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MVC-QF-TECH-008(19) QUALITY CONTROL DAILY ANALYSIS REPORT

Effectivity Date: February 15, 2011 MABUHAY VINYL CORPORATION


Date : 09//11 Time : 1130 AM [ ] IEM 1 [ ] IEM 2 [ ] MSG [ ] QC file
IEM 1 IEM 2
50 % CAUSTIC SODA 50 % CAUSTIC SODA Specs
Online Tk – A Online Tk - 9
% NaOH 48-50
32 % CAUSTIC SODA 32 % CAUSTIC SODA
Online Tk- Online Tk - 8
% NaOH 30-32
HYDROCHLORIC ACID HYDROCHLORIC ACID
Online Tk- Tk- Online CTB 2
% HCl NA 32-33.5
Color # 3, max
POLISHED BRINE(After Precoat) POLISHED BRINE(After Precoat)
Ca+Mg, ppm + NA = + NA = 5 ppm, max.
SPB (After Headtank) SPB (After Headtank)
Ca+Mg, ppb nil + nil = nil nil + nil = nil 20 ppb, max.
NaCl, gpl NA NA 290 gpl,min.
Na2SO4,gpl NA NA 7 gpl, max.
NaClO3,gpl NA NA 20 gpl,max.
DEPLETED BRINE DEPLETED BRINE
NaCl, gpl 200 gpl, min.
Free Cl2 negative positive Negative
NaClO3,gpl NA NA 27 gpl, max.

SODIUM HYPOCHLORITE PLANT


Tank No.
% NaOCl 7.40, min
% NaOH 0.40-1.0
Sp. Gr. 1.108, min

LIQUID CHLORINE PLANT UTILITIES


LIQUID CHLORINE SULFURIC ACID INSTRUMENT AIR @ AM
Source % Cl2 Specs Source % H2SO4 Specs Dew Point, °C ≤3.8 °C
LCP Tk.# NA 99.5 %,min BOILER WATER
LCP Comp NA 97 %, min.
Cl2 Feed 91.0 %,min. SiO2, ppm NA 150 ppm, max

GAS ANALYSIS
IEM 1 IEM 2 FLUE GAS
% Cl2 % H2 O2 + CO2 % Cl2 % H2 O2 + CO2 % CO % CO2 % O2
Line A NA NA NA
Line B

POLLUTION C O N T R O L - EFFLUENTS
pH OIL Hg TDS TSS Color COD
Source 6AM 7PM (+ or -) ppb ppm mg/L Pt-Co Units mg/L
S-2 -
S-5 NA -
Lagoon NA
Sludge Pond NA

Source pH gpl NaOH Source pH SPECIFICATIONS


JBC NA S-3 NA pH = 6-9 COD = 150 mg/li, max Hg = 2, ppb, max.
Evap Canal S-4 Oil = Negative TDS = 1000 ppm, max TSS = 150 mg/li, max
Total Canal S-7 Color = 200 Pt-Co units, max.

Remarks: IEM 1 : None Analyzed by Certified Correct


OFF-SPECS IEM 2 : Depleted brine - Free Cl2
Others : Instrument air - dewpoint NEY/ANB/RGD OVA
MVC-QF-TECH-004 (12)
Effectivity Date: May 20, 2010

MABUHAY VINYL CORPORATION PRODUCT TRANSFER CLEARANCE


Assumption Heights, Iligan City

Date : 09//11 [ ] IEM 1 [ ] IEM 2 [ ] Mktg [ ] QC file


IEM 1
HYDROCHLORIC ACID LIQUID CAUSTIC SODA SODIUM HYPOCHLORITE
Tk # % HCl SG @ 30”C Color Tk # 50% 32%. Tk # % NaOCl % NaOH SG @ 30”C
1 NA A NA NA 1 NA
2 NA B NA NA 2 NA
3 NA 3 NA
4 NA 4 NA
5 NA 5 NA
IEM 2 SPECIFICATIONS
HYDROCHLORIC ACID LIQUID CAUSTIC SODA HYDROCHLORIC ACID
Tk # % HCl SG @ 30”C Color Tk # 50% 32%. % HCl 32.0 - 33.5
CTA 1 NA 9 NA - SG @ 30”C, min 1.152
CTA 2 NA 8 - NA Color, max #3
CTA 3 NA LIQUID CAUSTIC SODA
CTB 1 NA 50% 32%
CTB 2 NA % NaOH 48 - 50 30 - 32
Remarks: % NaCl 0.10 0.10
WITHIN SPECS, OK for transfer ppm Fe, max 10 10
SODIUM HYPOCHLORITE
Analyzed by Certified Correct % NaOCl, min 7.40
% excess NaOH 0.40 - 1.00
RGD OVA SG @ 30”C, min 1.109
MVC-QF-TECH-008(24) QUALITY CONTROL DAILY ANALYSIS REPORT
Effectivity Date: October 1, 2016 MABUHAY VINYL CORPORATION
Date : 03/29/17 Time : 11:30 AM [ ]QC [ ]Technical [ ]IEM1/IEM2 [ ]AVP-Mfg
IEM 1 IEM 2
50 % CAUSTIC SODA 50 % CAUSTIC SODA Specs
Online Tk – A Tk - B Online Tk - 9
% NaOH 49.98 49.92 NA 49.59 NA 48.00-50.00
32 % CAUSTIC SODA 32 % CAUSTIC SODA
Online Tk – A Tk - B Online Tk - 8
% NaOH 30.45 NA NA 31.13 30.98 30.00-32.00
HYDROCHLORIC ACID HYDROCHLORIC ACID
Online Tk- Tk- Online CTB 1
% HCl SD 33.01 32.54 32.00-33.50
Color 1 1 # 3, max
POLISHED BRINE(After Precoat) POLISHED BRINE(After Precoat)
Ca+Mg, ppm + NA = + NA = 5.0 ppm,max.
SPB (After Headtank) SPB (After Headtank)
Ca+Mg, ppb 12 + 2 = 14 8 + nil = 8 20 ppb, max.
NaCl, gpl NA NA 290 gpl,min.
Na2SO4,gpl NA NA 7 gpl, max.
NaClO3,gpl NA NA 20 gpl,max.
DEPLETED BRINE DEPLETED BRINE
NaCl, gpl 196 226 200 gpl, min.
Free Cl2 negative negative Negative
NaClO3,gpl NA NA 20 gpl, max.
pH NA NA 2.0, max
S O D I U M H Y P O C H L O R I T E PLANT
Tank No. 1 2 3 6 7
% NaOCl NA NA NA 7.77 NA 7.40-8.00
% NaOH 0.82 0.40-1.00
Sp. Gravity 1.134 1.108, min
LI Q U I D C H LO R I N E PLAN T
Specs
Source LCP Tk.# Cl2 Feed LCP Tk # Cl2 Feed SULFURIC ACID
% Cl2 NA NA 99.5% min 91.0% min Source % H2SO4 Specs
% H2 NA NA NA NA LCP Comp. NA 97.0% min
UTILITIES
INSTRUMENT AIR @ AM Specs BOILER WATER Specs
Dew Point, °C ≤3.8 °C SiO2, ppm NA 150 ppm, max.
GAS ANALYSIS
IEM 1 IEM 2 FLUE GAS
% Cl2 % H2 O2 + CO2 % Cl2 % H2 O2 + CO2 % CO % CO2 % O2
Line A NA NA NA
Line B
POLLUTION C O N T R O L - EFFLUENTS
pH OIL Hg TDS TSS Color COD
Source 6AM 7PM (+ or -) ppb ppm mg/L Pt-Co Units mg/L
S-2 8.66 8.58 - NA NA NA NA NA
S-5 8.66 - NA NA NA NA NA
S-8 6.52 - NA NA 38 152 nil
S-9 8.21 - NA NA 1 16 nil
Lagoon NA NA NA NA NA NA NA
Source pH gpl NaOH Source pH SPECIFICATIONS
JBC NA S-3 NA pH = 6-9 COD = 100 mg/li, max Hg = 4 ppb, max.
Evap Canal S-4 Oil = Negative TDS = 1000 ppm, max TSS = 100 mg/li, max
Total Canal S-7 Color = 150 Pt-Co units, max.

Remarks: IEM 1 : Depleted brine - NaCl Analyzed by Certified Correct


OFF-SPECS IEM 2 : None (Original copy signed) (Original copy signed)

Others : None AND/RGD OVA


MVC-QF-TECH-004 (13)
Effectivity Date: August 5, 2014

MABUHAY VINYL CORPORATION PRODUCT TRANSFER CLEARANCE


Assumption Heights, Iligan City

Date : 03/29/17 [ ] IEM 1 [ ] IEM 2 [ ] Mktg [ ] QC file


IEM 1
HYDROCHLORIC ACID LIQUID CAUSTIC SODA SODIUM HYPOCHLORITE
Tk # % HCl SG @ 30”C Color Tk # 50% 32%. Tk # % NaOCl % NaOH SG @ 30”C
1 NA A 49.92 NA 1 NA
2 NA B NA NA 2 NA
3 NA 3 NA
4 NA 6 7.77 0.82 1.134
5 NA 7 NA
IEM 2 SPECIFICATIONS
HYDROCHLORIC ACID LIQUID CAUSTIC SODA HYDROCHLORIC ACID
Tk # % HCl SG @ 30”C Color Tk # 50% 32%. % HCl 32.00 - 33.50
CTA 1 NA 9 NA - SG @ 30”C, min 1.152
CTA 2 NA 8 - 30.98 Color, max #3
CTA 3 NA LIQUID CAUSTIC SODA
CTB 1 32.54 1.156 1 50% 32%
CTB 2 NA % NaOH 48.0-50.0 30.0 - 32.0
Remarks: % NaCl 0.10 0.10
WITHIN SPECS, OK for transfer ppm Fe, max 10 10
SODIUM HYPOCHLORITE
Analyzed by Certified Correct % NaOCl 7.40 - 8.00
(Original copy signed) (Original copy signed)
% excess NaOH 0.40 - 1.00
RGD OVA SG @ 30”C, min 1.108
ANB
MVC-QF-TECH-008(24) QUALITY CONTROL DAILY ANALYSIS REPORT
Effectivity Date: October 1, 2016 MABUHAY VINYL CORPORATION
Date : 03/30/17 Time : 11:30 AM [ ]QC [ ]Technical [ ]IEM1/IEM2 [ ]AVP-Mfg
IEM 1 IEM 2
50 % CAUSTIC SODA 50 % CAUSTIC SODA Specs
Online Tk – A Tk - B Online Tk - 9
% NaOH 49.73 NA NA SD NA 48.00-50.00
32 % CAUSTIC SODA 32 % CAUSTIC SODA
Online Tk – A Tk - B Online Tk - 8
% NaOH 31.15 NA NA 31.72 30.79 30.00-32.00
HYDROCHLORIC ACID HYDROCHLORIC ACID
Online Tk- Tk- Online CTB 2
% HCl SD 33.07 32.96 32.00-33.50
Color 1 1 # 3, max
POLISHED BRINE(After Precoat) POLISHED BRINE(After Precoat)
Ca+Mg, ppm 3.56 + nil = 3.56 5.34 + nil = 5.34 5.0 ppm,max.
SPB (After Headtank) SPB (After Headtank)
Ca+Mg, ppb 32 + 2 = 34 4 + nil = 4 20 ppb, max.
NaCl, gpl 291 317 290 gpl,min.
Na2SO4,gpl 2.96 4.74 7 gpl, max.
NaClO3,gpl 5.96 25.76 20 gpl,max.
DEPLETED BRINE DEPLETED BRINE
NaCl, gpl 197 227 200 gpl, min.
Free Cl2 negative negative Negative
NaClO3,gpl 11.57 37.51 20 gpl, max.
pH NA 1.83 2.0, max
S O D I U M H Y P O C H L O R I T E PLANT
Tank No. 1 2 3 6 7
% NaOCl NA NA NA NA 7.78 7.40-8.00
% NaOH 0.57 0.40-1.00
Sp. Gravity 1.138 1.108, min
LI Q U I D C H LO R I N E PLAN T
Specs
Source LCP Tk.# Cl2 Feed LCP Tk # Cl2 Feed SULFURIC ACID
% Cl2 NA NA 99.5% min 91.0% min Source % H2SO4 Specs
% H2 NA NA NA NA LCP Comp. NA 97.0% min
UTILITIES
INSTRUMENT AIR @ AM Specs BOILER WATER Specs
Dew Point, °C UNDER REPAIR ≤3.8 °C SiO2, ppm 130 150 ppm, max.
GAS ANALYSIS
IEM 1 IEM 2 FLUE GAS
% Cl2 % H2 O2 + CO2 % Cl2 % H2 O2 + CO2 % CO % CO2 % O2
Line A NA NA NA
Line B
POLLUTION C O N T R O L - EFFLUENTS
pH OIL Hg TDS TSS Color COD
Source 6AM 7PM (+ or -) ppb ppm mg/L Pt-Co Units mg/L
S-2 8.63 8.54 - 0.056 204 4 40 NA
S-5 8.61 - 0.168 263 2 17 NA
S-8 6.87 - NA NA 22 98 NA
S-9 8.25 - NA NA 1 8 NA
Lagoon NA NA NA NA NA NA NA
Source pH gpl NaOH Source pH SPECIFICATIONS
JBC 8.23 ND S-3 7.63 pH = 6-9 COD = 100 mg/li, max Hg = 4 ppb, max.
Evap Canal 8.31 ND S-4 8.85 Oil = Negative TDS = 1000 ppm, max TSS = 100 mg/li, max
Total Canal 8.07 ND S-7 7.84 Color = 150 Pt-Co units, max.

