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Materials and Design 56 (2014) 84–90

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Materials and Design


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Technical Report

Mechanical, fatigue and microstructural properties of friction stir welded


5083-H111 and 6082-T651 aluminum alloys
Beytullah Gungor a,b, Erdinc Kaluc b,c, Emel Taban b,c,⇑, Aydin Sik d
a
TR Naval Forces, Kocaeli, Turkey
b
Kocaeli University, Faculty of Engineering, Department of Mechanical Engineering, Kocaeli, Turkey
c
Kocaeli University, Welding Technology Research, Education and Training Center, Kocaeli, Turkey
d
Gazi University, Faculty of Architecture, Department of Industrial Design, Ankara, Turkey

a r t i c l e i n f o a b s t r a c t

Article history: In this study, 5083-H111 and 6082-T651 aluminum alloy plates in 6 mm thickness that are used
Received 19 August 2013 particularly for shipbuilding industry were welded using Friction Stir Welding (FSW) method as similar
Accepted 31 October 2013 and dissimilar joints with one side pass at PA position with the parameters of 1250 rpm tool rotation,
Available online 9 November 2013
64 mm/min welding speed and 2° tool tilt angle. Tensile tests results showed sufficient joint efficiencies
and surprisingly high yield stress values. Bending fatigue test results of all joint types showed fatigue
strength close to each other. Fatigue strength order of the joints were respectively FSWed 5083-5083,
and 6082-6082 similar joints and 5083-6082 dissimilar joint. Cross sections of the weld zones have been
analyzed with light optical microscopy (LOM) and fracture surface of fatigue test specimens were
examined by scanning electron microscopy (SEM). Although there were no voids in radiographic and
microscopic analyzes, 5083-6082 joint showed rarely encountered voiding effect under fatigue load.
Microhardness measurements revealed rare result for FSWed AW5083 and novel result for FSWed
6082 aluminum alloy.
Ó 2013 Elsevier Ltd. All rights reserved.

1. Introduction 5454 as sheet and plate (along with 6082 extruded shapes) with
all-welded construction [1–3].
Aluminum and aluminum alloys have become increasingly used Aluminum welding was once considered limited due to the
in production of automobiles and trucks, packaging of food and problems associated with welding processes such as oxide removal
beverages, construction of buildings, transmission of electricity, and reduced strength in the weld and heat affected zone (HAZ).
development of transportation infrastructures, production of New aluminum welding techniques have been developed and
defense and aerospace equipment, manufacture of machinery commercialized in significantly over the past 30 years that solves
and tools and marine structures with its unique properties such these welding problems [1,3]. Although Metal Inert Gas (MIG)
as corrosion resistance, thermal conductivity, electrical conductiv- and Tungsten Inert Gas (TIG) welding processes were developed
ity, high strength with low density, fracture toughness and energy in 1940s and used in many industries, there were still some joint
absorption capacity, cryogenic toughness, workability, ease of problems that reduced joint efficiency under % 50 [1,4–6]. To
joining (welding (both solid state and fusion), brazing, soldering, improve weld performance, Friction Stir Welding (FSW) – a solid
riveting, bolting) and recyclability. 5083 aluminum–magnesium state welding process – and a milestone in aluminum welding
alloys are strain hardenable and have excellent corrosion resis- was developed in 1991 by The Welding Institute (TWI). FSW
tance, toughness, weldability and moderate strength. 6082 alumi- disregarded most of the welding problems such as oxide removal,
num–magnesium–silicon alloys are heat treatable and have high distortion and porosity associated with conventional arc welding
corrosion resistance, excellent extrudibility and moderate processes without reaching melting temperature or change of
strength. Especially with their high corrosion resistance and mod- phases in the base material. FSW also made all aluminum alloys
erate strength, these alloys are widely used in shipbuilding indus- weldable that were once considered unweldable or limitedly weld-
try both separately and together. Single- or multiple-hull high able. Further, the reduced welding temperature made joints with
speed ferries employ several aluminum alloys, 5083, 5383 and lower distortions and residual stresses, enabling improved fatigue
performance, new construction techniques, and making possible
the welding of very thin and very thick materials. Even though
⇑ Corresponding author at: Kocaeli University, Faculty of Engineering, Depart-
FSW produced joints that were metallurgically, environmentally
ment of Mechanical Engineering and at Welding Technology Research, Education
and Training Center, Kocaeli, Turkey. Tel./fax: +90 262 303 34 43. and economically better than other welding processes, owing to
E-mail addresses: emel.taban@yahoo.com, emelt@kocaeli.edu.tr (E. Taban). the typically high forces in the process, FSW was usually practiced

