT sample at reservoir
conditions and enable us to analyse the interaction of the two fluids. The test method bears similarities to that
of a slim tube experiment for miscibility studies and effectively allows the two fluids to interact dynamically
within a porous media. The reservoir fluid composition, fingerprint, Condensate Gas Ratio (CGR), dew
point and Z-factor were measured prior to contamination, and on three contaminated sub-samples.
In order to test the experimental method, we used a gas condensate reservoir fluid and a base oil from a
synthetic OBM. For this study, a lean gas condensate reservoir fluid was targeted as minor contamination
can have a very large effect on measured PVT properties.
We observed a condensing-vaporising partial miscibility dynamic established between the gas condensate
reservoir fluid and base oil. This implies that not only are base oil components being vaporised into the
reservoir fluid phase, but also, heavy components in the reservoir fluid are being condensed into the base
oil. This was very dependent on the amount of time allowed for the two fluids to interact.
SPE-186256-MS 3
Multiple methods to mathematically correct contaminated reservoir fluid compositions exist. With the
data generated we were able to check the different methods and compare the mathematically cleaned
compositions to the original measured fluid sample. Overall, mathematically cleaned compositions matched
well with the original composition.
The data suggests that the wireline samples collected from OBM drilled wells have even further
complexity. Obtaining best samples may not only be due to duration of sampling, but also to the depth of
invasion, reservoir fluid composition, reservoir pressure and temperature, and base oil composition.
Background
The difficulty in determining the amount of effect the OBM contamination has on a given PVT sample is
that the clean reservoir fluid cannot be obtained for comparison. This work aims to solve that issue so that
studies may be conducted into the effect it may be having. In order to design the test a review of previous
work on the topic and related information was performed. A summary of relevant information follows.
Figure 1—GC-FID Chromatogram example of a narrow spectrum base oil, with only three key components, C15, C17 and C19.
4 SPE-186256-MS
Figure 3—GC-FID Chromatogram of a broad spectrum base oil with a very wide array of components from C9 to C22.
There is clearly a significant difference in the two "broad spectrum" base oils. The example in Fig. 2 has
much fewer components than the example in Fig. 3. From purely a reservoir fluids analyses point of view,
the narrow spectrum OBM are easier to account for than broad spectrum. Furthermore, if there are fewer
components in the base oil, it is much easier to see the content of the components native to the reservoir fluid.
This is because the OBM components mask fewer of the native reservoir fluid components, to the extent
that mathematical cleanup up can be done by skimming off the OBM components from the contaminated
composition.
Broad spectrum OBM can be difficult to mathematically remove. This is particularly true if the reservoir
fluid is a gas condensate with very few C20+ components, as the OBM components will mask virtually all
C10+. This can have a major effect on dew point and RLD prediction. Furthermore, if the stock tank liquid
fraction of the reservoir fluid (be it oil or gas) has some biodegradation, it can be difficult to determine the
concentration of OBM in the reservoir fluid.
4. Build an Equation of State (EoS) model and tune to the measured contaminated fluid data
5. Determine "Mathematically Cleaned" composition
6. Adjust EoS model to a "Mathematically Cleaned" composition
Note – step 6 (adjusting EoS) model can be done in a number of ways. Sah et al., 2012 suggested building
EoS models for the cleaned composition and base oil. Then combine these fluids numerically to seek to
match experimental data from contaminated reservoir fluid18.
A few methods exist for numerically removing the OBM components from the reservoir fluids
composition. In general, these work with the following assumptions:
• The C8+ weight fraction of the reservoir fluid follows a logarithmic decay function with molecular
weight.
• The base oil components are fully miscible and dissolve evenly within the reservoir fluid
Of the assumptions listed above, the first is robust since most OBM are made up of components C10+. The
second assumption holds true where no biodegradation exists, the more biodegraded the reservoir fluid, the
less linear the logarithmic function will be. The third assumption is where we observed most deviation. In
samples where OBM contamination is low, the effect is minimized, and the linear relationship between log
weight percent and molecular weight can be more easily obtained. After achieving the line of best fit, any
OBM components still not overlying the linear relationship can be forced to fit. Where there is high OBM
contamination, the linear relationship can become difficult to find, particularly if the OBM components
have not evenly dissolved into the contaminated sample. This introduces error to the numerically cleaned
composition.