Remarks: IEM 1 : SPB - Ca+Mg, NaCl; Depleted brine - NaCl Analyzed by Certified Correct
OFF-SPECS IEM 2 : Polished Brine -Ca + Mg; SPB - NaClO3; Depleted brine -NaClO (Original
3 copy signed) (Original copy signed)

Others : None NEY/ANB/RGD OVA


MVC-QF-TECH-004 (13)
Effectivity Date: August 5, 2014

MABUHAY VINYL CORPORATION PRODUCT TRANSFER CLEARANCE


Assumption Heights, Iligan City

Date : 03/30/17 [ ] IEM 1 [ ] IEM 2 [ ] Mktg [ ] QC file


IEM 1
HYDROCHLORIC ACID LIQUID CAUSTIC SODA SODIUM HYPOCHLORITE
Tk # % HCl SG @ 30”C Color Tk # 50% 32%. Tk # % NaOCl % NaOH SG @ 30”C
1 NA A NA NA 1 NA
2 NA B NA NA 2 NA
3 NA 3 NA
4 NA 6 NA
5 NA 7 7.78 0.57 1.138
IEM 2 SPECIFICATIONS
HYDROCHLORIC ACID LIQUID CAUSTIC SODA HYDROCHLORIC ACID
Tk # % HCl SG @ 30”C Color Tk # 50% 32%. % HCl 32.00 - 33.50
CTA 1 NA 9 NA - SG @ 30”C, min 1.152
CTA 2 NA 8 - 30.79 Color, max #3
CTA 3 NA LIQUID CAUSTIC SODA
CTB 1 NA 50% 32%
CTB 2 32.96 1.160 1 % NaOH 48.0-50.0 30.0 - 32.0
Remarks: % NaCl 0.10 0.10
WITHIN SPECS, OK for transfer ppm Fe, max 10 10
SODIUM HYPOCHLORITE
Analyzed by Certified Correct % NaOCl 7.40 - 8.00
(Original copy signed) (Original copy signed)
% excess NaOH 0.40 - 1.00
RGD OVA SG @ 30”C, min 1.108
MVC-QF-TECH-008(24) QUALITY CONTROL DAILY ANALYSIS REPORT
Effectivity Date: October 1, 2016 MABUHAY VINYL CORPORATION
Date : 03/31/17 Time : 11:50 AM [ ]QC [ ]Technical [ ]IEM1/IEM2 [ ]AVP-Mfg
IEM 1 IEM 2
50 % CAUSTIC SODA 50 % CAUSTIC SODA Specs
Online Tk – A Tk - B Online Tk - 9
% NaOH 49.64 50.00 NA 51.59 48.26 48.00-50.00
32 % CAUSTIC SODA 32 % CAUSTIC SODA
Online Tk – A Tk - B Online Tk - 8
% NaOH 30.07 NA NA 31.09 NA 30.00-32.00
HYDROCHLORIC ACID HYDROCHLORIC ACID
Online Tk- Tk- Online CTA 2 CTB 2
% HCl SD 33.31 33.25 33.10 32.00-33.50
Color 1 1 1 # 3, max
POLISHED BRINE(After Precoat) POLISHED BRINE(After Precoat)
Ca+Mg, ppm + NA = + NA = 5.0 ppm,max.
SPB (After Headtank) SPB (After Headtank)
Ca+Mg, ppb 12 + 2 = 14 20 + nil = 20 20 ppb, max.
NaCl, gpl NA NA 290 gpl,min.
Na2SO4,gpl NA NA 7 gpl, max.
NaClO3,gpl NA NA 20 gpl,max.
DEPLETED BRINE DEPLETED BRINE
NaCl, gpl 202 225 200 gpl, min.
Free Cl2 negative negative Negative
NaClO3,gpl NA NA 20 gpl, max.
pH NA NA 2.0, max
S O D I U M H Y P O C H L O R I T E PLANT
Tank No. 1 2 3 6 7
% NaOCl NA NA NA 7.57 NA 7.40-8.00
% NaOH 0.65 0.40-1.00
Sp. Gravity 1.134 1.108, min
LI Q U I D C H LO R I N E PLAN T
Specs
Source LCP Tk.# Cl2 Feed LCP Tk # Cl2 Feed SULFURIC ACID
% Cl2 NA NA 99.5% min 91.0% min Source % H2SO4 Specs
% H2 NA NA NA NA LCP Comp. NA 97.0% min
UTILITIES
INSTRUMENT AIR @ AM Specs BOILER WATER Specs
Dew Point, °C UNDER REPAIR ≤3.8 °C SiO2, ppm NA 150 ppm, max.
GAS ANALYSIS
IEM 1 IEM 2 FLUE GAS
% Cl2 % H2 O2 + CO2 % Cl2 % H2 O2 + CO2 % CO % CO2 % O2
Line A NA NA NA
Line B
POLLUTION C O N T R O L - EFFLUENTS
pH OIL Hg TDS TSS Color COD
Source 6AM 7PM (+ or -) ppb ppm mg/L Pt-Co Units mg/L
S-2 8.58 8.52 - NA NA NA NA NA
S-5 8.67 - NA NA NA NA NA
S-8 7.07 - NA NA 16 96 NA
S-9 8.28 - NA NA 2 8 NA
Lagoon NA NA NA NA NA NA NA
Source pH gpl NaOH Source pH SPECIFICATIONS
JBC NA S-3 NA pH = 6-9 COD = 100 mg/li, max Hg = 4 ppb, max.
Evap Canal S-4 Oil = Negative TDS = 1000 ppm, max TSS = 100 mg/li, max
Total Canal S-7 Color = 150 Pt-Co units, max.

Remarks: IEM 1 : None Analyzed by Certified Correct


OFF-SPECS IEM 2 : NaOH- online(50%) (Original copy signed) (Original copy signed)

Others : None NEY/ANB OVA


MVC-QF-TECH-004 (13)
Effectivity Date: August 5, 2014

MABUHAY VINYL CORPORATION PRODUCT TRANSFER CLEARANCE


Assumption Heights, Iligan City

Date : 03/31/17 [ ] IEM 1 [ ] IEM 2 [ ] Mktg [ ] QC file


IEM 1
HYDROCHLORIC ACID LIQUID CAUSTIC SODA SODIUM HYPOCHLORITE
Tk # % HCl SG @ 30”C Color Tk # 50% 32%. Tk # % NaOCl % NaOH SG @ 30”C
1 NA A 50.00 NA 1 NA
2 NA B NA NA 2 NA
3 NA 3 NA
4 NA 6 7.57 0.65 1.134
5 NA 7 NA
IEM 2 SPECIFICATIONS
HYDROCHLORIC ACID LIQUID CAUSTIC SODA HYDROCHLORIC ACID
Tk # % HCl SG @ 30”C Color Tk # 50% 32%. % HCl 32.00 - 33.50
CTA 1 NA 9 48.26 - SG @ 30”C, min 1.152
CTA 2 33.25 1.160 1 8 - NA Color, max #3
CTA 3 NA LIQUID CAUSTIC SODA
CTB 1 NA 50% 32%
CTB 2 33.10 1.160 1 % NaOH 48.0-50.0 30.0 - 32.0
Remarks: % NaCl 0.10 0.10
WITHIN SPECS, OK for transfer ppm Fe, max 10 10
SODIUM HYPOCHLORITE
Analyzed by Certified Correct % NaOCl 7.40 - 8.00
(Original copy signed) (Original copy signed)
% excess NaOH 0.40 - 1.00
ANB OVA SG @ 30”C, min 1.108
MVC-QF-TECH-008(24) QUALITY CONTROL DAILY ANALYSIS REPORT
Effectivity Date: October 1, 2016 MABUHAY VINYL CORPORATION
Date : 04/01/17 Time : 11:30 AM [ ]QC [ ]Technical [ ]IEM1/IEM2 [ ]AVP-Mfg
IEM 1 IEM 2
50 % CAUSTIC SODA 50 % CAUSTIC SODA Specs
Online Tk – A Tk - B Online Tk - 9
% NaOH 49.28 49.71 NA 49.09 NA 48.00-50.00
32 % CAUSTIC SODA 32 % CAUSTIC SODA
Online Tk – A Tk - B Online Tk - 8
% NaOH 30.44 NA NA 31.13 NA 30.00-32.00
HYDROCHLORIC ACID HYDROCHLORIC ACID
Online Tk- Tk- Online CTB 1
% HCl NA 32.39 33.27 32.00-33.50
Color 1 1 # 3, max
POLISHED BRINE(After Precoat) POLISHED BRINE(After Precoat)
Ca+Mg, ppm + NA = + NA = 5.0 ppm,max.
SPB (After Headtank) SPB (After Headtank)
Ca+Mg, ppb 64 + 2 = 68 nil + nil = nil 20 ppb, max.
NaCl, gpl NA NA 290 gpl,min.
Na2SO4,gpl NA NA 7 gpl, max.
NaClO3,gpl NA NA 20 gpl,max.
DEPLETED BRINE DEPLETED BRINE
NaCl, gpl 204 222 200 gpl, min.
Free Cl2 positive negative Negative
NaClO3,gpl NA NA 20 gpl, max.
pH NA NA 2.0, max
S O D I U M H Y P O C H L O R I T E PLANT
Tank No. 1 2 3 6 7
% NaOCl NA NA NA NA 7.97 7.40-8.00
% NaOH 0.53 0.40-1.00
Sp. Gravity 1.136 1.108, min
LI Q U I D C H LO R I N E PLAN T
Specs
Source LCP Tk.# Cl2 Feed LCP Tk # Cl2 Feed SULFURIC ACID
% Cl2 NA NA 99.5% min 91.0% min Source % H2SO4 Specs
% H2 NA NA NA NA LCP Comp. NA 97.0% min
UTILITIES
INSTRUMENT AIR @ AM Specs BOILER WATER Specs
Dew Point, °C for repair ≤3.8 °C SiO2, ppm NA 150 ppm, max.
GAS ANALYSIS
IEM 1 IEM 2 FLUE GAS
% Cl2 % H2 O2 + CO2 % Cl2 % H2 O2 + CO2 % CO % CO2 % O2
Line A NA NA NA
Line B
POLLUTION C O N T R O L - EFFLUENTS
pH OIL Hg TDS TSS Color COD
Source 6AM 7PM (+ or -) ppb ppm mg/L Pt-Co Units mg/L
S-2 8.56 8.66 - NA NA NA NA NA
S-5 9.20 - NA NA NA NA NA
S-8 7.33 - NA NA 7 75 NA
S-9 8.25 - NA NA 2 0 NA
Lagoon NA NA NA NA NA NA NA
Source pH gpl NaOH Source pH SPECIFICATIONS
JBC NA S-3 NA pH = 6-9 COD = 100 mg/li, max Hg = 4 ppb, max.
Evap Canal S-4 Oil = Negative TDS = 1000 ppm, max TSS = 100 mg/li, max
Total Canal S-7 Color = 150 Pt-Co units, max.

Remarks: IEM 1 : SPB - Ca+Mg; Depleted brine - Free Cl2 Analyzed by Certified Correct
OFF-SPECS IEM 2 : None (Original copy signed) (Original copy signed)

Others : Effluents - S5(pH) NEY/ANB/RGD OVA


MVC-QF-TECH-004 (13)
Effectivity Date: August 5, 2014

MABUHAY VINYL CORPORATION PRODUCT TRANSFER CLEARANCE


Assumption Heights, Iligan City

Date : 04/01/17 [ ] IEM 1 [ ] IEM 2 [ ] Mktg [ ] QC file


IEM 1
HYDROCHLORIC ACID LIQUID CAUSTIC SODA SODIUM HYPOCHLORITE
Tk # % HCl SG @ 30”C Color Tk # 50% 32%. Tk # % NaOCl % NaOH SG @ 30”C
1 NA A 49.71 NA 1 NA
2 NA B NA NA 2 NA
3 NA 3 NA
4 NA 6 NA
5 NA 7 7.97 0.53 1.136
IEM 2 SPECIFICATIONS
HYDROCHLORIC ACID LIQUID CAUSTIC SODA HYDROCHLORIC ACID
Tk # % HCl SG @ 30”C Color Tk # 50% 32%. % HCl 32.00 - 33.50
CTA 1 NA 9 NA - SG @ 30”C, min 1.152
CTA 2 NA 8 - NA Color, max #3
CTA 3 NA LIQUID CAUSTIC SODA
CTB 1 33.27 1.160 1 50% 32%
CTB 2 NA % NaOH 48.0-50.0 30.0 - 32.0
Remarks: % NaCl 0.10 0.10
WITHIN SPECS, OK for transfer ppm Fe, max 10 10
SODIUM HYPOCHLORITE
Analyzed by Certified Correct % NaOCl 7.40 - 8.00
(Original copy signed) (Original copy signed)
% excess NaOH 0.40 - 1.00
ANB OVA SG @ 30”C, min 1.108
MVC-QF-TECH-008(24) QUALITY CONTROL DAILY ANALYSIS REPORT
Effectivity Date: October 1, 2016 MABUHAY VINYL CORPORATION
Date : 04/02/17 Time : 11:45 AM [ ]QC [ ]Technical [ ]IEM1/IEM2 [ ]AVP-Mfg
IEM 1 IEM 2
50 % CAUSTIC SODA 50 % CAUSTIC SODA Specs
Online Tk – A Tk - B Online Tk - 9
% NaOH 49.81 49.87 NA SD NA 48.00-50.00
32 % CAUSTIC SODA 32 % CAUSTIC SODA
Online Tk – A Tk - B Online Tk - 8
% NaOH 30.17 NA NA 30.91 30.90 30.00-32.00
HYDROCHLORIC ACID HYDROCHLORIC ACID
Online Tk- Tk- Online CTA 2
% HCl NA 33.09 33.16 32.00-33.50
Color 1 1 # 3, max
POLISHED BRINE(After Precoat) POLISHED BRINE(After Precoat)
Ca+Mg, ppm + NA = + NA = 5.0 ppm,max.
SPB (After Headtank) SPB (After Headtank)
Ca+Mg, ppb NA NA 20 ppb, max.
NaCl, gpl 290 gpl,min.
Na2SO4,gpl 7 gpl, max.
NaClO3,gpl 20 gpl,max.
DEPLETED BRINE DEPLETED BRINE
NaCl, gpl NA NA 200 gpl, min.
Free Cl2 Negative
NaClO3,gpl 20 gpl, max.
pH 2.0, max
S O D I U M H Y P O C H L O R I T E PLANT
Tank No. 1 2 3 6 7
% NaOCl NA NA NA 7.89 NA 7.40-8.00
% NaOH 0.72 0.40-1.00
Sp. Gravity 1.130 1.108, min
LI Q U I D C H LO R I N E PLAN T
Specs
Source LCP Tk.# Cl2 Feed LCP Tk # Cl2 Feed SULFURIC ACID
% Cl2 NA NA 99.5% min 91.0% min Source % H2SO4 Specs
% H2 NA NA NA NA LCP Comp. NA 97.0% min
UTILITIES
INSTRUMENT AIR @ AM Specs BOILER WATER Specs
Dew Point, °C NA ≤3.8 °C SiO2, ppm NA 150 ppm, max.
GAS ANALYSIS
IEM 1 IEM 2 FLUE GAS
% Cl2 % H2 O2 + CO2 % Cl2 % H2 O2 + CO2 % CO % CO2 % O2
Line A NA NA NA
Line B
POLLUTION C O N T R O L - EFFLUENTS
pH OIL Hg TDS TSS Color COD
Source 6AM 7PM (+ or -) ppb ppm mg/L Pt-Co Units mg/L
S-2 NA - NA NA NA NA NA
S-5 NA - NA NA NA NA NA
S-8 NA - NA NA NA NA NA
S-9 NA - NA NA NA NA NA
Lagoon NA NA NA NA NA NA NA
Source pH gpl NaOH Source pH SPECIFICATIONS
JBC NA S-3 NA pH = 6-9 COD = 100 mg/li, max Hg = 4 ppb, max.
Evap Canal S-4 Oil = Negative TDS = 1000 ppm, max TSS = 100 mg/li, max
Total Canal S-7 Color = 150 Pt-Co units, max.