0261-3069/$ - see front matter Ó 2013 Elsevier Ltd. All rights reserved.
http://dx.doi.org/10.1016/j.matdes.2013.10.090
B. Gungor et al. / Materials and Design 56 (2014) 84–90 85

as a fully mechanized process, increasing the cost of the equipment evaluated the microstructure and fatigue properties of dissimilar
compared to arc welding techniques, while reducing the degree of AA7075/AA6061 joints produced by friction stir welding by using
operator skill required. [7–10]. In spite of all of its benefits and two different pin profiles with two rotational speeds and three
studies that has showed better performance than fusion weldings, welding speeds. From the results of microstructure analyses and
FSW has not been still widely commercialized around world, ow- mechanical test, it was clear that welding properties, such as the
ing to lack of industry standards and specifications, design guide- microstructure and fatigue life, were strongly influenced by tra-
lines and design allowables, informed workforce and high cost of verse speed and tool profile. Sarsılmaz et al. found that best fatigue
capital equipment and licensing [8,10]. performance was provided with application of treated cylindrical
FSW produces welds by using a rotating, nonconsumable weld- pin profile, 1120 rpm tool rotational speed and 250 mm/min [17].
ing tool to locally soften a workpiece, through heat produced by Ericsson and Sandström studied influence of welding speed on
friction and plastic work, thereby allowing the tool to ‘‘stir’’ the the fatigue of friction stir welds, and comparison with MIG and
joint surfaces. The tool serves three primary functions, that is, TIG welded joints. According to the results, welding speed in the
heating of the workpiece, movement of material to produce the tested range, representing low and high commercial welding
joint, and containment of the hot metal beneath the tool shoulder speed, had no major influence on the mechanical and fatigue prop-
[8–10]. erties of the FS welds while FS welds showed better fatigue perfor-
As of its invention, FSW process has been found very interesting mance then MIG and TIG [18]. Lombard et al. used 11 different
and widely studied [10]. Many studies have been carried out to values of combination of tool rotational speed, feed and pitch val-
understand and analyze the effect of process parameters and tool ues for optimizing FSW process parameters to minimize defects
geometries on microstructural and mechanical properties and and maximize fatigue life in 5083-H321 aluminum alloy. Their
formability of joints. Taban and Kaluc successfully welded study has demonstrated that rotational speed governs defect
6.45 mm thick 5086-H32 aluminum alloy with TIG, MIG and FSW occurrence in this 5083-H321 aluminum alloy and that there was
processes, and their results has demonstrated that the tensile a strong correlation between frictional power input, tensile
properties of FSW joints were more satisfactory than fusion welded strength and low cycle fatigue life [19].
joints [6]. Adamowski and Szkodo investigated effect of process Although there were many achievements in FSW of aluminum
parameters on the properties and microstructural changes in Fric- alloys and both 5083-H111 and 6082-T651 aluminum alloys were
tion Stir Welds in the aluminum alloy 6082-T6 with 22 different studied widely as similar alloy FSWed joints, there were not en-
parameters and found that FSW welds is directly proportional to ough studies about these aluminum alloys as dissimilar alloy
the tool rotation and welding speeds [11]. Cavaliere et al. studied joints. In contradiction to their wide usage in industry, especially
effect of varying welding speeds on mechanical and microstruc- in shipbuilding industry, there was not enough knowledge about
tural properties of FSWed AA6082-T6 aluminum alloy. Cavaliere these alloys as dissimilar welds. We aimed to contribute to knowl-
et al. welded 4 mm thick plates with 1600 rpm tool rotation and edge of friction stir welding of 5083-H111 and 6082-T651 as sim-
welding speed varying 40–460 mm/min. Cavaliere et al. found that ilar alloy joints and fulfill the deficiency of knowledge about these