A few different methods to numerically clean the contaminated composition are summarized below,
Nagarajan et al., (2010) describe these in greater detail13.
Skimming Method
In the Skimming method, a linear relationship is sought for the log decay function in the flash liquid, that is,
log wt% versus molecular weight (MW). Components in the OBM are disregarded when seeking the linear
relationship. The components where OBM exists are then picked from the best fit of the linear relationship
determined13.
Subtraction Method
In the subtraction method, each of the OBM components is proportionately subtracted from the
contaminated flash liquid composition. A contamination factor is applied to the base oil composition and
adjusted until the best fit is achieved on the log decay function13.
K-Value Method
Nagarajan et al. (2010) proposed the K-Value method to adjust for OBM when partial miscibility has
occurred and components have not evenly dissolved into the reservoir fluid13. Furthermore, it does not rely
on the log linear relationship of the C8+ components.
In this method, a preliminary cleaned composition is obtained by either the skimming or subtraction
method. Then the base oil composition is added back in and the contaminated composition is recalculated
and compared to the measured values. In components where the composition does not match, the OBM
contamination factor is adjusted (component by component) in a manner proportional to the reservoir
condition K-value of that component.
• The reservoir fluid and the mud filtrate being miscible. Therefore, with sufficient flow the oil itself
should clean the near wellbore zone of invasion of mud filtrate on its path to the WFT probe5.
• Since the reservoir fluid carries large quantities of C10+ components, once OBM contamination is
minimized to a low content (e.g. <2% by weight), the effects on both the composition and PVT
properties are minimal and correction has shown very good results.
On the other hand, gas condensate reservoirs have shown to suffer significantly more from OBM
contamination5,15. This is due to:
• The reservoir fluid and the mud filtrate often being immiscible with each other (yet partial
miscibility occurs). This implies that two-phase flow occurs in the near wellbore region of reservoir
gas and mud filtrate. A relative permeability effect is created and the mud filtrate is far more
difficult to clean out.
• The reservoir fluid carries very small, but significant, quantities of C10+. Although OBM
contamination may be decreased to a minimal and asymptotic level (e.g. < 2 % by weight), this
amount of contamination will still account for a significant part of the C10+ in the contaminated
sample and lead to an OBM contamination of a large proportion of the stock tank condensate
(depending on CGR of fluid sample it could be 10-80 % by weight).
Much of the recent developments associated with WFT type samplers has been related to determination
of the point at which contamination is minimized or reduced to undetectable levels, speeding up time to
clean up the samples2-5,21-23.
A schematic of a generic wireline formation tester (WFT) sampling tool configuration is shown in Fig.
4 (left). Multiple analytical equipment may be added to these tools to measure fluid properties prior to
and during sampling. This enables sampling personnel to initially dump filtrate prior to catching a PVT
sample and determine the appropriate time to commence sampling. A schematic of sampling process by
WFT within the wellbore is shown in Fig. 4 (right). The near wellbore zone shows the invaded near wellbore
SPE-186256-MS 7
region. The sample probe is pressed up against the side of the wellbore and draws fluid into the tool. The
reservoir fluid must first displace filtrate from the invaded zone, then travel through the reservoir rock in
this region to the sampling probe in order to be sampled.
Figure 4—(left) Schematic of generic wireline formation tester (WFT) sampling tool
configuration. Figure 4 (right): Schematic of sampling process by WFT within wellbore.
Miscibility occurs when both fluids mix completely in a single continuous phase (even if they are two
different phases in their extremes) in this dynamic porous medium. Miscibility can be established a number
of ways:
• First contact miscible – the two fluids immediately dissolve within one another in all proportions
• Multi-contact miscible – the two fluids are initially partially miscible but form a bank of fluid with
components from each of the two fluids which is miscible with the two original fluids. This can
occur in a few ways:
○ Vaporising Gas Drive – some components of the liquid phase are vaporized into the injection gas
○ Condensing Gas Drive – some components of the gas phase are condensed into a portion of
the reservoir oil
○ Condensing-Vaporising Gas Drive – both of these happening at the same time, where injection
gas components dissolve into a portion of the reservoir oil, and some reservoir oil components
are vaporized into the injection gas. Dynamically and with further injection, a miscible bank is
formed with a spectrum of compositions ranging from 100% injection gas to 100% reservoir oil.