Remarks: IEM 1 : None Analyzed by Certified Correct


OFF-SPECS IEM 2 : None (Original copy signed) (Original copy signed)

Others : None ANB OVA


MVC-QF-TECH-004 (13)
Effectivity Date: August 5, 2014

MABUHAY VINYL CORPORATION PRODUCT TRANSFER CLEARANCE


Assumption Heights, Iligan City

Date : 04/02/17 [ ] IEM 1 [ ] IEM 2 [ ] Mktg [ ] QC file


IEM 1
HYDROCHLORIC ACID LIQUID CAUSTIC SODA SODIUM HYPOCHLORITE
Tk # % HCl SG @ 30”C Color Tk # 50% 32%. Tk # % NaOCl % NaOH SG @ 30”C
1 NA A 49.87 NA 1 NA
2 NA B NA NA 2 NA
3 NA 3 NA
4 NA 6 7.89 0.72 1.130
5 NA 7 NA
IEM 2 SPECIFICATIONS
HYDROCHLORIC ACID LIQUID CAUSTIC SODA HYDROCHLORIC ACID
Tk # % HCl SG @ 30”C Color Tk # 50% 32%. % HCl 32.00 - 33.50
CTA 1 NA 9 NA - SG @ 30”C, min 1.152
CTA 2 33.16 1.160 1 8 - 30.90 Color, max #3
CTA 3 NA LIQUID CAUSTIC SODA
CTB 1 NA 50% 32%
CTB 2 NA % NaOH 48.0-50.0 30.0 - 32.0
Remarks: % NaCl 0.10 0.10
WITHIN SPECS, OK for transfer ppm Fe, max 10 10
SODIUM HYPOCHLORITE
Analyzed by Certified Correct % NaOCl 7.40 - 8.00
(Original copy signed) (Original copy signed)
% excess NaOH 0.40 - 1.00
ANB OVA SG @ 30”C, min 1.108
RGD
MVC-QF-TECH-008(24) QUALITY CONTROL DAILY ANALYSIS REPORT
Effectivity Date: October 1, 2016 MABUHAY VINYL CORPORATION
Date : 04/03/17 Time : 11:30 AM [ ]QC [ ]Technical [ ]IEM1/IEM2 [ ]AVP-Mfg
IEM 1 IEM 2
50 % CAUSTIC SODA 50 % CAUSTIC SODA Specs
Online Tk – A Tk - B Online Tk - 9
% NaOH NA NA NA 48.00-50.00
32 % CAUSTIC SODA 32 % CAUSTIC SODA
Online Tk – A Tk - B Online Tk - 8
% NaOH NA NA NA 30.00-32.00
HYDROCHLORIC ACID HYDROCHLORIC ACID
Online Tk- Tk- Online CTA 2
% HCl NA 32.00-33.50
Color # 3, max
POLISHED BRINE(After Precoat) POLISHED BRINE(After Precoat)
Ca+Mg, ppm + NA = + NA = 5.0 ppm,max.
SPB (After Headtank) SPB (After Headtank)
Ca+Mg, ppb nil + nil = nil nil + nil = nil 20 ppb, max.
NaCl, gpl NA NA 290 gpl,min.
Na2SO4,gpl NA NA 7 gpl, max.
NaClO3,gpl NA NA 20 gpl,max.
DEPLETED BRINE DEPLETED BRINE
NaCl, gpl 200 gpl, min.
Free Cl2 negative negative Negative
NaClO3,gpl NA NA 20 gpl, max.
pH NA NA 2.0, max
S O D I U M H Y P O C H L O R I T E PLANT
Tank No. 1 2 3 6 7
% NaOCl NA NA NA NA NA 7.40-8.00
% NaOH 0.40-1.00
Sp. Gravity 1.108, min
LI Q U I D C H LO R I N E PLAN T
Specs
Source LCP Tk.# Cl2 Feed LCP Tk # Cl2 Feed SULFURIC ACID
% Cl2 NA NA 99.5% min 91.0% min Source % H2SO4 Specs
% H2 NA NA NA NA LCP Comp. NA 97.0% min
UTILITIES
INSTRUMENT AIR @ AM Specs BOILER WATER Specs
Dew Point, °C ≤3.8 °C SiO2, ppm NA 150 ppm, max.
GAS ANALYSIS
IEM 1 IEM 2 FLUE GAS
% Cl2 % H2 O2 + CO2 % Cl2 % H2 O2 + CO2 % CO % CO2 % O2
Line A NA NA NA
Line B
POLLUTION C O N T R O L - EFFLUENTS
pH OIL Hg TDS TSS Color COD
Source 6AM 7PM (+ or -) ppb ppm mg/L Pt-Co Units mg/L
S-2 - NA NA NA NA NA
S-5 NA - NA NA NA NA NA
S-8 NA - NA NA NA NA NA
S-9 NA - NA NA NA NA NA
Lagoon NA NA NA NA NA NA NA
Source pH gpl NaOH Source pH SPECIFICATIONS
JBC NA S-3 NA pH = 6-9 COD = 100 mg/li, max Hg = 4 ppb, max.
Evap Canal S-4 Oil = Negative TDS = 1000 ppm, max TSS = 100 mg/li, max
Total Canal S-7 Color = 150 Pt-Co units, max.

Remarks: IEM 1 : NaOH- online(50%); SPB - Ca+Mg, NaCl; Depleted brine - Free
Analyzed
Cl2 by Certified Correct
OFF-SPECS IEM 2 : SPB - Ca+Mg, Na2SO4; Depleted brine - Free Cl2, NaClO3 (Original copy signed) (Original copy signed)

Others : Instrument Air - dewpoint; Effluents - S8(pH), S9(Color) NEY/ANB/RGD OVA


MVC-QF-TECH-004 (13)
Effectivity Date: August 5, 2014

MABUHAY VINYL CORPORATION PRODUCT TRANSFER CLEARANCE


Assumption Heights, Iligan City

Date : 04/03/17 [ ] IEM 1 [ ] IEM 2 [ ] Mktg [ ] QC file


IEM 1
HYDROCHLORIC ACID LIQUID CAUSTIC SODA SODIUM HYPOCHLORITE
Tk # % HCl SG @ 30”C Color Tk # 50% 32%. Tk # % NaOCl % NaOH SG @ 30”C
1 NA A NA NA 1 NA 0.00 0.000
2 NA B NA NA 2 NA 0.00 0.000
3 NA 3 NA 0.00 0.000
4 NA 6 NA 0.00 0.000
5 NA 7 NA 0.00 0.000
IEM 2 SPECIFICATIONS
HYDROCHLORIC ACID LIQUID CAUSTIC SODA HYDROCHLORIC ACID
Tk # % HCl SG @ 30”C Color Tk # 50% 32%. % HCl 32.00 - 33.50
CTA 1 NA 9 NA - SG @ 30”C, min 1.152
CTA 2 NA 8 - NA Color, max #3
CTA 3 NA LIQUID CAUSTIC SODA
CTB 1 NA 50% 32%
CTB 2 NA % NaOH 48.0-50.0 30.0 - 32.0
Remarks: % NaCl 0.10 0.10
WITHIN SPECS, OK for transfer ppm Fe, max 10 10
SODIUM HYPOCHLORITE
Analyzed by Certified Correct % NaOCl 7.40 - 8.00
(Original copy signed) (Original copy signed)
% excess NaOH 0.40 - 1.00
ANB OVA SG @ 30”C, min 1.108
MVC-QF-TECH-008(24) QUALITY CONTROL DAILY ANALYSIS REPORT
Effectivity Date: October 1, 2016 MABUHAY VINYL CORPORATION
Date : 04/04/17 Time : 11:30 AM [ ]QC [ ]Technical [ ]IEM1/IEM2 [ ]AVP-Mfg
IEM 1 IEM 2
50 % CAUSTIC SODA 50 % CAUSTIC SODA Specs
Online Tk – A Tk - B Online Tk - 9
% NaOH 49.49 NA NA 51.50 48.83 48.00-50.00
32 % CAUSTIC SODA 32 % CAUSTIC SODA
Online Tk – A Tk - B Online Tk - 8
% NaOH 30.45 NA NA 31.42 NA 30.00-32.00
HYDROCHLORIC ACID HYDROCHLORIC ACID
Online Tk- Tk- Online CTA 2 CTB 1
% HCl NA 33.42 32.54 33.33 32.00-33.50
Color 1 1 1 # 3, max
POLISHED BRINE(After Precoat) POLISHED BRINE(After Precoat)
Ca+Mg, ppm + NA = + NA = 5.0 ppm,max.
SPB (After Headtank) SPB (After Headtank)
Ca+Mg, ppb 12 + nil = 12 nil + 12 = 12 20 ppb, max.
NaCl, gpl NA NA 290 gpl,min.
Na2SO4,gpl NA NA 7 gpl, max.
NaClO3,gpl NA NA 20 gpl,max.
DEPLETED BRINE DEPLETED BRINE
NaCl, gpl 228 240 200 gpl, min.
Free Cl2 negative negative Negative
NaClO3,gpl NA NA 20 gpl, max.
pH NA NA 2.0, max
S O D I U M H Y P O C H L O R I T E PLANT
Tank No. 1 2 3 6 7
% NaOCl NA NA NA 7.48 NA 7.40-8.00
% NaOH 0.72 0.40-1.00
Sp. Gravity 1.132 1.108, min
LI Q U I D C H LO R I N E PLAN T
Specs
Source LCP Tk.# Cl2 Feed LCP Tk # Cl2 Feed SULFURIC ACID
% Cl2 NA NA 99.5% min 91.0% min Source % H2SO4 Specs
% H2 NA NA NA NA LCP Comp. NA 97.0% min
UTILITIES
INSTRUMENT AIR @ AM Specs BOILER WATER Specs
Dew Point, °C for repair ≤3.8 °C SiO2, ppm NA 150 ppm, max.
GAS ANALYSIS
IEM 1 IEM 2 FLUE GAS
% Cl2 % H2 O2 + CO2 % Cl2 % H2 O2 + CO2 % CO % CO2 % O2
Line A NA NA NA
Line B
POLLUTION C O N T R O L - EFFLUENTS
pH OIL Hg TDS TSS Color COD
Source 6AM 7PM (+ or -) ppb ppm mg/L Pt-Co Units mg/L
S-2 8.55 9.23 - NA NA NA NA NA
S-5 8.68 - NA NA NA NA NA
S-8 7.97 - NA NA 9 43 NA
S-9 8.43 - NA NA 2 7 NA
Lagoon NA NA NA NA NA NA NA
Source pH gpl NaOH Source pH SPECIFICATIONS
JBC NA S-3 NA pH = 6-9 COD = 100 mg/li, max Hg = 4 ppb, max.
Evap Canal S-4 Oil = Negative TDS = 1000 ppm, max TSS = 100 mg/li, max
Total Canal S-7 Color = 150 Pt-Co units, max.

Remarks: IEM 1 : None Analyzed by Certified Correct


OFF-SPECS IEM 2 : NaOH - online(50%) (Original copy signed) (Original copy signed)

Others : Effluents - S2 PM(pH) NEY/ANB OVA


MVC-QF-TECH-004 (13)
Effectivity Date: August 5, 2014

MABUHAY VINYL CORPORATION PRODUCT TRANSFER CLEARANCE


Assumption Heights, Iligan City

Date : 04/04/17 [ ] IEM 1 [ ] IEM 2 [ ] Mktg [ ] QC file


IEM 1
HYDROCHLORIC ACID LIQUID CAUSTIC SODA SODIUM HYPOCHLORITE
Tk # % HCl SG @ 30”C Color Tk # 50% 32%. Tk # % NaOCl % NaOH SG @ 30”C
1 NA A NA NA 1 NA
2 NA B NA NA 2 NA
3 NA 3 NA
4 NA 6 7.48 0.72 1.132
5 NA 7 NA
IEM 2 SPECIFICATIONS
HYDROCHLORIC ACID LIQUID CAUSTIC SODA HYDROCHLORIC ACID
Tk # % HCl SG @ 30”C Color Tk # 50% 32%. % HCl 32.00 - 33.50
CTA 1 NA 9 48.83 - SG @ 30”C, min 1.152
CTA 2 32.54 1.160 1 8 - NA Color, max #3
CTA 3 NA LIQUID CAUSTIC SODA
CTB 1 33.33 1.160 1 50% 32%
CTB 2 NA % NaOH 48.0-50.0 30.0 - 32.0
Remarks: % NaCl 0.10 0.10
WITHIN SPECS, OK for transfer ppm Fe, max 10 10
SODIUM HYPOCHLORITE
Analyzed by Certified Correct % NaOCl 7.40 - 8.00
(Original copy signed) (Original copy signed)
% excess NaOH 0.40 - 1.00
ANB OVA SG @ 30”C, min 1.108
MVC-QF-TECH-008(24) QUALITY CONTROL DAILY ANALYSIS REPORT
Effectivity Date: October 1, 2016 MABUHAY VINYL CORPORATION
Date : 04/05/17 Time : 11:30 AM [ ]QC [ ]Technical [ ]IEM1/IEM2 [ ]AVP-Mfg
IEM 1 IEM 2
50 % CAUSTIC SODA 50 % CAUSTIC SODA Specs
Online Tk – A Tk - B Online Tk - 9
% NaOH 48.96 49.76 NA SD NA 48.00-50.00
32 % CAUSTIC SODA 32 % CAUSTIC SODA
Online Tk – A Tk - B Online Tk - 8
% NaOH 30.77 NA NA 30.82 30.88 30.00-32.00
HYDROCHLORIC ACID HYDROCHLORIC ACID
Online Tk- Tk- Online CTBA 2
% HCl NA 33.15 33.37 32.00-33.50
Color 1 1 # 3, max
POLISHED BRINE(After Precoat) POLISHED BRINE(After Precoat)
Ca+Mg, ppm + NA = + NA = 5.0 ppm,max.
SPB (After Headtank) SPB (After Headtank)
Ca+Mg, ppb 20 + 5 = 25 4 + nil = 4 20 ppb, max.
NaCl, gpl NA NA 290 gpl,min.
Na2SO4,gpl NA NA 7 gpl, max.
NaClO3,gpl NA NA 20 gpl,max.
DEPLETED BRINE DEPLETED BRINE
NaCl, gpl 209 226 200 gpl, min.
Free Cl2 negative negative Negative
NaClO3,gpl NA NA 20 gpl, max.
pH NA NA 2.0, max
S O D I U M H Y P O C H L O R I T E PLANT
Tank No. 1 2 3 6 7
% NaOCl NA NA NA NA 7.55 7.40-8.00
% NaOH 0.70 0.40-1.00
Sp. Gravity 1.132 1.108, min
LI Q U I D C H LO R I N E PLAN T
Specs
Source LCP Tk.# Cl2 Feed LCP Tk # Cl2 Feed SULFURIC ACID
% Cl2 NA NA 99.5% min 91.0% min Source % H2SO4 Specs
% H2 NA NA NA NA LCP Comp. NA 97.0% min
UTILITIES
INSTRUMENT AIR @ AM Specs BOILER WATER Specs
Dew Point, °C for repair ≤3.8 °C SiO2, ppm NA 150 ppm, max.
GAS ANALYSIS
IEM 1 IEM 2 FLUE GAS
% Cl2 % H2 O2 + CO2 % Cl2 % H2 O2 + CO2 % CO % CO2 % O2
Line A NA NA NA
Line B
POLLUTION C O N T R O L - EFFLUENTS
pH OIL Hg TDS TSS Color COD
Source 6AM 7PM (+ or -) ppb ppm mg/L Pt-Co Units mg/L
S-2 8.54 8.52 - NA NA NA NA NA
S-5 8.83 - NA NA NA NA NA
S-8 7.40 - NA NA 16 104 NA
S-9 8.62 - NA NA 1 11 NA
Lagoon NA NA NA NA NA NA NA
Source pH gpl NaOH Source pH SPECIFICATIONS
JBC NA S-3 NA pH = 6-9 COD = 100 mg/li, max Hg = 4 ppb, max.
Evap Canal S-4 Oil = Negative TDS = 1000 ppm, max TSS = 100 mg/li, max
Total Canal S-7 Color = 150 Pt-Co units, max.