welding speed had a threshold points for grain structure, yield alloys as dissimilar FSWed joints. Also, we used different parame-
stress and ductility that reversed these properties behavior to the ters from previous studies to vary knowledge about both similar
opposite side [12]. Palanivel et al. studied effect of tool rotational and dissimilar alloy joints of FSWed 5083-H111 and 6082-T651
speed and pin profile on microstructure and tensile strength of dis- especially in low welding speed.
similar friction stir welded AA5083-H111 and AA6351-T6 alumi-
num alloys. Palanivel et al. used pin profiles of straight square,
straight hexagon, straight octagon, tapered square, and tapered 2. Materials and experimental procedure
octagon and three different tool rotational speeds and found that
straight square pin profile with 950 rpm tool rotational speed In this study, 5083-H111 and 6082-T651 aluminum alloys were
yielded highest strength [13]. Moreira et al. studied to characterize used as base metals. Chemical composition data obtained by glow
mechanical and metallurgical properties of friction stir welded discharge optical emission spectroscopy (GDOES) and mechanical
butt joints of aluminum alloy 6061-T6 with 6082-T6. For compar- properties obtained by tensile test are given in Table 1.
ison, similar and dissimilar material joints made from each one of Aluminum alloy plates were cut into coupons according to TS
the two alloys were micro structurally examined, and micro hard- EN ISO 15614-2 [20] for I- butt welding. H13 tool steel with chem-
ness, tensile and bending tests were carried out. Moreira et al. ical composition of % 0.406 C, % 1.096 Si, % 0.443 Mn, % 4.952 Cr, %
found that AA 6082-T6 aluminum alloy revealed lower yield and 1.251 Mo, % 0.813 V, hardness of HRC48 and the dimensions shown
ultimate stress as well as lowest hardness values [14]. Rajakumar in Fig. 1 was used as FSW tool. Welding parameters were 1250 rpm
et al. used 5 different values for each of tool rotational speed, weld- tool rotational speed (counter clockwise), 64 mm/min welding
ing speed, axial force, shoulder diameter, pin diameter and tool speed and 2° tool tilt angle. Similar joints of 5083–5083 (called
hardness parameters of FSW to understand influence of FSW as F55) and 6082-6082 (called as F56) and dissimilar joints of
process and tool parameters on strength properties of AA7075-T6 5083–6082 (called as F66) aluminum alloys were fabricated with
aluminum alloy joints. Rajakumar et al. found that optimum these parameters.
parameters for providing maximum strength properties of Visual and radiographical examination was performed in order
315 MPa yield strength, 373 MPa of tensile strength, 397 MPa of to detect possible surface and inner errors after welding test sam-
notch tensile strength, 203 HV of hardness and 77% of joint effi- ples in accordance with TS EN ISO 17637 [21] for visual examina-
ciency were 1400 rpm (tool rotational speed), 60 mm/min (weld- tion before further destructive tests. According to test plan, test
ing speed), 8 kN (axial force), with the tool parameters of 15 mm samples suitable for TS EN ISO 15614-1:2004 + A2:2012 [22] were
(shoulder diameter), 5 mm (pin diameter), 45 HRC (tool hardness) extracted from weld plates which had past visual and radiograph-
[15]. Kulekci_ et al. studied effects of tool rotation and pin diameter ical examination. Tensile test specimens were prepared according
on fatigue properties of friction stir welded lap joints of AA5754 to TS EN ISO 4136:2012 [23], bending test specimens were pre-
aluminum alloy. Test results showed that increasing one value pared according to TS EN ISO 5173 [24], fatigue test specimens
while fixing other resulted worse fatigue strengths. Kulekci_ et al. were prepared according to DIN 50142 [25]. In order to determine
found that optimization of tool rotation and pin diameter were re- microstructure properties of these joints, the specimens were
quired to have better fatigue performance [16]. Sarsılmaz et al. cross-sectioned perpendicular to the weld interface using a
86 B. Gungor et al. / Materials and Design 56 (2014) 84–90