In miscible gas flooding, focus is often placed on the pressure at which the injection gas is miscible
with the reservoir oil and reservoir temperature, this is the minimum miscibility pressure or MMP. Often
injection conditions just below the MMP are selected as it can deliver excellent oil recoveries, minimizing
the compression costs required. In this "near miscible" condition, the two fluids are not quite miscible, but
benefit occurs through partial (and almost complete) miscibility of the two fluids.
The OBM filtrate and reservoir gas will likely behave as an immiscible gas flood, but may achieve partial
miscibility. In general it is assumed that only filtrate components will be vaporized into the reservoir gas,
but another condition exists where reservoir gas components are also dissolving into the filtrate.
Carrying this analogy further, the laboratory industry standard for analyzing the interaction of an injection
gas and a reservoir oil is to use a Slim Tube. As such, we felt that to study the interaction of a gas condensate
reservoir fluid system and a base oil, a similar experimental design would be of great value.
Methodology
We were targeting the development of a method to contaminate a sample under dynamic conditions with
a dynamic interaction between the gas condensate and reservoir fluid. In particular we wanted to observe
whether particular OBM components were preferentially being dissolved into the reservoir gas. As such,
and with our laboratory's experience in miscible flooding, our first attempt was to essentially run a modified
Slim Tube test.
through this immobile phase on its way to the PVT sampling manifold. The reservoir gas vaporized some of
the OBM components, but also some of the reservoir gas components condensed into the immobile liquid
phase.
The flood had been immiscible, shown by the low recovery and observation of two-phases in the sight
glass – yet clearly some degree of component exchange between the base oil and reservoir gas had occurred,
as such it should be described as a partially miscible (but still immiscible) displacement. The heavier
components of the reservoir gas condensing into the immobile base oil well after breakthrough had occurred.
After making this initial experiment, we decided that a significantly shorter tube would better represent
the process of sampling by WFT.
Figure 5—Packing material used for Short Slim Tube, glass beads of 125-250 mesh
The sight glass, common in a Slim Tube set-up, was removed to minimize volumes aside from the porous
media itself. The SST had the following properties:
A reservoir gas was created from separator samples from a well drilled with Water Based Mud (WBM).
As such, no contamination would be expected and none was detected in the original reservoir fluid.
The experimental schematic is shown below in Fig. 6. Initially, the experiment is set up per Fig. 6 (a), with
the pressure throughout the system maintained at injection conditions up to the back-pressure regulator, then
flashed to a liquids trap. This part of the experiment is representative of the WFT filtrate dumping phase,
10 SPE-186256-MS
prior to capturing sample. Once reservoir gas was coming out at the back end of the SST with minimal
liquids (indicative of increased GOR) the sampling process was commenced. At this stage we switch to
the schematic in Fig. 6 (b), where a PVT cylinder is placed at the back end of the SST. The system is
maintained at sampling pressure all the way to and including the PVT sample cylinder and the reservoir
fluid is gradually sampled.
Figure 6—Schematic set-up of Short Slim Tube for collection of contaminated samples.
This contamination free sample was created with a CGR of 25 bbl/MMscf. At 100°C we observed a
dew point of 3,170 psig. The results of compositional analysis and summarized data including dew point
measurements are presented in Table 2.
SPE-186256-MS 11
Table 2—Results from compositional analysis of clean sample and resulting samples collected at back end of SST
Base oil from a synthetic oil based mud, was used in this analysis. The composition of this base oil can
be found on Table 3, along with the fingerprint data from the flash liquids before and after mathematical
cleanup.
12 SPE-186256-MS
Sample #1
After flowing for 1.33 PV, capture of the first sample was commenced and continued until 2.69 PV. Sample
#1 was heavily contaminated, the flash condensate contained 46.8 % (by weight) OBM contamination. The
compositional data was consistent with this, with C12+ increasing from 0.40 mol% to 1.09 mol%. It is not
uncommon to obtain a sample like this in a field scenario.