Remarks: IEM 1 : SPB - Ca+Mg Analyzed by Certified Correct


OFF-SPECS IEM 2 : None (Original copy signed) (Original copy signed)

Others : None ANB OVA


MVC-QF-TECH-004 (13)
Effectivity Date: August 5, 2014

MABUHAY VINYL CORPORATION PRODUCT TRANSFER CLEARANCE


Assumption Heights, Iligan City

Date : 04/05/17 [ ] IEM 1 [ ] IEM 2 [ ] Mktg [ ] QC file


IEM 1
HYDROCHLORIC ACID LIQUID CAUSTIC SODA SODIUM HYPOCHLORITE
Tk # % HCl SG @ 30”C Color Tk # 50% 32%. Tk # % NaOCl % NaOH SG @ 30”C
1 NA A 49.76 NA 1 NA
2 NA B NA NA 2 NA
3 NA 3 NA
4 NA 6 NA
5 NA 7 7.55 0.70 1.132
IEM 2 SPECIFICATIONS
HYDROCHLORIC ACID LIQUID CAUSTIC SODA HYDROCHLORIC ACID
Tk # % HCl SG @ 30”C Color Tk # 50% 32%. % HCl 32.00 - 33.50
CTA 1 NA 9 NA - SG @ 30”C, min 1.152
CTA 2 NA 8 - 30.88 Color, max #3
CTA 3 NA LIQUID CAUSTIC SODA
CTB 1 NA 50% 32%
CTB 2 33.37 1.160 1 % NaOH 48.0-50.0 30.0 - 32.0
Remarks: % NaCl 0.10 0.10
WITHIN SPECS, OK for transfer ppm Fe, max 10 10
SODIUM HYPOCHLORITE
Analyzed by Certified Correct % NaOCl 7.40 - 8.00
(Original copy signed) (Original copy signed)
% excess NaOH 0.40 - 1.00
ANB OVA SG @ 30”C, min 1.108
MVC-QF-TECH-008(24) QUALITY CONTROL DAILY ANALYSIS REPORT
Effectivity Date: October 1, 2016 MABUHAY VINYL CORPORATION
Date : 04/06/17 Time : 11:30 AM [ ]QC [ ]Technical [ ]IEM1/IEM2 [ ]AVP-Mfg
IEM 1 IEM 2
50 % CAUSTIC SODA 50 % CAUSTIC SODA Specs
Online Tk – A Tk - B Online Tk - 9
% NaOH 49.27 NA NA 50.04 NA 48.00-50.00
32 % CAUSTIC SODA 32 % CAUSTIC SODA
Online Tk – A Tk - B Online Tk - 8
% NaOH 29.66 NA NA 31.05 31.04 30.00-32.00
HYDROCHLORIC ACID HYDROCHLORIC ACID
Online Tk- Tk- Online CTB 1
% HCl NA 33.20 33.33 32.00-33.50
Color 1 1 # 3, max
POLISHED BRINE(After Precoat) POLISHED BRINE(After Precoat)
Ca+Mg, ppm + NA = + NA = 5.0 ppm,max.
SPB (After Headtank) SPB (After Headtank)
Ca+Mg, ppb 8 + 10 = 18 nil + nil = nil 20 ppb, max.
NaCl, gpl NA NA 290 gpl,min.
Na2SO4,gpl 2.81 5.48 7 gpl, max.
NaClO3,gpl NA NA 20 gpl,max.
DEPLETED BRINE DEPLETED BRINE
NaCl, gpl 209 226 200 gpl, min.
Free Cl2 negative negative Negative
NaClO3,gpl NA NA 20 gpl, max.
pH NA NA 2.0, max
S O D I U M H Y P O C H L O R I T E PLANT
Tank No. 1 2 3 6 7
% NaOCl NA NA NA 7.54 NA 7.40-8.00
% NaOH 0.75 0.40-1.00
Sp. Gravity 1.132 1.108, min
LI Q U I D C H LO R I N E PLAN T
Specs
Source LCP Tk.# Cl2 Feed LCP Tk # Cl2 Feed SULFURIC ACID
% Cl2 NA NA 99.5% min 91.0% min Source % H2SO4 Specs
% H2 NA NA NA NA LCP Comp. NA 97.0% min
UTILITIES
INSTRUMENT AIR @ AM Specs BOILER WATER Specs
Dew Point, °C for repair ≤3.8 °C SiO2, ppm NA 150 ppm, max.
GAS ANALYSIS
IEM 1 IEM 2 FLUE GAS
% Cl2 % H2 O2 + CO2 % Cl2 % H2 O2 + CO2 % CO % CO2 % O2
Line A NA NA NA
Line B
POLLUTION C O N T R O L - EFFLUENTS
pH OIL Hg TDS TSS Color COD
Source 6AM 7PM (+ or -) ppb ppm mg/L Pt-Co Units mg/L
S-2 8.55 8.44 - NA NA NA NA NA
S-5 8.63 - NA NA NA NA NA
S-8 7.83 - NA NA 17 89 NA
S-9 8.33 - NA NA 3 25 NA
Lagoon NA NA NA NA NA NA NA
Source pH gpl NaOH Source pH SPECIFICATIONS
JBC NA S-3 NA pH = 6-9 COD = 100 mg/li, max Hg = 4 ppb, max.
Evap Canal S-4 Oil = Negative TDS = 1000 ppm, max TSS = 100 mg/li, max
Total Canal S-7 Color = 150 Pt-Co units, max.

Remarks: IEM 1 : NaOH- online(32%) Analyzed by Certified Correct


OFF-SPECS IEM 2 : NaOH - online(50%) (Original copy signed) (Original copy signed)

Others : None ANB OVA


MVC-QF-TECH-004 (13)
Effectivity Date: August 5, 2014

MABUHAY VINYL CORPORATION PRODUCT TRANSFER CLEARANCE


Assumption Heights, Iligan City

Date : 04/06/17 [ ] IEM 1 [ ] IEM 2 [ ] Mktg [ ] QC file


IEM 1
HYDROCHLORIC ACID LIQUID CAUSTIC SODA SODIUM HYPOCHLORITE
Tk # % HCl SG @ 30”C Color Tk # 50% 32%. Tk # % NaOCl % NaOH SG @ 30”C
1 NA A NA NA 1 NA
2 NA B NA NA 2 NA
3 NA 3 NA
4 NA 6 7.54 0.75 1.132
5 NA 7 NA 0.00 0.000
IEM 2 SPECIFICATIONS
HYDROCHLORIC ACID LIQUID CAUSTIC SODA HYDROCHLORIC ACID
Tk # % HCl SG @ 30”C Color Tk # 50% 32%. % HCl 32.00 - 33.50
CTA 1 NA 9 NA - SG @ 30”C, min 1.152
CTA 2 NA 8 - 31.04 Color, max #3
CTA 3 NA LIQUID CAUSTIC SODA
CTB 1 33.33 1.160 1 50% 32%
CTB 2 NA % NaOH 48.0-50.0 30.0 - 32.0
Remarks: % NaCl 0.10 0.10
WITHIN SPECS, OK for transfer ppm Fe, max 10 10
SODIUM HYPOCHLORITE
Analyzed by Certified Correct % NaOCl 7.40 - 8.00
(Original copy signed) (Original copy signed)
% excess NaOH 0.40 - 1.00
ANB OVA SG @ 30”C, min 1.108
MVC-QF-TECH-008(24) QUALITY CONTROL DAILY ANALYSIS REPORT
Effectivity Date: October 1, 2016 MABUHAY VINYL CORPORATION
Date : 04/07/17 Time : 11:30 AM [ ]QC [ ]Technical [ ]IEM1/IEM2 [ ]AVP-Mfg
IEM 1 IEM 2
50 % CAUSTIC SODA 50 % CAUSTIC SODA Specs
Online Tk – A Tk - B Online Tk - 9
% NaOH SD 49.70 NA SD NA 48.00-50.00
32 % CAUSTIC SODA 32 % CAUSTIC SODA
Online Tk – A Tk - B Online Tk - 8
% NaOH SD NA NA 30.86 31.30 30.00-32.00
HYDROCHLORIC ACID HYDROCHLORIC ACID
Online Tk- Tk- Online CTA 2 CTB 1
% HCl SD 34.05 33.30 33.44 32.00-33.50
Color 1 1 1 # 3, max
POLISHED BRINE(After Precoat) POLISHED BRINE(After Precoat)
Ca+Mg, ppm + NA = + NA = 5.0 ppm,max.
SPB (After Headtank) SPB (After Headtank)
Ca+Mg, ppb 16 + 9 = 25 nil + nil = nil 20 ppb, max.
NaCl, gpl NA 315 290 gpl,min.
Na2SO4,gpl NA NA 7 gpl, max.
NaClO3,gpl NA 25.41 20 gpl,max.
DEPLETED BRINE DEPLETED BRINE
NaCl, gpl SD 226 200 gpl, min.
Free Cl2 negative Negative
NaClO3,gpl 34.97 20 gpl, max.
pH 2.89 2.0, max
S O D I U M H Y P O C H L O R I T E PLANT
Tank No. 1 2 3 6 7
% NaOCl NA NA NA NA NA 7.40-8.00
% NaOH 0.40-1.00
Sp. Gravity 1.108, min
LI Q U I D C H LO R I N E PLAN T
Specs
Source LCP Tk.# Cl2 Feed LCP Tk # Cl2 Feed SULFURIC ACID
% Cl2 NA NA 99.5% min 91.0% min Source % H2SO4 Specs
% H2 NA NA NA NA LCP Comp. NA 97.0% min
UTILITIES
INSTRUMENT AIR @ AM Specs BOILER WATER Specs
Dew Point, °C for repair ≤3.8 °C SiO2, ppm NA 150 ppm, max.
GAS ANALYSIS
IEM 1 IEM 2 FLUE GAS
% Cl2 % H2 O2 + CO2 % Cl2 % H2 O2 + CO2 % CO % CO2 % O2
Line A NA NA NA
Line B
POLLUTION C O N T R O L - EFFLUENTS
pH OIL Hg TDS TSS Color COD
Source 6AM 7PM (+ or -) ppb ppm mg/L Pt-Co Units mg/L
S-2 8.68 8.61 - NA NA NA NA NA
S-5 8.62 - NA NA NA NA NA
S-8 7.78 - NA NA 11 73 NA
S-9 8.36 - NA NA 3 11 NA
Lagoon NA NA NA NA NA NA NA
Source pH gpl NaOH Source pH SPECIFICATIONS
JBC NA S-3 NA pH = 6-9 COD = 100 mg/li, max Hg = 4 ppb, max.
Evap Canal S-4 Oil = Negative TDS = 1000 ppm, max TSS = 100 mg/li, max
Total Canal S-7 Color = 150 Pt-Co units, max.

Remarks: IEM 1 : SPB - Ca+Mg Analyzed by Certified Correct


OFF-SPECS IEM 2 : HCl - online; SPB - NaClO3; Depleted brine - pH, NaClO3 (Original copy signed) (Original copy signed)

Others : None NEY OVA


MVC-QF-TECH-004 (13)
Effectivity Date: August 5, 2014

MABUHAY VINYL CORPORATION PRODUCT TRANSFER CLEARANCE


Assumption Heights, Iligan City

Date : 04/07/17 [ ] IEM 1 [ ] IEM 2 [ ] Mktg [ ] QC file


IEM 1
HYDROCHLORIC ACID LIQUID CAUSTIC SODA SODIUM HYPOCHLORITE
Tk # % HCl SG @ 30”C Color Tk # 50% 32%. Tk # % NaOCl % NaOH SG @ 30”C
1 NA A 49.70 NA 1 NA
2 NA B NA NA 2 NA
3 NA 3 NA
4 NA 6 NA
5 NA 7 NA
IEM 2 SPECIFICATIONS
HYDROCHLORIC ACID LIQUID CAUSTIC SODA HYDROCHLORIC ACID
Tk # % HCl SG @ 30”C Color Tk # 50% 32%. % HCl 32.00 - 33.50
CTA 1 NA 9 NA - SG @ 30”C, min 1.152
CTA 2 33.30 1.160 1 8 - 31.30 Color, max #3
CTA 3 NA LIQUID CAUSTIC SODA
CTB 1 33.44 1.160 1 50% 32%
CTB 2 NA % NaOH 48.0-50.0 30.0 - 32.0
Remarks: % NaCl 0.10 0.10
WITHIN SPECS, OK for transfer ppm Fe, max 10 10
SODIUM HYPOCHLORITE
Analyzed by Certified Correct % NaOCl 7.40 - 8.00
(Original copy signed) (Original copy signed)
% excess NaOH 0.40 - 1.00
NEY OVA SG @ 30”C, min 1.108
MVC-QF-TECH-008(24) QUALITY CONTROL DAILY ANALYSIS REPORT
Effectivity Date: October 1, 2016 MABUHAY VINYL CORPORATION
Date : 04/08/17 Time : 11:30 AM [ ]QC [ ]Technical [ ]IEM1/IEM2 [ ]AVP-Mfg
IEM 1 IEM 2
50 % CAUSTIC SODA 50 % CAUSTIC SODA Specs
Online Tk – A Tk - B Online Tk - 9
% NaOH 49.87 49.56 NA 49.83 NA 48.00-50.00
32 % CAUSTIC SODA 32 % CAUSTIC SODA
Online Tk – A Tk - B Online Tk - 8
% NaOH 30.76 NA NA 31.15 NA 30.00-32.00
HYDROCHLORIC ACID HYDROCHLORIC ACID
Online Tk- 3 Tk- Online CTB 2
% HCl 32.68 33.20 33.57 32.88 32.00-33.50
Color 1 1 1 1 # 3, max
POLISHED BRINE(After Precoat) POLISHED BRINE(After Precoat)
Ca+Mg, ppm + NA = + NA = 5.0 ppm,max.
SPB (After Headtank) SPB (After Headtank)
Ca+Mg, ppb nil + 5 = 5 nil + nil = nil 20 ppb, max.
NaCl, gpl NA NA 290 gpl,min.
Na2SO4,gpl NA NA 7 gpl, max.
NaClO3,gpl NA NA 20 gpl,max.
DEPLETED BRINE DEPLETED BRINE
NaCl, gpl 207 222 200 gpl, min.
Free Cl2 negative negative Negative
NaClO3,gpl NA NA 20 gpl, max.
pH NA NA 2.0, max
S O D I U M H Y P O C H L O R I T E PLANT
Tank No. 1 2 3 6 7
% NaOCl NA NA NA 7.80 7.61 7.40-8.00
% NaOH 0.81 0.82 0.40-1.00
Sp. Gravity 1.132 1.146 1.108, min
LI Q U I D C H LO R I N E PLAN T
Specs
Source LCP Tk.# Cl2 Feed LCP Tk # Cl2 Feed SULFURIC ACID
% Cl2 NA NA 99.5% min 91.0% min Source % H2SO4 Specs
% H2 NA NA NA NA LCP Comp. NA 97.0% min
UTILITIES
INSTRUMENT AIR @ 1115 AM Specs BOILER WATER Specs
Dew Point, °C 5.7 ≤3.8 °C SiO2, ppm NA 150 ppm, max.
GAS ANALYSIS
IEM 1 IEM 2 FLUE GAS
% Cl2 % H2 O2 + CO2 % Cl2 % H2 O2 + CO2 % CO % CO2 % O2
Line A NA NA NA
Line B
POLLUTION C O N T R O L - EFFLUENTS
pH OIL Hg TDS TSS Color COD
Source 6AM 7PM (+ or -) ppb ppm mg/L Pt-Co Units mg/L
S-2 8.68 8.48 - 0.056 256 6 43 NA
S-5 8.62 - 0.335 368 3 24 NA
S-8 7.63 - NA NA 9 110 NA
S-9 8.42 - NA NA 11 15 NA
Lagoon 8.26 - 0.056 159 4 28 NA
Source pH gpl NaOH Source pH SPECIFICATIONS
JBC 8.17 ND S-3 8.25 pH = 6-9 COD = 100 mg/li, max Hg = 4 ppb, max.
Evap Canal 8.34 ND S-4 8.82 Oil = Negative TDS = 1000 ppm, max TSS = 100 mg/li, max
Total Canal 8.03 ND S-7 8.48 Color = 150 Pt-Co units, max.