Table 1
Chemical composition and mechanical properties of base metals.

Aluminum alloy Chemical composition (in wt.%) (data obtained by GDOES).


Si Fe Cu Mn Mg Cr Ni Zn Ti Al
5083 0.076 0.13 0.032 0.63 4.34 0.064 0.003 0.035 0.055 94.6
6082 1.02 0.23 0.052 0.63 0.69 0.066 0.002 0.033 0.048 97.2
Mechanical properties
(Rp0.2), MPa (Rm), MPa Elongation %
5083 239 331 16.4
6082 321 329 11.1

of fatigue test specimens were analyzed with scanning electron


microscopy (SEM).

3. Results and discussion

3.1. Nondestructive testing

As a result of visual inspection on welded plates, surface type


errors such as too much flash, galling, and lack of penetration have
not been seen. Any wormhole, kissing bond, porosity, inclusion or
oxide layer has not been detected by radiography. Second phase
particles and oxides alignment under shoulder were inspected by
LOM and none of them were detected in weld zone [10]. Thickness
reductions were measured in 0.05 mm level in zone under tool
shoulder. When welding tool arrived at the end of the joints, it
was allowed to run out the end of the workpiece, producing a tear
out. These tear outs was trimmed away by sawing before further
destructive tests (Fig. 2).

3.2. Microstructural behavior

The micro structural behavior of aluminum alloys joined by


FSW was studied by employing LOM. Images of weld zones’ cross
section are outlined in Fig. 3.
Although formation of onion ring has been evaluated character-
istic in FSWed nugget zone [26], it might not always be seen
apparently in the weld macrostructure [8,14,15,27]. Onion ring
formation has not been seen in F55 joint weld nugget while clearly
Fig. 1. FSW Tool geometry (conically threaded).
seen in F56 and F66 nugget zone. In the weld nuggets of all joints,
grains have been refined as a result of dynamic recrystallization
low-speed saw. The cross-section of these joints was metallo- (continuous dynamic recrystallization (CDRX) [8,26]. The strain-
graphically polished and Keller etchant was used for LOM exami- hardened 5083 base material was likely completely recrystallized
nation. After microstructural examinations, these specimens were in TMAZ close to the nugget of F55, and the fraction of recrystal-
used for detailed microhardness assessment under 200 g (HV0,2) lized material decreased to zero as the distance from weld nugget
load. For further examination of microstructure, fractured surface increased. Pancake grains in TMAZ of F66 were deformed,

Fig. 2. General views of FSWed joints: F55, F56, F66).


B. Gungor et al. / Materials and Design 56 (2014) 84–90 87

Fig. 3. LOM images of weld zones’ cross section.

elongated and rotated due to the strain that they were subjected to Fractured surfaces were analyzed by LOM and SEM. All fractions
[11]. Heterogeneous mixing of recrystallized fine grains of 5083 of all joint types have been started from between flow arm and
and pancake grains of 6082 had been clearly seen in F56 nugget weld nugget in advancing sides. In F55 fracture surface appeared
zone. populated of very fine dimples revealing a very ductile behavior

Fig. 4. Macrograph of fractured surface of F55 fatigue specimen and SEM images of this fracture surface.
88 B. Gungor et al. / Materials and Design 56 (2014) 84–90

F56 joints were analyzed in accordance with cross section of its


weld zone (Fig. 5). Although there was no weld defect like second
phase particles, oxides alignment or voids detected by microscopy
or radiography, fractured surfaces of F56 at the intersection point
of flow arm, TMAZ and weld nugget. Three distinct regions were
separated under loading as if they were bonded, not welded. These
rarely encountered voids at the intersection point of flow arm,
TMAZ and weld nugget. Three distinct regions were separated un-
der loading as if they were bonded, not welded. These rarely
encountered voids aroused from a fluid dynamics voiding effect,
either associated with the singularities, or possibly due to vortex
generation behind the tool probe while fabricating the joint
[11,28].

3.3. Microhardness

Microhardness data were obtained with 200 g load (Fig. 7).


5083 similar alloy weld joint’s (F55) microhardness were mea-
sured between 80–84 HV0,2 and almost there were no drops in
microhardness values. 6082 similar alloy weld joint’s (F66)
microhardness were measured between 67–85 HV0,2, hardnesses
in weld zone were measured around 82 HV0,2, while hardness de-
crease in thermo mechanically affected zone (TMAZ) were mea-
sured 67.9 HV0,2. 5083 and 6082 dissimilar alloy weld joint’s
(F56) were measured between 62.6–84 HV0,2. TMAZ’s of F56 joint
were slightly similar to that of F66 and F55 for same material as
seen in Fig. 7.
Microhardness results of F55 joint were best of all joints as ex-
pected but hardness traverse across weldments differ from some
studies [1,29]. Average hardness values were 84 HV0,2 for weld
nugget and 81 HV0,2 for TMAZ. Hardness increase was approxi-
mately % 4. Although hardness increase in FSWed aluminum alloys
Fig. 5. Cross view of F56 weld zone (a), Macrograph of fractured surface of F56 were rare, Mishra and Mahoney referred a study showing a slight
fatigue specimen (b) and SEM images of this fractured surface (c–e).
increase in hardness across the weld nugget compared to the TMAZ
for a slightly (less than 6%) hardened 5083-H112 as a result of the
of the material before failure, and fatigue striations were clearly very fine grain size created by FSW [8]. Koilraj et al. also found
seen in SEM images (Fig. 4) [12]. Fracture surface of F66 joints same hardness traverse for 5083 side of dissimilar joint [30]. Sur-
showed coarse dimples in SEM images (Fig. 6) [15]. Fracture of prisingly, microhardness drop had not been seen in weld zone in

