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Campus UAB
Ronda de la Font del Carme s/n
E-08193 Bellaterra (Barcelona)
T +34 93 567 20 00
www.appluslaboratories.com
th
Bellaterra : 13 September 2016
Dossier number : 16/12498-1266
Petitioner Reference : BASF Coatings GmbH
Glasuritstraße 1
D-48165 Münster
GERMANY
TEST REPORT
RECEIVED MATERIAL:
On 01st June 2016, a coating for the protection and repair of concretes structures, were
received at Applus Laboratories, with the following references:
MasterSeal 7000 CR
(Primer: MasterSeal P 770 & Membrane: MasterSeal M 790)
PRODUCTS AND SYSTEMS FOR THE PROTECTION AND REPAIR OF CONCRETE STRUCTURES.
Definitions, requirements, quality control and evaluation of conformity. UNE-EN 1504-2:2005 Part
2: Surface protection systems for concrete.
1- Measurement of bond strength by pull-off , UNE-EN 1542:1999
2- Determination of water-vapour transmission properties, UNE-EN ISO 7783:2012
3- Determination of liquid water permeability, UNE-EN 1062-3:2008
4- Determination of carbon dioxide permeability, UNE-EN 1062-6:2003
5- Adhesion after thermal compatibility, UNE-EN 13687-1:2002 and UNE-EN 13687-2:2002
6- Abrasion resitance (Taber), UNE-EN ISO 5470-1:1999
7- Falling-weight test, UNE-EN ISO 6272-1:2012
8- Determination of crack bridging properties, UNE-EN 1062-7:2004 Method A - C.2 and Method
B - B.3.2
9- Depth of penetration of water under pressure according to basic principles of
UNE-EN 12390-8:2009
10- Determination of resistance to severe chemical attack, UNE-EN 13529:2005
RESULTS:
The reference samples, are 300 x 300 x 100 mm specimen, with a maximum aggregate size of 8
mm or 10 mm and prepared with agrit-blasted surface, according to EN 1766 (MC 0,40).
The specimens were preserved in the laboratory covered with a plastic film for 72 hours and
after that, they were conserved 21ºC - 60% RH for 25 days.
Tensile strength
Specimen
( N/mm² )
1 2,82 (A)
2 3,02 (A)
3 2,84 (A)
4 3,06 (A)
5 2,96 (A)
Average 2,9 MPa
NOTE: between brackets the failure pattern.
A: Cohesion failure in the concrete substrate
A/B: Adhesion failure between the substrate and product
B: Cohesion failure
Final results:
Water-vapour Diffusion- Water vapour
Water-vapour
Specimen transmission Equivalent air resistance
flow rate
no. rate V layer thickness factor
G (g/h) 2
(g/m * day) Sd (m) µ
1 0,00005 0,15 132 69525
2 0,00006 0,18 112 53294
3 0,00005 0,15 134 71436
Mean 0,0001 0,16 126 64752
W
Specimen
(Kg/m2 h0,5 )
1 0,0004
2 0,0005
3 0,0004
Average 0,0005
Requirements according to
UNE-EN 1504-2:2005 Table 5
Weight loss < 3000 mg
Height from which the first cracks are produced > 2500 mm*
*
From this height NO cracks are produced
The reference samples are specimens of dimensions 160x40x40 mm, manufactured according
UNE-EN 1062-7, C.3.2 section.
Conditioning Method before test: 7 days at 70ºC according to EN 1062-11 4.1
The obtained results after conditioning method are as follows:
After the artificial weathering, there were no observed changes in appearance
such as chalking, blistering, peeling or flaking following the methods described in
to EN ISO 4628-2, EN ISO 4628-4 and EN ISO 4628-5
Dossier no. 16/12498-1266 Page 8
MasterSeal 7000 CR
BASF Coatings GmbH (Primer: MasterSeal P 770 & Membrane:
MasterSeal M 790)
Final results:
- Test description
The tests were developed according to the applicable sections of the UNE-EN 1062-7:2004. The
dynamic tensile test 1 (section C.3) for a class B (ANNEX B) of the UNE-EN 1062-7:2004 has
been performed.
Prior to the test, an instant crack is created at the midpoint of the notch, with a crack width of
less than 100μm.
Given below the measure of the resistance to cracking of the coating is shown, according to
method B section 8 of the reference standard.
The test is developed with a crack width control by a COD extensometer.
The test consist of periodically change the width of the crack at the defined test temperature.
The curve is defined by the frequency f, the width w/2 and the average width of the crack. For B
3.2 class test parameters are shown in the table 2 and figure 1.
Figure 1. Modification of the crack width versus time for B 3.1 class.
Dossier no. 16/12498-1266 Page 9
MasterSeal 7000 CR
BASF Coatings GmbH (Primer: MasterSeal P 770 & Membrane:
MasterSeal M 790)
- Results
- Sample 1: After 1.000 cycles any crack or damage appear in the waterproofing layer surface
- Sample 2: After 1.000 cycles any crack or damage appear in the waterproofing layer surface
- Sample 3: After 1.000 cycles any crack or damage appear in the waterproofing layer surface
The concrete produced have a average compressive strength of 25 MPa and medium-high
3 3
porosity of 18%, density 2.25 g/cm , containing 300 kg/m cement without additives.
The concrete specimens have a thickness of 15 cm aprox. It is tested under direct pressure
with the penetration front on the water-proof product.
Finally, the water penetration in the specimens is assessed.
2
- Penetration depth at 5 Kg/cm of pressure for 3 days:
1 2 3
Specimen
0 0 0
Dossier no. 16/12498-1266 Page 10
MasterSeal 7000 CR
BASF Coatings GmbH (Primer: MasterSeal P 770 & Membrane:
MasterSeal M 790)
10- Determination of resistance to severe chemical attack, UNE-EN 13529:2005
9a. Organic acids (except formic acid) and their salts (in aqueous 50,0 Vol.-% acetic acic
solution) 50,0 Vol.-% propionic acid
10. Inorganic acids up to 20 % and acidic hydrolysing salts in
aqueous solution (pH < 6) except hydrofluoric acid and oxidizing sulfuric acid (20 %)
acids and their salts
11. Inorganic bases and their alkaline hydrolysing salts in
aqueous solution (pH > 8) except solutions of ammonium and sodium hydroxide (20 %)
oxidizing solutions of salts (e. g. hypochloride)
12. Solutions of inorganic non-oxidizing salts showing a pH = 6 – aqueous solution of sodium chloride
8 (20 %)
35,0 Vol.-% triethanolamine
13. Amines and their salts (in aqueous solution) 30,0 Vol.-% n-butylamine
35,0 Vol.-% N, N-dimethylaniline
After 5 days in contact with chemicals reagents Groups 4a, 6a, 9, 9a, 13 and 15 have not
noticed any flaws in the test conducted (blistering, flaking, cracking, or loss of colour etc.).
Groups 6a, 9a, 13 and 15: Blisters, cracking and flaking have appeared and the surface has
been destroyed.
Group 4a, 9: Change of colour of surface
5 5 5 13 19 24
5 6 5 12
After 5 days in contact with chemicals reagents Groups 4a, 6a, 9, 9a, 13 and 15 have not
noticed any flaws in the test conducted (blistering, flaking, cracking, or loss of colour etc.).
Groups 6a, 9a, 13 and 15: Blisters, cracking and flaking have appeared and the surface has
been destroyed.
Group 4a, 9: Change of colour of surface
11 13 10 19