Remarks: IEM 1 : None Analyzed by Certified Correct


OFF-SPECS IEM 2 : HCl - online (Original copy signed) (Original copy signed)

Others : Instrument Air - dewpoint NEY/ANB OVA


MVC-QF-TECH-004 (13)
Effectivity Date: August 5, 2014

MABUHAY VINYL CORPORATION PRODUCT TRANSFER CLEARANCE


Assumption Heights, Iligan City

Date : 04/08/17 [ ] IEM 1 [ ] IEM 2 [ ] Mktg [ ] QC file


IEM 1
HYDROCHLORIC ACID LIQUID CAUSTIC SODA SODIUM HYPOCHLORITE
Tk # % HCl SG @ 30”C Color Tk # 50% 32%. Tk # % NaOCl % NaOH SG @ 30”C
1 NA A 49.56 NA 1 NA
2 NA B NA NA 2 NA
3 33.20 1.160 1 3 NA
4 NA 6 7.80 0.81 1.132
5 NA 7 7.61 0.82 1.146
IEM 2 SPECIFICATIONS
HYDROCHLORIC ACID LIQUID CAUSTIC SODA HYDROCHLORIC ACID
Tk # % HCl SG @ 30”C Color Tk # 50% 32%. % HCl 32.00 - 33.50
CTA 1 NA 9 NA - SG @ 30”C, min 1.152
CTA 2 NA 8 - NA Color, max #3
CTA 3 NA LIQUID CAUSTIC SODA
CTB 1 NA 50% 32%
CTB 2 32.88 1.158 1 % NaOH 48.0-50.0 30.0 - 32.0
Remarks: % NaCl 0.10 0.10
WITHIN SPECS, OK for transfer ppm Fe, max 10 10
SODIUM HYPOCHLORITE
Analyzed by Certified Correct % NaOCl 7.40 - 8.00
(Original copy signed) (Original copy signed)
% excess NaOH 0.40 - 1.00
ANB OVA SG @ 30”C, min 1.108
MVC-QF-TECH-008(24) QUALITY CONTROL DAILY ANALYSIS REPORT
Effectivity Date: October 1, 2016 MABUHAY VINYL CORPORATION
Date : 04/09/17 Time : 11:30 AM [ ]QC [ ]Technical [ ]IEM1/IEM2 [ ]AVP-Mfg
IEM 1 IEM 2
50 % CAUSTIC SODA 50 % CAUSTIC SODA Specs
Online Tk – A Tk - B Online Tk - 9
% NaOH 49.70 NA NA 46.88 NA 48.00-50.00
32 % CAUSTIC SODA 32 % CAUSTIC SODA
Online Tk – A Tk - B Online Tk - 8
% NaOH 30.78 NA NA 30.56 NA 30.00-32.00
HYDROCHLORIC ACID HYDROCHLORIC ACID
Online Tk- 5 Tk- Online CTA 2
% HCl 33.50 32.87 33.50 33.41 32.00-33.50
Color 1 1 1 1 # 3, max
POLISHED BRINE(After Precoat) POLISHED BRINE(After Precoat)
Ca+Mg, ppm + NA = + NA = 5.0 ppm,max.
SPB (After Headtank) SPB (After Headtank)
Ca+Mg, ppb NA NA 20 ppb, max.
NaCl, gpl 290 gpl,min.
Na2SO4,gpl 7 gpl, max.
NaClO3,gpl 20 gpl,max.
DEPLETED BRINE DEPLETED BRINE
NaCl, gpl NA NA 200 gpl, min.
Free Cl2 Negative
NaClO3,gpl 20 gpl, max.
pH 2.0, max
S O D I U M H Y P O C H L O R I T E PLANT
Tank No. 1 2 3 6 7
% NaOCl NA NA NA NA 8.70 7.40-8.00
% NaOH 0.91 0.40-1.00
Sp. Gravity 1.134 1.108, min
LI Q U I D C H LO R I N E PLAN T
Specs
Source LCP Tk.# Cl2 Feed LCP Tk # Cl2 Feed SULFURIC ACID
% Cl2 NA NA 99.5% min 91.0% min Source % H2SO4 Specs
% H2 NA NA NA NA LCP Comp. NA 97.0% min
UTILITIES
INSTRUMENT AIR @ AM Specs BOILER WATER Specs
Dew Point, °C NA ≤3.8 °C SiO2, ppm NA 150 ppm, max.
GAS ANALYSIS
IEM 1 IEM 2 FLUE GAS
% Cl2 % H2 O2 + CO2 % Cl2 % H2 O2 + CO2 % CO % CO2 % O2
Line A NA NA NA
Line B
POLLUTION C O N T R O L - EFFLUENTS
pH OIL Hg TDS TSS Color COD
Source 6AM 7PM (+ or -) ppb ppm mg/L Pt-Co Units mg/L
S-2 NA - NA NA NA NA NA
S-5 NA - NA NA NA NA NA
S-8 NA - NA NA NA NA NA
S-9 NA - NA NA NA NA NA
Lagoon NA NA NA NA NA NA NA
Source pH gpl NaOH Source pH SPECIFICATIONS
JBC NA S-3 NA pH = 6-9 COD = 100 mg/li, max Hg = 4 ppb, max.
Evap Canal S-4 Oil = Negative TDS = 1000 ppm, max TSS = 100 mg/li, max
Total Canal S-7 Color = 150 Pt-Co units, max.

Remarks: IEM 1 : None Analyzed by Certified Correct


OFF-SPECS IEM 2 : NaOH - online(50%) (Original copy signed) (Original copy signed)

Others : None ANB OVA


MVC-QF-TECH-004 (13)
Effectivity Date: August 5, 2014

MABUHAY VINYL CORPORATION PRODUCT TRANSFER CLEARANCE


Assumption Heights, Iligan City

Date : 04/09/17 [ ] IEM 1 [ ] IEM 2 [ ] Mktg [ ] QC file


IEM 1
HYDROCHLORIC ACID LIQUID CAUSTIC SODA SODIUM HYPOCHLORITE
Tk # % HCl SG @ 30”C Color Tk # 50% 32%. Tk # % NaOCl % NaOH SG @ 30”C
1 NA A NA NA 1 NA
2 NA B NA NA 2 NA
3 NA 3 NA
4 NA 6 NA
5 32.87 1.158 1 7 NA
IEM 2 SPECIFICATIONS
HYDROCHLORIC ACID LIQUID CAUSTIC SODA HYDROCHLORIC ACID
Tk # % HCl SG @ 30”C Color Tk # 50% 32%. % HCl 32.00 - 33.50
CTA 1 NA 9 NA - SG @ 30”C, min 1.152
CTA 2 33.41 1.160 1 8 - NA Color, max #3
CTA 3 NA LIQUID CAUSTIC SODA
CTB 1 NA 50% 32%
CTB 2 NA % NaOH 48.0-50.0 30.0 - 32.0
Remarks: % NaCl 0.10 0.10
WITHIN SPECS, OK for transfer ppm Fe, max 10 10
SODIUM HYPOCHLORITE
Analyzed by Certified Correct % NaOCl 7.40 - 8.00
(Original copy signed) (Original copy signed)
% excess NaOH 0.40 - 1.00
ANB OVA SG @ 30”C, min 1.108
MVC-QF-TECH-008(24) QUALITY CONTROL DAILY ANALYSIS REPORT
Effectivity Date: October 1, 2016 MABUHAY VINYL CORPORATION
Date : 04/10/17 Time : 11:30 AM [ ]QC [ ]Technical [ ]IEM1/IEM2 [ ]AVP-Mfg
IEM 1 IEM 2
50 % CAUSTIC SODA 50 % CAUSTIC SODA Specs
Online Tk – A Tk - B Online Tk - 9
% NaOH 50.35 50.56 NA SD 49.35 48.00-50.00
32 % CAUSTIC SODA 32 % CAUSTIC SODA
Online Tk – A Tk - B Online Tk - 8
% NaOH 30.08 NA NA SD NA 30.00-32.00
HYDROCHLORIC ACID HYDROCHLORIC ACID
Online Tk- 1 Tk- 4 Online CTB 2
% HCl 33.03 32.82 34.28 SD 33.18 32.00-33.50
Color 1 1 1 1 # 3, max
POLISHED BRINE(After Precoat) POLISHED BRINE(After Precoat)
Ca+Mg, ppm + NA = + NA = 5.0 ppm,max.
SPB (After Headtank) SPB (After Headtank)
Ca+Mg, ppb 32 + 2 = 34 SD 20 ppb, max.
NaCl, gpl NA 290 gpl,min.
Na2SO4,gpl 2.22 7 gpl, max.
NaClO3,gpl NA 20 gpl,max.
DEPLETED BRINE DEPLETED BRINE
NaCl, gpl 198 SD 200 gpl, min.
Free Cl2 positive Negative
NaClO3,gpl NA 20 gpl, max.
pH NA 2.0, max
S O D I U M H Y P O C H L O R I T E PLANT
Tank No. 1 2 3 6 7
% NaOCl NA NA NA 7.80 7.72 7.40-8.00
% NaOH 0.75 0.73 0.40-1.00
Sp. Gravity 1.140 1.134 1.108, min
LI Q U I D C H LO R I N E PLAN T
Specs
Source LCP Tk.# Cl2 Feed LCP Tk # Cl2 Feed SULFURIC ACID
% Cl2 NA NA 99.5% min 91.0% min Source % H2SO4 Specs
% H2 NA NA NA NA LCP Comp. NA 97.0% min
UTILITIES
INSTRUMENT AIR @ 2PM Specs BOILER WATER Specs
Dew Point, °C 8.6 ≤3.8 °C SiO2, ppm NA 150 ppm, max.
GAS ANALYSIS
IEM 1 IEM 2 FLUE GAS
% Cl2 % H2 O2 + CO2 % Cl2 % H2 O2 + CO2 % CO % CO2 % O2
Line A NA NA NA
Line B
POLLUTION C O N T R O L - EFFLUENTS
pH OIL Hg TDS TSS Color COD
Source 6AM 7PM (+ or -) ppb ppm mg/L Pt-Co Units mg/L
S-2 8.68 8.64 - NA NA NA NA NA
S-5 8.62 - NA NA NA NA NA
S-8 7.67 - NA NA 12 116 NA
S-9 8.32 - NA NA 4 12 NA
Lagoon NA NA NA NA NA NA NA
Source pH gpl NaOH Source pH SPECIFICATIONS
JBC NA S-3 NA pH = 6-9 COD = 100 mg/li, max Hg = 4 ppb, max.
Evap Canal S-4 Oil = Negative TDS = 1000 ppm, max TSS = 100 mg/li, max
Total Canal S-7 Color = 150 Pt-Co units, max.

Remarks: NaOH- online(50%), Tk-A; HCl - Tk 4; SPB - Ca+Mg;


IEM 1 : Depleted brine - NaCl, Free Cl2 Analyzed by Certified Correct
OFF-SPECS IEM 2 : None (Original copy signed) (Original copy signed)

Others : Instrument Air - dewpoint NEY OVA


MVC-QF-TECH-004 (13)
Effectivity Date: August 5, 2014

MABUHAY VINYL CORPORATION PRODUCT TRANSFER CLEARANCE


Assumption Heights, Iligan City

Date : 04/10/17 [ ] IEM 1 [ ] IEM 2 [ ] Mktg [ ] QC file


IEM 1
HYDROCHLORIC ACID LIQUID CAUSTIC SODA SODIUM HYPOCHLORITE
Tk # % HCl SG @ 30”C Color Tk # 50% 32%. Tk # % NaOCl % NaOH SG @ 30”C
1 32.82 1.156 1 A NA NA 1 NA
2 NA B NA NA 2 NA
3 NA 3 NA
4 NA 6 7.80 0.75 1.140
5 NA 7 7.72 0.73 1.134
IEM 2 SPECIFICATIONS
HYDROCHLORIC ACID LIQUID CAUSTIC SODA HYDROCHLORIC ACID
Tk # % HCl SG @ 30”C Color Tk # 50% 32%. % HCl 32.00 - 33.50
CTA 1 NA 9 49.35 - SG @ 30”C, min 1.152
CTA 2 NA 8 - NA Color, max #3
CTA 3 NA LIQUID CAUSTIC SODA
CTB 1 NA 50% 32%
CTB 2 33.18 1.160 1 % NaOH 48.0-50.0 30.0 - 32.0
Remarks: % NaCl 0.10 0.10
WITHIN SPECS, OK for transfer ppm Fe, max 10 10
SODIUM HYPOCHLORITE
Analyzed by Certified Correct % NaOCl 7.40 - 8.00
(Original copy signed) (Original copy signed)
% excess NaOH 0.40 - 1.00
NEY OVA SG @ 30”C, min 1.108
MVC-QF-TECH-008(24) QUALITY CONTROL DAILY ANALYSIS REPORT
Effectivity Date: October 1, 2016 MABUHAY VINYL CORPORATION
Date : 04/11/17 Time : 11:30 AM [ ]QC [ ]Technical [ ]IEM1/IEM2 [ ]AVP-Mfg
IEM 1 IEM 2
50 % CAUSTIC SODA 50 % CAUSTIC SODA Specs
Online Tk – A Tk - B Online Tk - 9
% NaOH 50.14 49.67 NA SD NA 48.00-50.00
32 % CAUSTIC SODA 32 % CAUSTIC SODA
Online Tk – A Tk - B Online Tk - 8
% NaOH 29.53 NA NA SD 31.22 30.00-32.00
HYDROCHLORIC ACID HYDROCHLORIC ACID
Online Tk- 2 Tk- Online CTA 2
% HCl 32.59 33.02 SD 32.00-33.50
Color 1 1 # 3, max
POLISHED BRINE(After Precoat) POLISHED BRINE(After Precoat)
Ca+Mg, ppm 4.00 + nil = 4.00 + SD = 5.0 ppm,max.
SPB (After Headtank) SPB (After Headtank)
Ca+Mg, ppb 12 + nil = 2 SD 20 ppb, max.
NaCl, gpl 273 290 gpl,min.
Na2SO4,gpl 2.22 7 gpl, max.
NaClO3,gpl 3.51 20 gpl,max.
DEPLETED BRINE DEPLETED BRINE
NaCl, gpl 181 SD 200 gpl, min.
Free Cl2 positive Negative
NaClO3,gpl 8.06 20 gpl, max.
pH NA 2.0, max
S O D I U M H Y P O C H L O R I T E PLANT
Tank No. 1 2 3 6 7
% NaOCl NA NA NA 7.68 NA 7.40-8.00
% NaOH 0.68 0.40-1.00
Sp. Gravity 1.132 1.108, min
LI Q U I D C H LO R I N E PLAN T
Specs
Source LCP Tk.# Cl2 Feed LCP Tk # Cl2 Feed SULFURIC ACID
% Cl2 NA NA 99.5% min 91.0% min Source % H2SO4 Specs
% H2 NA NA NA NA LCP Comp. NA 97.0% min
UTILITIES
INSTRUMENT AIR @ 1140 AM Specs BOILER WATER Specs
Dew Point, °C 7.6 ≤3.8 °C SiO2, ppm NA 150 ppm, max.
GAS ANALYSIS
IEM 1 IEM 2 FLUE GAS
% Cl2 % H2 O2 + CO2 % Cl2 % H2 O2 + CO2 % CO % CO2 % O2
Line A NA NA NA
Line B
POLLUTION C O N T R O L - EFFLUENTS
pH OIL Hg TDS TSS Color COD
Source 6AM 7PM (+ or -) ppb ppm mg/L Pt-Co Units mg/L
S-2 8.88 8.62 - NA NA NA NA NA
S-5 8.53 - NA NA NA NA NA
S-8 7.27 - NA NA 7 14 25
S-9 8.28 - NA NA 2 2 10
Lagoon NA NA NA NA NA NA NA
Source pH gpl NaOH Source pH SPECIFICATIONS
JBC NA S-3 NA pH = 6-9 COD = 100 mg/li, max Hg = 4 ppb, max.
Evap Canal S-4 Oil = Negative TDS = 1000 ppm, max TSS = 100 mg/li, max
Total Canal S-7 Color = 150 Pt-Co units, max.