Fig. 6. Macrograph of fractured surface of F66 fatigue specimen and SEM images of this fractured surface.
B. Gungor et al. / Materials and Design 56 (2014) 84–90 89

Micro hardness drops in precipitation hardened AW 6082 in far


TMAZ of F56 and F66 were results of overaged zone where precip-
itate coarsening has taken place [3].

3.4. Tensile properties

Tensile properties for base material and cross-welds were given


in Table 2 and comparison of the properties are provided in Fig. 8.
Average yield and tensile strengths were 198.5 and 285 N/mm2 for
F55, respectively, for F56 193 and 212 N/mm2, and for F66 189.9
and 203 N/mm2. Tensile test results for F55 joints were above val-
ues results has been obtained from previous studies [29], and at
the same level for F56 and F66 [11–13,18,31]. Weld performance
of welded joints were % 86 for F55, % 65 for F56 and % 62 for F66
according to average maximum strength of base metal 5083 and
Fig. 7. Microhardness values for FSWed Joints.
6082. Failures of F55 tensile test specimens were in the weld me-
tal. This was due to the recrystalization process accounted for
majority strength loss in weldments in strain-hardened aluminum
F66 joint. Microhardness traverse of F66 joint was novel result for
alloys with its annealing effect [1]. In contradiction to F55 joint,
FSWed 6082 T651. Ericsson and Sandstrom had similar hardness
other welded joint tensile test specimens were fractured normally
values for both for high and low speed welding of AW6082 after
in TMAZ of AW 6082 parent material side. While welding of 6082
post-weld aging [18]. Mishra and Mahoney came up with similar
alloy, in far TMAZ micro hardness drops in overaged zone where
hardness pattern for FSWed and artificially aged AW6082 alumi-
precipitate coarsening has been taken place as also mentioned
num alloy [8]. It was concluded that increasing heat input depend-
above in microhardness evaluation. These overaged zones were
ing on low travel speed with high tool rotational speed resulted
weakest zones of welded 6082 TMAZ [1,3]. Finally, yield stress re-
naturally aging of weld zone with fine dispersion of precipitates
sults of all welded joints were surprisingly high from previous
within the grains since these tests were conducted a few weeks
studies for all joints type [8,18,29–33].
after production [3]. F56 joint’s micro hardness traverse were sim-
ilar to that of previous studies [1,14]. Both F56 and F66 joints’
hardnesses dropped in far TMAZ of AW6082 aluminum alloy. 3.5. Fatigue behavior

Fatigue test results for welded joints and base material were
given in Fig. 9. Fatigue test were conducted under yield stresses.

Fig. 8. Comparison of average tensile properties of the base metal with welded
joints. Fig. 9. Fatigue test results for welded joints.

Table 2
Tensile test results of welded joints.

Tensile specimen Rp 0.2 (N/mm2) Rm (N/mm2) Elongation (%) Rupture zone


F55_1 191 281 14 Weld metal
F55_2 – 284 14 Weld metal
F55_3 206 290 14 Weld metal
F55 average 198.5 285 14
F56_1 – 211 5.6 TMAZ (AW 6082 side)
F56_2 193 214 5.6 TMAZ (AW 6082 side)
F56_3 – 211 5.6 Weld metal
F56 average 193 212 5.6
F66_1 – 204 8 Weld metal
F66_2 – 211 8.4 TMAZ
F66_3 189.9 194 7.6 TMAZ
F66 average 189.9 203 8
90 B. Gungor et al. / Materials and Design 56 (2014) 84–90

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