Sample #2
After flowing for 4.04 PV, capture of the first sample was commenced and continued until 5.47 PV. Sample
#2 looked very good and no detectable base oil content was measured in the flash condensate. The resulting
PVT work showed strong similarities to the original reservoir fluid. However, the measured flash CGR
differed more than is desirable.
Sample #3
After flowing for 5.47 PV, capture of the first sample was commenced and continued until 6.89 PV. Sample
#3 also showed no OBM contamination in the flash condensate. However, similarly to what we observed
during the 40 foot study, the C12+ was significantly lower than that of the original sample. The measured dew
point was lower, and retrograde liquid dropout was significantly less – all consistent with less C12+ content.
The results of the PVT analysis are shown below in Fig. 7. Overall, as observed with the compositions, the
results from Sample #1 show an excess of heavy end components. Dew point has increased by approximately
300 psi.
14 SPE-186256-MS
Figure 7—Results from Constant Mass Expansion study of Clean and Captured Samples
Results from Sample #2 compare very well with that of the original reservoir fluid. The dew point was
measured approximately 2% above that of the original reservoir fluid and retrograde liquid dropout is similar
with similar maximum content.
Results from Sample #3 interestingly appear to have a significant portion of the heavy components native
to the reservoir fluid stripped out. These have likely remained on the SST column locked up by the immobile
base oil phase remaining on the column.
Of the PVT properties for the lean gas condensate system studied, CGR and dew point were most affected,
while Z-factor was less affected, however we can see that Sample #3 was most different from the original
reservoir fluid.
Mathematical Methods to Clean Up Contaminated Compositions. Both subtraction and K-value method
were employed in the cleanup of composition from Sample #1. As can be seen on Table 3, the results from
both methods compared very well to each other (almost identical results), and the cleaned up Sample #1
composition resulted in a fairly similar composition to the original sample. There are some substantial errors
between the corrected composition from Sample#1 and the original clean sample (over 30% in components
with small content to start with), but overall however, a composition of this quality would provide fairly
valuable information for a reservoir engineer in an exploration well.
The resulting CGR using flash data from the contaminated sample and correcting for cleanup differed
too much from the original sample. If we analyse the data closer, we can see that the flash condensate
composition of the contaminated sample carried less intermediate component compared to the flash of
the original sample, implying that these components were flashed off in the vapor phase rather than
condensing. So while the wellstream composition could be corrected back to the original composition, the
flash condensate appeared to still be affected by the OBM contamination even after correction.
Conclusions
• An experimental apparatus was designed to enable OBM contamination of a clean reservoir fluid
sample through a dynamic process, flowing through a porous media at reservoir conditions.
• Using this apparatus, an experimental test method was designed to obtain both uncontaminated
and OBM contaminated PVT data from the same base reservoir fluid. This enabled us to study the
effects of OBM contamination on PVT samples taken by WFT in OBM drilled wells.
• The experimental apparatus and test method were trialed with success.
SPE-186256-MS 15
• The data obtained from the experimental test method indicated that:
○ A contaminated sample could be obtained.
○ Contamination free samples can be obtained with sufficient flow.
○ The base oil may be stripping heavy end components native to the reservoir fluid in the near
wellbore region. This may be due to a condensing-vaporising drive mechanism being developed
between the reservoir gas and remnant base oil locked in the near wellbore region.
• Proposed future studies to improve the experimental test method would include:
○ Numerical modeling to match experimental data and then test an experimental forward plan.
○ Using the numerical model, perform parametric sensitivity study of:
■ The flow rate of reservoir gas passing through the SST.
■ The effect of pressure and temperature on partial miscibility of OBM and gas condensate
reservoir fluids.
■ The effect of OBM composition.
○ Apply learnings from parametric sensitivity to fine tune the experimental method.
Acknowledgement
The authors thank Petrolab Australia Pty. Ltd. for providing the laboratory resources and allowing time to
conduct this work. Also, we extend special thanks to Jan G. Bon (Sr.) and Gavin Munn for their assistance
in editing and reviewing our work.
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