NaOH- online(50%, 32%); SPB - NaCl; Depleted


Remarks:
IEM 1 : brine - NaCl, Free Cl2 Analyzed by Certified Correct
OFF-SPECS IEM 2 : None (Original copy signed) (Original copy signed)

Others : Instrument Air - dewpoint NEY/RGD OVA


MVC-QF-TECH-004 (13)
Effectivity Date: August 5, 2014

MABUHAY VINYL CORPORATION PRODUCT TRANSFER CLEARANCE


Assumption Heights, Iligan City

Date : 04/11/17 [ ] IEM 1 [ ] IEM 2 [ ] Mktg [ ] QC file


IEM 1
HYDROCHLORIC ACID LIQUID CAUSTIC SODA SODIUM HYPOCHLORITE
Tk # % HCl SG @ 30”C Color Tk # 50% 32%. Tk # % NaOCl % NaOH SG @ 30”C
1 NA A 49.67 NA 1 NA
2 NA B NA NA 2 NA
3 NA 3 NA
4 NA 6 7.68 0.68 1.132
5 NA 7 NA
IEM 2 SPECIFICATIONS
HYDROCHLORIC ACID LIQUID CAUSTIC SODA HYDROCHLORIC ACID
Tk # % HCl SG @ 30”C Color Tk # 50% 32%. % HCl 32.00 - 33.50
CTA 1 NA 9 NA - SG @ 30”C, min 1.152
CTA 2 NA 8 - 31.22 Color, max #3
CTA 3 NA LIQUID CAUSTIC SODA
CTB 1 NA 50% 32%
CTB 2 NA % NaOH 48.0-50.0 30.0 - 32.0
Remarks: % NaCl 0.10 0.10
WITHIN SPECS, OK for transfer ppm Fe, max 10 10
SODIUM HYPOCHLORITE
Analyzed by Certified Correct % NaOCl 7.40 - 8.00
(Original copy signed) (Original copy signed)
% excess NaOH 0.40 - 1.00
RGD OVA SG @ 30”C, min 1.108
MVC-QF-TECH-008(24) QUALITY CONTROL DAILY ANALYSIS REPORT
Effectivity Date: October 1, 2016 MABUHAY VINYL CORPORATION
Date : 04/12/17 Time : 11:30 AM [ ]QC [ ]Technical [ ]IEM1/IEM2 [ ]AVP-Mfg
IEM 1 IEM 2
50 % CAUSTIC SODA 50 % CAUSTIC SODA Specs
Online Tk – A Tk - B Online Tk - 9
% NaOH 48.77 NA NA NA NA 48.00-50.00
32 % CAUSTIC SODA 32 % CAUSTIC SODA
Online Tk – A Tk - B Online Tk - 8
% NaOH 30.29 NA NA 30.37 NA 30.00-32.00
HYDROCHLORIC ACID HYDROCHLORIC ACID
Online Tk- 3 Tk- Online CTB 1
% HCl 32.34 32.51 32.59 33.39 32.00-33.50
Color 1 1 1 1 # 3, max
POLISHED BRINE(After Precoat) POLISHED BRINE(After Precoat)
Ca+Mg, ppm + NA = + NA = 5.0 ppm,max.
SPB (After Headtank) SPB (After Headtank)
Ca+Mg, ppb 12 + nil = 12 nil + 10 = 10 20 ppb, max.
NaCl, gpl NA NA 290 gpl,min.
Na2SO4,gpl NA NA 7 gpl, max.
NaClO3,gpl NA NA 20 gpl,max.
DEPLETED BRINE DEPLETED BRINE
NaCl, gpl 183 184 200 gpl, min.
Free Cl2 negative negative Negative
NaClO3,gpl NA NA 20 gpl, max.
pH NA NA 2.0, max
S O D I U M H Y P O C H L O R I T E PLANT
Tank No. 1 2 3 6 7
% NaOCl NA NA NA 7.61 NA 7.40-8.00
% NaOH 0.70 0.40-1.00
Sp. Gravity 1.132 1.108, min
LI Q U I D C H LO R I N E PLAN T
Specs
Source LCP Tk.# Cl2 Feed LCP Tk # Cl2 Feed SULFURIC ACID
% Cl2 NA NA 99.5% min 91.0% min Source % H2SO4 Specs
% H2 NA NA NA NA LCP Comp. NA 97.0% min
UTILITIES
INSTRUMENT AIR @ 10 AM Specs BOILER WATER Specs
Dew Point, °C 5.6 ≤3.8 °C SiO2, ppm NA 150 ppm, max.
GAS ANALYSIS
IEM 1 IEM 2 FLUE GAS
% Cl2 % H2 O2 + CO2 % Cl2 % H2 O2 + CO2 % CO % CO2 % O2
Line A NA NA NA
Line B
POLLUTION C O N T R O L - EFFLUENTS
pH OIL Hg TDS TSS Color COD
Source 6AM 7PM (+ or -) ppb ppm mg/L Pt-Co Units mg/L
S-2 8.85 8.79 - 0.112 3800 5 35 NA
S-5 8.70 - 0.224 251 2 17 NA
S-8 7.23 - NA NA 7 8 NA
S-9 8.68 - NA NA 3 4 NA
Lagoon 8.28 - 0.056 280 5 30 NA
Source pH gpl NaOH Source pH SPECIFICATIONS
JBC 7.78 ND S-3 7.95 pH = 6-9 COD = 100 mg/li, max Hg = 4 ppb, max.
Evap Canal 2.12 ND S-4 .8.78 Oil = Negative TDS = 1000 ppm, max TSS = 100 mg/li, max
Total Canal 6.12 ND S-7 9.68 Color = 150 Pt-Co units, max.

Remarks: IEM 1 : Depleted brine - NaCl Analyzed by Certified Correct


OFF-SPECS IEM 2 : Depleted brine - NaCl (Original copy signed) (Original copy signed)

Others : Inst Air - dewpoint; Effluents -Evap canal, S7(pH), S2(TDS) NEY/ANB/RGD OVA
MVC-QF-TECH-004 (13)
Effectivity Date: August 5, 2014

MABUHAY VINYL CORPORATION PRODUCT TRANSFER CLEARANCE


Assumption Heights, Iligan City

Date : 04/12/17 [ ] IEM 1 [ ] IEM 2 [ ] Mktg [ ] QC file


IEM 1
HYDROCHLORIC ACID LIQUID CAUSTIC SODA SODIUM HYPOCHLORITE
Tk # % HCl SG @ 30”C Color Tk # 50% 32%. Tk # % NaOCl % NaOH SG @ 30”C
1 NA A NA NA 1 NA
2 NA B NA NA 2 NA
3 32.51 1.154 1 3 NA
4 NA 6 7.61 0.70 1.132
5 NA 7 NA
IEM 2 SPECIFICATIONS
HYDROCHLORIC ACID LIQUID CAUSTIC SODA HYDROCHLORIC ACID
Tk # % HCl SG @ 30”C Color Tk # 50% 32%. % HCl 32.00 - 33.50
CTA 1 NA 9 NA - SG @ 30”C, min 1.152
CTA 2 NA 8 - NA Color, max #3
CTA 3 NA LIQUID CAUSTIC SODA
CTB 1 33.39 1.160 1 50% 32%
CTB 2 NA % NaOH 48.0-50.0 30.0 - 32.0
Remarks: % NaCl 0.10 0.10
WITHIN SPECS, OK for transfer ppm Fe, max 10 10
SODIUM HYPOCHLORITE
Analyzed by Certified Correct % NaOCl 7.40 - 8.00
(Original copy signed) (Original copy signed)
% excess NaOH 0.40 - 1.00
ANB OVA SG @ 30”C, min 1.108
MVC-QF-TECH-008(24) QUALITY CONTROL DAILY ANALYSIS REPORT
Effectivity Date: October 1, 2016 MABUHAY VINYL CORPORATION
Date : 04/13/17 Time : 11:30 AM [ ]QC [ ]Technical [ ]IEM1/IEM2 [ ]AVP-Mfg
IEM 1 IEM 2
50 % CAUSTIC SODA 50 % CAUSTIC SODA Specs
Online Tk – A Tk - B Online Tk - 9
% NaOH 49.38 NA NA SD SD 48.00-50.00
32 % CAUSTIC SODA 32 % CAUSTIC SODA
Online Tk – A Tk - B Online Tk - 8
% NaOH 29.66 NA NA 30.52 30.41 30.00-32.00
HYDROCHLORIC ACID HYDROCHLORIC ACID
Online Tk- 5 Tk- Online CTB 2
% HCl NA 32.16 33.19 33.38 32.00-33.50
Color 1 1 1 # 3, max
POLISHED BRINE(After Precoat) POLISHED BRINE(After Precoat)
Ca+Mg, ppm 2.67 + nil = 2.67 1.78 + nil = 1.78 5.0 ppm,max.
SPB (After Headtank) SPB (After Headtank)
Ca+Mg, ppb 28 + 2 = 30 nil + 2 = 2 20 ppb, max.
NaCl, gpl 264 314 290 gpl,min.
Na2SO4,gpl 2.22 4.14 7 gpl, max.
NaClO3,gpl 4.82 18.84 20 gpl,max.
DEPLETED BRINE DEPLETED BRINE
NaCl, gpl 183 215 200 gpl, min.
Free Cl2 negative negative Negative
NaClO3,gpl 8.33 29.36 20 gpl, max.
pH NA NA 2.0, max
S O D I U M H Y P O C H L O R I T E PLANT
Tank No. 1 2 3 6 7
% NaOCl NA NA NA NA 7.80 7.40-8.00
% NaOH 0.64 0.40-1.00
Sp. Gravity 1.140 1.108, min
LI Q U I D C H LO R I N E PLAN T
Specs
Source LCP Tk.# Cl2 Feed LCP Tk # Cl2 Feed SULFURIC ACID
% Cl2 NA NA 99.5% min 91.0% min Source % H2SO4 Specs
% H2 NA NA NA NA LCP Comp. NA 97.0% min
UTILITIES
INSTRUMENT AIR @ 1130 AM Specs BOILER WATER Specs
Dew Point, °C 8.6 ≤3.8 °C SiO2, ppm NA 150 ppm, max.
GAS ANALYSIS
IEM 1 IEM 2 FLUE GAS
% Cl2 % H2 O2 + CO2 % Cl2 % H2 O2 + CO2 % CO % CO2 % O2
Line A NA NA NA
Line B
POLLUTION C O N T R O L - EFFLUENTS
pH OIL Hg TDS TSS Color COD
Source 6AM 7PM (+ or -) ppb ppm mg/L Pt-Co Units mg/L
S-2 8.70 8.65 - NA NA NA NA NA
S-5 8.63 - NA NA NA NA NA
S-8 NA - NA NA NA NA NA
S-9 NA - NA NA NA NA NA
Lagoon NA NA NA NA NA NA NA
Source pH gpl NaOH Source pH SPECIFICATIONS
JBC NA S-3 NA pH = 6-9 COD = 100 mg/li, max Hg = 4 ppb, max.
Evap Canal S-4 Oil = Negative TDS = 1000 ppm, max TSS = 100 mg/li, max
Total Canal S-7 Color = 150 Pt-Co units, max.

Remarks: IEM 1 : NaOH- online(32%); SPB - Ca+Mg, NaCl; Depleted brine - NaCl
Analyzed by Certified Correct
OFF-SPECS IEM 2 : Depleted brine - NaClO3 (Original copy signed) (Original copy signed)

Others : Instrument Air - dewpoint ANB/RGD OVA


MVC-QF-TECH-004 (13)
Effectivity Date: August 5, 2014

MABUHAY VINYL CORPORATION PRODUCT TRANSFER CLEARANCE


Assumption Heights, Iligan City

Date : 04/13/17 [ ] IEM 1 [ ] IEM 2 [ ] Mktg [ ] QC file


IEM 1
HYDROCHLORIC ACID LIQUID CAUSTIC SODA SODIUM HYPOCHLORITE
Tk # % HCl SG @ 30”C Color Tk # 50% 32%. Tk # % NaOCl % NaOH SG @ 30”C
1 NA A NA NA 1 NA
2 NA B NA NA 2 NA
3 NA 3 NA
4 NA 6 NA
5 32.16 1.152 1 7 7.80 0.64 1.140
IEM 2 SPECIFICATIONS
HYDROCHLORIC ACID LIQUID CAUSTIC SODA HYDROCHLORIC ACID
Tk # % HCl SG @ 30”C Color Tk # 50% 32%. % HCl 32.00 - 33.50
CTA 1 NA 9 SD - SG @ 30”C, min 1.152
CTA 2 NA 8 - 30.41 Color, max #3
CTA 3 NA LIQUID CAUSTIC SODA
CTB 1 NA 50% 32%
CTB 2 33.38 1.160 1 % NaOH 48.0-50.0 30.0 - 32.0
Remarks: % NaCl 0.10 0.10
WITHIN SPECS, OK for transfer ppm Fe, max 10 10
SODIUM HYPOCHLORITE
Analyzed by Certified Correct % NaOCl 7.40 - 8.00
(Original copy signed) (Original copy signed)
% excess NaOH 0.40 - 1.00
ANB OVA SG @ 30”C, min 1.108
MVC-QF-TECH-008(24) QUALITY CONTROL DAILY ANALYSIS REPORT
Effectivity Date: October 1, 2016 MABUHAY VINYL CORPORATION
Date : 04/14/17 Time : 11:35 AM [ ]QC [ ]Technical [ ]IEM1/IEM2 [ ]AVP-Mfg
IEM 1 IEM 2
50 % CAUSTIC SODA 50 % CAUSTIC SODA Specs
Online Tk – A Tk - B Online Tk - 9
% NaOH 50.14 49.66 NA 50.27 NA 48.00-50.00
32 % CAUSTIC SODA 32 % CAUSTIC SODA
Online Tk – A Tk - B Online Tk - 8
% NaOH 29.88 NA NA 31.27 NA 30.00-32.00
HYDROCHLORIC ACID HYDROCHLORIC ACID
Online Tk- Tk- Online CTA 1
% HCl NA 33.56 33.84 32.00-33.50
Color 1 1 # 3, max
POLISHED BRINE(After Precoat) POLISHED BRINE(After Precoat)
Ca+Mg, ppm + NA = + NA = 5.0 ppm,max.
SPB (After Headtank) SPB (After Headtank)
Ca+Mg, ppb NA NA 20 ppb, max.
NaCl, gpl 290 gpl,min.
Na2SO4,gpl 7 gpl, max.
NaClO3,gpl 20 gpl,max.
DEPLETED BRINE DEPLETED BRINE
NaCl, gpl NA NA 200 gpl, min.
Free Cl2 Negative
NaClO3,gpl 20 gpl, max.
pH 2.0, max
S O D I U M H Y P O C H L O R I T E PLANT
Tank No. 1 2 3 6 7
% NaOCl NA NA NA NA NA 7.40-8.00
% NaOH 0.40-1.00
Sp. Gravity 1.108, min
LI Q U I D C H LO R I N E PLAN T
Specs
Source LCP Tk.# Cl2 Feed LCP Tk # Cl2 Feed SULFURIC ACID
% Cl2 NA NA 99.5% min 91.0% min Source % H2SO4 Specs
% H2 NA NA NA NA LCP Comp. NA 97.0% min
UTILITIES
INSTRUMENT AIR @ AM Specs BOILER WATER Specs
Dew Point, °C NA ≤3.8 °C SiO2, ppm NA 150 ppm, max.
GAS ANALYSIS
IEM 1 IEM 2 FLUE GAS
% Cl2 % H2 O2 + CO2 % Cl2 % H2 O2 + CO2 % CO % CO2 % O2
Line A NA NA NA
Line B
POLLUTION C O N T R O L - EFFLUENTS
pH OIL Hg TDS TSS Color COD
Source 6AM 7PM (+ or -) ppb ppm mg/L Pt-Co Units mg/L
S-2 NA - NA NA NA NA NA
S-5 NA - NA NA NA NA NA
S-8 NA - NA NA NA NA NA
S-9 NA - NA NA NA NA NA
Lagoon NA NA NA NA NA NA NA
Source pH gpl NaOH Source pH SPECIFICATIONS
JBC NA S-3 NA pH = 6-9 COD = 100 mg/li, max Hg = 4 ppb, max.
Evap Canal S-4 Oil = Negative TDS = 1000 ppm, max TSS = 100 mg/li, max
Total Canal S-7 Color = 150 Pt-Co units, max.

Remarks: IEM 1 : NaOH- online(50%, 32%) Analyzed by Certified Correct


OFF-SPECS IEM 2 : NaOH - online(50%); HCl - online, CTA1 (Original copy signed) (Original copy signed)

Others : None ANB OVA


MVC-QF-TECH-004 (13)
Effectivity Date: August 5, 2014

MABUHAY VINYL CORPORATION PRODUCT TRANSFER CLEARANCE


Assumption Heights, Iligan City

Date : 04/14/17 [ ] IEM 1 [ ] IEM 2 [ ] Mktg [ ] QC file


IEM 1
HYDROCHLORIC ACID LIQUID CAUSTIC SODA SODIUM HYPOCHLORITE
Tk # % HCl SG @ 30”C Color Tk # 50% 32%. Tk # % NaOCl % NaOH SG @ 30”C
1 NA A 49.66 NA 1 NA
2 NA B NA NA 2 NA
3 NA 3 NA
4 NA 6 NA
5 NA 7 NA
IEM 2 SPECIFICATIONS
HYDROCHLORIC ACID LIQUID CAUSTIC SODA HYDROCHLORIC ACID
Tk # % HCl SG @ 30”C Color Tk # 50% 32%. % HCl 32.00 - 33.50
CTA 1 NA 9 NA - SG @ 30”C, min 1.152
CTA 2 NA 8 - NA Color, max #3
CTA 3 NA LIQUID CAUSTIC SODA
CTB 1 NA 50% 32%
CTB 2 NA % NaOH 48.0-50.0 30.0 - 32.0
Remarks: % NaCl 0.10 0.10
WITHIN SPECS, OK for transfer ppm Fe, max 10 10
SODIUM HYPOCHLORITE
Analyzed by Certified Correct % NaOCl 7.40 - 8.00
(Original copy signed) (Original copy signed)
% excess NaOH 0.40 - 1.00
ANB OVA SG @ 30”C, min 1.108
MVC-QF-TECH-008(24) QUALITY CONTROL DAILY ANALYSIS REPORT
Effectivity Date: October 1, 2016 MABUHAY VINYL CORPORATION
Date : 04/15/17 Time : 11:30 AM [ ]QC [ ]Technical [ ]IEM1/IEM2 [ ]AVP-Mfg
IEM 1 IEM 2
50 % CAUSTIC SODA 50 % CAUSTIC SODA Specs
Online Tk – A Tk - B Online Tk - 9
% NaOH 49.70 49.63 NA SD NA 48.00-50.00
32 % CAUSTIC SODA 32 % CAUSTIC SODA
Online Tk – A Tk - B Online Tk - 8
% NaOH 30.59 NA NA 31.01 NA 30.00-32.00
HYDROCHLORIC ACID HYDROCHLORIC ACID
Online Tk- Tk- Online CTA 3 CTB 1
% HCl NA 33.87 33.45 33.13 32.00-33.50
Color 1 1 2 # 3, max
POLISHED BRINE(After Precoat) POLISHED BRINE(After Precoat)
Ca+Mg, ppm + NA = + NA = 5.0 ppm,max.
SPB (After Headtank) SPB (After Headtank)
Ca+Mg, ppb 36 + nil = 36 nil + 2 = 2 20 ppb, max.
NaCl, gpl NA NA 290 gpl,min.
Na2SO4,gpl NA NA 7 gpl, max.
NaClO3,gpl NA NA 20 gpl,max.
DEPLETED BRINE DEPLETED BRINE
NaCl, gpl 188 244 200 gpl, min.
Free Cl2 negative negative Negative
NaClO3,gpl NA NA 20 gpl, max.
pH NA NA 2.0, max
S O D I U M H Y P O C H L O R I T E PLANT
Tank No. 1 2 3 6 7
% NaOCl NA NA NA 7.56 7.77 7.40-8.00
% NaOH 0.60 0.53 0.40-1.00
Sp. Gravity 1.134 1.138 1.108, min
LI Q U I D C H LO R I N E PLAN T
Specs
Source LCP Tk.# Cl2 Feed LCP Tk # Cl2 Feed SULFURIC ACID
% Cl2 NA NA 99.5% min 91.0% min Source % H2SO4 Specs
% H2 NA NA NA NA LCP Comp. NA 97.0% min
UTILITIES
INSTRUMENT AIR @ 1030 AM Specs BOILER WATER Specs
Dew Point, °C 7.1 ≤3.8 °C SiO2, ppm NA 150 ppm, max.
GAS ANALYSIS
IEM 1 IEM 2 FLUE GAS
% Cl2 % H2 O2 + CO2 % Cl2 % H2 O2 + CO2 % CO % CO2 % O2
Line A NA NA NA
Line B
POLLUTION C O N T R O L - EFFLUENTS
pH OIL Hg TDS TSS Color COD
Source 6AM 7PM (+ or -) ppb ppm mg/L Pt-Co Units mg/L
S-2 8.58 8.63 - NA NA NA NA NA
S-5 8.67 - NA NA NA NA NA
S-8 7.50 - NA NA 2 14 NA
S-9 8.77 - NA NA 4 12 NA
Lagoon NA NA NA NA NA NA NA
Source pH gpl NaOH Source pH SPECIFICATIONS
JBC NA S-3 NA pH = 6-9 COD = 100 mg/li, max Hg = 4 ppb, max.
Evap Canal S-4 Oil = Negative TDS = 1000 ppm, max TSS = 100 mg/li, max
Total Canal S-7 Color = 150 Pt-Co units, max.

Remarks: IEM 1 : SPB - Ca+Mg; Depleted brine - NaCl Analyzed by Certified Correct
OFF-SPECS IEM 2 : HCl - online (Original copy signed) (Original copy signed)

Others : Instrument Air - dewpoint ANB/RGD OVA


MVC-QF-TECH-004 (13)
Effectivity Date: August 5, 2014

MABUHAY VINYL CORPORATION PRODUCT TRANSFER CLEARANCE


Assumption Heights, Iligan City

Date : 04/15/17 [ ] IEM 1 [ ] IEM 2 [ ] Mktg [ ] QC file


IEM 1
HYDROCHLORIC ACID LIQUID CAUSTIC SODA SODIUM HYPOCHLORITE
Tk # % HCl SG @ 30”C Color Tk # 50% 32%. Tk # % NaOCl % NaOH SG @ 30”C
1 NA A 49.63 NA 1 NA
2 NA B NA NA 2 NA
3 NA 3 NA
4 NA 6 7.56 0.60 1.134
5 NA 7 7.77 0.53 1.138
IEM 2 SPECIFICATIONS
HYDROCHLORIC ACID LIQUID CAUSTIC SODA HYDROCHLORIC ACID
Tk # % HCl SG @ 30”C Color Tk # 50% 32%. % HCl 32.00 - 33.50
CTA 1 NA 9 NA - SG @ 30”C, min 1.152
CTA 2 NA 8 - NA Color, max #3
CTA 3 33.45 1.160 1 LIQUID CAUSTIC SODA
CTB 1 33.13 1.160 2 50% 32%
CTB 2 NA % NaOH 48.0-50.0 30.0 - 32.0
Remarks: % NaCl 0.10 0.10
WITHIN SPECS, OK for transfer ppm Fe, max 10 10
SODIUM HYPOCHLORITE
Analyzed by Certified Correct % NaOCl 7.40 - 8.00
(Original copy signed) (Original copy signed)
% excess NaOH 0.40 - 1.00
ANB OVA SG @ 30”C, min 1.108
MVC-QF-TECH-008(24) QUALITY CONTROL DAILY ANALYSIS REPORT
Effectivity Date: October 1, 2016 MABUHAY VINYL CORPORATION
Date : 04/16/17 Time : 11:30 AM [ ]QC [ ]Technical [ ]IEM1/IEM2 [ ]AVP-Mfg
IEM 1 IEM 2
50 % CAUSTIC SODA 50 % CAUSTIC SODA Specs
Online Tk – A Tk - B Online Tk - 9
% NaOH 48.49 49.40 NA SD 48.67 48.00-50.00
32 % CAUSTIC SODA 32 % CAUSTIC SODA
Online Tk – A Tk - B Online Tk - 8
% NaOH 30.13 NA NA 30.76 NA 30.00-32.00
HYDROCHLORIC ACID HYDROCHLORIC ACID
Online Tk- Tk- Online CTA 2
% HCl NA 33.73 33.45 32.00-33.50
Color 1 1 # 3, max
POLISHED BRINE(After Precoat) POLISHED BRINE(After Precoat)
Ca+Mg, ppm + NA = + NA = 5.0 ppm,max.
SPB (After Headtank) SPB (After Headtank)
Ca+Mg, ppb NA NA 20 ppb, max.
NaCl, gpl 290 gpl,min.
Na2SO4,gpl 7 gpl, max.
NaClO3,gpl 20 gpl,max.
DEPLETED BRINE DEPLETED BRINE
NaCl, gpl NA NA 200 gpl, min.
Free Cl2 Negative
NaClO3,gpl 20 gpl, max.
pH 2.0, max
S O D I U M H Y P O C H L O R I T E PLANT
Tank No. 1 2 3 6 7
% NaOCl NA NA NA 7.45 NA 7.40-8.00
% NaOH 0.72 0.40-1.00
Sp. Gravity 1.134 1.108, min
LI Q U I D C H LO R I N E PLAN T
Specs
Source LCP Tk.# Cl2 Feed LCP Tk # Cl2 Feed SULFURIC ACID
% Cl2 NA NA 99.5% min 91.0% min Source % H2SO4 Specs
% H2 NA NA NA NA LCP Comp. NA 97.0% min
UTILITIES
INSTRUMENT AIR @ AM Specs BOILER WATER Specs
Dew Point, °C NA ≤3.8 °C SiO2, ppm NA 150 ppm, max.
GAS ANALYSIS
IEM 1 IEM 2 FLUE GAS
% Cl2 % H2 O2 + CO2 % Cl2 % H2 O2 + CO2 % CO % CO2 % O2
Line A NA NA NA
Line B
POLLUTION C O N T R O L - EFFLUENTS
pH OIL Hg TDS TSS Color COD
Source 6AM 7PM (+ or -) ppb ppm mg/L Pt-Co Units mg/L
S-2 NA - NA NA NA NA NA
S-5 NA - NA NA NA NA NA
S-8 NA - NA NA NA NA NA
S-9 NA - NA NA NA NA NA
Lagoon NA NA NA NA NA NA NA
Source pH gpl NaOH Source pH SPECIFICATIONS
JBC NA S-3 NA pH = 6-9 COD = 100 mg/li, max Hg = 4 ppb, max.
Evap Canal S-4 Oil = Negative TDS = 1000 ppm, max TSS = 100 mg/li, max
Total Canal S-7 Color = 150 Pt-Co units, max.

Remarks: IEM 1 : None Analyzed by Certified Correct


OFF-SPECS IEM 2 : HCl - online (Original copy signed) (Original copy signed)

Others : None ANB OVA


MVC-QF-TECH-004 (13)
Effectivity Date: August 5, 2014

MABUHAY VINYL CORPORATION PRODUCT TRANSFER CLEARANCE


Assumption Heights, Iligan City

Date : 04/16/17 [ ] IEM 1 [ ] IEM 2 [ ] Mktg [ ] QC file


IEM 1
HYDROCHLORIC ACID LIQUID CAUSTIC SODA SODIUM HYPOCHLORITE
Tk # % HCl SG @ 30”C Color Tk # 50% 32%. Tk # % NaOCl % NaOH SG @ 30”C
1 NA A 49.40 NA 1 NA
2 NA B NA NA 2 NA
3 NA 3 NA
4 NA 6 7.45 0.72 1.134
5 NA 7 NA
IEM 2 SPECIFICATIONS
HYDROCHLORIC ACID LIQUID CAUSTIC SODA HYDROCHLORIC ACID
Tk # % HCl SG @ 30”C Color Tk # 50% 32%. % HCl 32.00 - 33.50
CTA 1 NA 9 48.67 - SG @ 30”C, min 1.152
CTA 2 33.45 1.160 1 8 - NA Color, max #3
CTA 3 NA LIQUID CAUSTIC SODA
CTB 1 NA 50% 32%
CTB 2 NA % NaOH 48.0-50.0 30.0 - 32.0
Remarks: % NaCl 0.10 0.10
WITHIN SPECS, OK for transfer ppm Fe, max 10 10
SODIUM HYPOCHLORITE
Analyzed by Certified Correct % NaOCl 7.40 - 8.00
(Original copy signed) (Original copy signed)
% excess NaOH 0.40 - 1.00
ANB OVA SG @ 30”C, min 1.108
MVC-QF-TECH-008(24) QUALITY CONTROL DAILY ANALYSIS REPORT
Effectivity Date: October 1, 2016 MABUHAY VINYL CORPORATION
Date : 04/17/17 Time : 11:30 AM [ ]QC [ ]Technical [ ]IEM1/IEM2 [ ]AVP-Mfg
IEM 1 IEM 2
50 % CAUSTIC SODA 50 % CAUSTIC SODA Specs
Online Tk – A Tk - B Online Tk - 9
% NaOH 49.94 49.37 NA 48.44 48.44 48.00-50.00
32 % CAUSTIC SODA 32 % CAUSTIC SODA
Online Tk – A Tk - B Online Tk - 8
% NaOH 29.45 NA NA 30.64 NA 30.00-32.00
HYDROCHLORIC ACID HYDROCHLORIC ACID
Online Tk- Tk- Online CTA 3 CTB 2
% HCl NA 32.07 33.19 32.67 32.00-33.50
Color 1 1 1 # 3, max
POLISHED BRINE(After Precoat) POLISHED BRINE(After Precoat)
Ca+Mg, ppm 2.67 + nil = 2.67 7.12 + nil = 7.12 5.0 ppm,max.
SPB (After Headtank) SPB (After Headtank)
Ca+Mg, ppb 12 + nil = 12 nil + nil = nil 20 ppb, max.
NaCl, gpl 281 306 290 gpl,min.
Na2SO4,gpl 2.52 4.14 7 gpl, max.
NaClO3,gpl 4.38 18.49 20 gpl,max.
DEPLETED BRINE DEPLETED BRINE
NaCl, gpl 182 211 200 gpl, min.
Free Cl2 negative negative Negative
NaClO3,gpl 9.46 28.39 20 gpl, max.
pH NA 2.11 2.0, max
S O D I U M H Y P O C H L O R I T E PLANT
Tank No. 1 2 3 6 7
% NaOCl NA NA NA NA 7.96 7.40-8.00
% NaOH 0.74 0.40-1.00
Sp. Gravity 1.138 1.108, min
LI Q U I D C H LO R I N E PLAN T
Specs
Source LCP Tk.# Cl2 Feed LCP Tk # Cl2 Feed SULFURIC ACID
% Cl2 NA NA 99.5% min 91.0% min Source % H2SO4 Specs
% H2 NA NA NA NA LCP Comp. 97.22 97.0% min
UTILITIES
INSTRUMENT AIR @ 10:05 AM Specs BOILER WATER Specs
Dew Point, °C 6.5 ≤3.8 °C SiO2, ppm NA 150 ppm, max.
GAS ANALYSIS
IEM 1 IEM 2 FLUE GAS
% Cl2 % H2 O2 + CO2 % Cl2 % H2 O2 + CO2 % CO % CO2 % O2
Line A NA NA NA
Line B
POLLUTION C O N T R O L - EFFLUENTS
pH OIL Hg TDS TSS Color COD
Source 6AM 7PM (+ or -) ppb ppm mg/L Pt-Co Units mg/L
S-2 8.78 8.71 - NA NA NA NA NA
S-5 8.65 - NA NA NA NA NA
S-8 7.49 - NA NA 12 16 15
S-9 8.44 - NA NA 5 6 4
Lagoon NA NA NA NA NA NA NA
Source pH gpl NaOH Source pH SPECIFICATIONS
JBC NA S-3 NA pH = 6-9 COD = 100 mg/li, max Hg = 4 ppb, max.
Evap Canal S-4 Oil = Negative TDS = 1000 ppm, max TSS = 100 mg/li, max
Total Canal S-7 Color = 150 Pt-Co units, max.

Remarks: IEM 1 : NaOH- online(32%); SPB, Depleted brine - NaCl Analyzed by Certified Correct
OFF-SPECS IEM 2 : Polished brine - Ca+Mg; Depleted brine - pH, NaClO3 (Original copy signed) (Original copy signed)

Others : Instrument Air - dewpoint NEY/ANB OVA


MVC-QF-TECH-004 (13)
Effectivity Date: August 5, 2014

MABUHAY VINYL CORPORATION PRODUCT TRANSFER CLEARANCE


Assumption Heights, Iligan City

Date : 04/17/17 [ ] IEM 1 [ ] IEM 2 [ ] Mktg [ ] QC file


IEM 1
HYDROCHLORIC ACID LIQUID CAUSTIC SODA SODIUM HYPOCHLORITE
Tk # % HCl SG @ 30”C Color Tk # 50% 32%. Tk # % NaOCl % NaOH SG @ 30”C
1 NA A 49.37 NA 1 NA
2 NA B NA NA 2 NA
3 NA 3 NA
4 NA 6 NA
5 NA 7 7.96 0.74 1.138
IEM 2 SPECIFICATIONS
HYDROCHLORIC ACID LIQUID CAUSTIC SODA HYDROCHLORIC ACID
Tk # % HCl SG @ 30”C Color Tk # 50% 32%. % HCl 32.00 - 33.50
CTA 1 NA 9 48.44 - SG @ 30”C, min 1.152
CTA 2 NA 8 - NA Color, max #3
CTA 3 33.19 1.160 1 LIQUID CAUSTIC SODA
CTB 1 NA 50% 32%
CTB 2 32.67 1.154 1 % NaOH 48.0-50.0 30.0 - 32.0
Remarks: % NaCl 0.10 0.10
WITHIN SPECS, OK for transfer ppm Fe, max 10 10
SODIUM HYPOCHLORITE
Analyzed by Certified Correct % NaOCl 7.40 - 8.00
(Original copy signed) (Original copy signed)
% excess NaOH 0.40 - 1.00
ANB OVA SG @ 30”C, min 1.108
MVC-QF-TECH-008(24) QUALITY CONTROL DAILY ANALYSIS REPORT
Effectivity Date: October 1, 2016 MABUHAY VINYL CORPORATION
Date : 04/18/17 Time : 11:30 AM [ ]QC [ ]Technical [ ]IEM1/IEM2 [ ]AVP-Mfg
IEM 1 IEM 2
50 % CAUSTIC SODA 50 % CAUSTIC SODA Specs
Online Tk – A Tk - B Online Tk - 9
% NaOH SD 48.28 NA 48.00-50.00
32 % CAUSTIC SODA 32 % CAUSTIC SODA
Online Tk – A Tk - B Online Tk - 8
% NaOH SD 30.76 30.68 30.00-32.00
HYDROCHLORIC ACID HYDROCHLORIC ACID
Online Tk- Tk- Online CTB-1
% HCl SD 32.86 33.16 32.00-33.50
Color 1 1 # 3, max
POLISHED BRINE(After Precoat) POLISHED BRINE(After Precoat)
Ca+Mg, ppm + NA = + NA = 5.0 ppm,max.
SPB (After Headtank) SPB (After Headtank)
Ca+Mg, ppb SD 4 + nil = 4 20 ppb, max.
NaCl, gpl NA 290 gpl,min.
Na2SO4,gpl NA 7 gpl, max.
NaClO3,gpl NA 20 gpl,max.
DEPLETED BRINE DEPLETED BRINE
NaCl, gpl SD 212 200 gpl, min.
Free Cl2 negative Negative
NaClO3,gpl NA 20 gpl, max.
pH NA 2.0, max
S O D I U M H Y P O C H L O R I T E PLANT
Tank No. 1 2 3 6 7
% NaOCl NA NA NA 7.68 NA 7.40-8.00
% NaOH 0.79 0.40-1.00
Sp. Gravity 1.136 1.108, min
LI Q U I D C H LO R I N E PLAN T
Specs
Source LCP Tk.# Cl2 Feed LCP Tk # Cl2 Feed SULFURIC ACID
% Cl2 NA NA 99.5% min 91.0% min Source % H2SO4 Specs
% H2 NA NA NA NA LCP Comp. NA 97.0% min
UTILITIES
INSTRUMENT AIR @ 10:30 AM Specs BOILER WATER Specs
Dew Point, °C 6.5 ≤3.8 °C SiO2, ppm NA 150 ppm, max.
GAS ANALYSIS
IEM 1 IEM 2 FLUE GAS
% Cl2 % H2 O2 + CO2 % Cl2 % H2 O2 + CO2 % CO % CO2 % O2
Line A NA NA NA
Line B
POLLUTION C O N T R O L - EFFLUENTS
pH OIL Hg TDS TSS Color COD
Source 6AM 7PM (+ or -) ppb ppm mg/L Pt-Co Units mg/L
S-2 8.60 8.57 - NA NA NA NA NA
S-5 8.62 - NA NA NA NA NA
S-8 7.57 - NA NA 5 15 NA
S-9 8.26 - NA NA 3 15 NA
Lagoon NA NA NA NA NA NA NA
Source pH gpl NaOH Source pH SPECIFICATIONS
JBC NA S-3 NA pH = 6-9 COD = 100 mg/li, max Hg = 4 ppb, max.
Evap Canal S-4 Oil = Negative TDS = 1000 ppm, max TSS = 100 mg/li, max
Total Canal S-7 Color = 150 Pt-Co units, max.

Remarks: IEM 1 : None Analyzed by Certified Correct


OFF-SPECS IEM 2 : None (Original copy signed) (Original copy signed)

Others : Instrument Air - dewpoint NEY/ANB OVA


MVC-QF-TECH-004 (13)
Effectivity Date: August 5, 2014

MABUHAY VINYL CORPORATION PRODUCT TRANSFER CLEARANCE


Assumption Heights, Iligan City

Date : 04/18/17 [ ] IEM 1 [ ] IEM 2 [ ] Mktg [ ] QC file


IEM 1
HYDROCHLORIC ACID LIQUID CAUSTIC SODA SODIUM HYPOCHLORITE
Tk # % HCl SG @ 30”C Color Tk # 50% 32%. Tk # % NaOCl % NaOH SG @ 30”C
1 NA A 1 NA
2 NA B 2 NA
3 NA 3 NA
4 NA 6 7.68 0.79 1.136
5 NA 7 NA
IEM 2 SPECIFICATIONS
HYDROCHLORIC ACID LIQUID CAUSTIC SODA HYDROCHLORIC ACID
Tk # % HCl SG @ 30”C Color Tk # 50% 32%. % HCl 32.00 - 33.50
CTA 1 NA 9 NA - SG @ 30”C, min 1.152
CTA 2 NA 8 - 30.68 Color, max #3
CTA 3 NA LIQUID CAUSTIC SODA
CTB 1 33.16 1.160 1 50% 32%
CTB 2 NA % NaOH 48.0-50.0 30.0 - 32.0
Remarks: % NaCl 0.10 0.10
WITHIN SPECS, OK for transfer ppm Fe, max 10 10
SODIUM HYPOCHLORITE
Analyzed by Certified Correct % NaOCl 7.40 - 8.00
(Original copy signed) (Original copy signed)
% excess NaOH 0.40 - 1.00
ANB OVA SG @ 30”C, min 1.108
MVC-QF-TECH-008(24) QUALITY CONTROL DAILY ANALYSIS REPORT
Effectivity Date: October 1, 2016 MABUHAY VINYL CORPORATION
Date : 04/19/17 Time : 11:30 AM [ ]QC [ ]Technical [ ]IEM1/IEM2 [ ]AVP-Mfg
IEM 1 IEM 2
50 % CAUSTIC SODA 50 % CAUSTIC SODA Specs
Online Tk – A Tk - B Online Tk - 9
% NaOH NA NA NA 48.00-50.00
32 % CAUSTIC SODA 32 % CAUSTIC SODA
Online Tk – A Tk - B Online Tk - 8
% NaOH NA NA NA 30.00-32.00
HYDROCHLORIC ACID HYDROCHLORIC ACID
Online Tk- Tk- Online CTA 2
% HCl NA 32.00-33.50
Color # 3, max
POLISHED BRINE(After Precoat) POLISHED BRINE(After Precoat)
Ca+Mg, ppm + NA = + NA = 5.0 ppm,max.
SPB (After Headtank) SPB (After Headtank)
Ca+Mg, ppb nil + nil = nil nil + nil = nil 20 ppb, max.
NaCl, gpl NA NA 290 gpl,min.
Na2SO4,gpl NA NA 7 gpl, max.
NaClO3,gpl NA NA 20 gpl,max.
DEPLETED BRINE DEPLETED BRINE
NaCl, gpl 200 gpl, min.
Free Cl2 negative negative Negative
NaClO3,gpl NA NA 20 gpl, max.
pH NA NA 2.0, max
S O D I U M H Y P O C H L O R I T E PLANT
Tank No. 1 2 3 6 7
% NaOCl NA NA NA NA NA 7.40-8.00
% NaOH 0.40-1.00
Sp. Gravity 1.108, min
LI Q U I D C H LO R I N E PLAN T
Specs
Source LCP Tk.# Cl2 Feed LCP Tk # Cl2 Feed SULFURIC ACID
% Cl2 NA NA 99.5% min 91.0% min Source % H2SO4 Specs
% H2 NA NA NA NA LCP Comp. NA 97.0% min
UTILITIES
INSTRUMENT AIR @ AM Specs BOILER WATER Specs
Dew Point, °C ≤3.8 °C SiO2, ppm NA 150 ppm, max.
GAS ANALYSIS
IEM 1 IEM 2 FLUE GAS
% Cl2 % H2 O2 + CO2 % Cl2 % H2 O2 + CO2 % CO % CO2 % O2
Line A NA NA NA
Line B
POLLUTION C O N T R O L - EFFLUENTS
pH OIL Hg TDS TSS Color COD
Source 6AM 7PM (+ or -) ppb ppm mg/L Pt-Co Units mg/L
S-2 - NA NA NA NA NA
S-5 NA - NA NA NA NA NA
S-8 NA - NA NA NA NA NA
S-9 NA - NA NA NA NA NA
Lagoon NA NA NA NA NA NA NA
Source pH gpl NaOH Source pH SPECIFICATIONS
JBC NA S-3 NA pH = 6-9 COD = 100 mg/li, max Hg = 4 ppb, max.
Evap Canal S-4 Oil = Negative TDS = 1000 ppm, max TSS = 100 mg/li, max
Total Canal S-7 Color = 150 Pt-Co units, max.

Remarks: IEM 1 : NaOH- online(50%); SPB - Ca+Mg, NaCl; Depleted brine - Free
Analyzed
Cl2 by Certified Correct
OFF-SPECS IEM 2 : SPB - Ca+Mg, Na2SO4; Depleted brine - Free Cl2, NaClO3 (Original copy signed) (Original copy signed)

Others : Instrument Air - dewpoint; Effluents - S8(pH), S9(Color) NEY/ANB/RGD OVA


MVC-QF-TECH-004 (13)
Effectivity Date: August 5, 2014

MABUHAY VINYL CORPORATION PRODUCT TRANSFER CLEARANCE


Assumption Heights, Iligan City

Date : 04/19/17 [ ] IEM 1 [ ] IEM 2 [ ] Mktg [ ] QC file


IEM 1
HYDROCHLORIC ACID LIQUID CAUSTIC SODA SODIUM HYPOCHLORITE
Tk # % HCl SG @ 30”C Color Tk # 50% 32%. Tk # % NaOCl % NaOH SG @ 30”C
1 NA A NA NA 1 NA 0.00 0.000
2 NA B NA NA 2 NA 0.00 0.000
3 NA 3 NA 0.00 0.000
4 NA 6 NA 0.00 0.000
5 NA 7 NA 0.00 0.000
IEM 2 SPECIFICATIONS
HYDROCHLORIC ACID LIQUID CAUSTIC SODA HYDROCHLORIC ACID
Tk # % HCl SG @ 30”C Color Tk # 50% 32%. % HCl 32.00 - 33.50
CTA 1 NA 9 NA - SG @ 30”C, min 1.152
CTA 2 NA 8 - NA Color, max #3
CTA 3 NA LIQUID CAUSTIC SODA
CTB 1 NA 50% 32%
CTB 2 NA % NaOH 48.0-50.0 30.0 - 32.0
Remarks: % NaCl 0.10 0.10
WITHIN SPECS, OK for transfer ppm Fe, max 10 10
SODIUM HYPOCHLORITE
Analyzed by Certified Correct % NaOCl 7.40 - 8.00
(Original copy signed) (Original copy signed)
% excess NaOH 0.40 - 1.00
ANB OVA SG @ 30”C, min 1.108
MVC-QF-TECH-008(24) QUALITY CONTROL DAILY ANALYSIS REPORT
Effectivity Date: October 1, 2016 MABUHAY VINYL CORPORATION
Date : 04/20/17 Time : 11:30 AM [ ]QC [ ]Technical [ ]IEM1/IEM2 [ ]AVP-Mfg
IEM 1 IEM 2
50 % CAUSTIC SODA 50 % CAUSTIC SODA Specs
Online Tk – A Tk - B Online Tk - 9
% NaOH NA NA NA 48.00-50.00
32 % CAUSTIC SODA 32 % CAUSTIC SODA
Online Tk – A Tk - B Online Tk - 8
% NaOH NA NA NA 30.00-32.00
HYDROCHLORIC ACID HYDROCHLORIC ACID
Online Tk- Tk- Online CTA 2
% HCl NA 32.00-33.50
Color # 3, max
POLISHED BRINE(After Precoat) POLISHED BRINE(After Precoat)
Ca+Mg, ppm + NA = + NA = 5.0 ppm,max.
SPB (After Headtank) SPB (After Headtank)
Ca+Mg, ppb nil + nil = nil nil + nil = nil 20 ppb, max.
NaCl, gpl NA NA 290 gpl,min.
Na2SO4,gpl NA NA 7 gpl, max.
NaClO3,gpl NA NA 20 gpl,max.
DEPLETED BRINE DEPLETED BRINE
NaCl, gpl 200 gpl, min.
Free Cl2 negative negative Negative
NaClO3,gpl NA NA 20 gpl, max.
pH NA NA 2.0, max
S O D I U M H Y P O C H L O R I T E PLANT
Tank No. 1 2 3 6 7
% NaOCl NA NA NA NA NA 7.40-8.00
% NaOH 0.40-1.00
Sp. Gravity 1.108, min
LI Q U I D C H LO R I N E PLAN T
Specs
Source LCP Tk.# Cl2 Feed LCP Tk # Cl2 Feed SULFURIC ACID
% Cl2 NA NA 99.5% min 91.0% min Source % H2SO4 Specs
% H2 NA NA NA NA LCP Comp. NA 97.0% min
UTILITIES
INSTRUMENT AIR @ AM Specs BOILER WATER Specs
Dew Point, °C ≤3.8 °C SiO2, ppm NA 150 ppm, max.
GAS ANALYSIS
IEM 1 IEM 2 FLUE GAS
% Cl2 % H2 O2 + CO2 % Cl2 % H2 O2 + CO2 % CO % CO2 % O2
Line A NA NA NA
Line B
POLLUTION C O N T R O L - EFFLUENTS
pH OIL Hg TDS TSS Color COD
Source 6AM 7PM (+ or -) ppb ppm mg/L Pt-Co Units mg/L
S-2 - NA NA NA NA NA
S-5 NA - NA NA NA NA NA
S-8 NA - NA NA NA NA NA
S-9 NA - NA NA NA NA NA
Lagoon NA NA NA NA NA NA NA
Source pH gpl NaOH Source pH SPECIFICATIONS
JBC NA S-3 NA pH = 6-9 COD = 100 mg/li, max Hg = 4 ppb, max.
Evap Canal S-4 Oil = Negative TDS = 1000 ppm, max TSS = 100 mg/li, max
Total Canal S-7 Color = 150 Pt-Co units, max.

Remarks: IEM 1 : NaOH- online(50%); SPB - Ca+Mg, NaCl; Depleted brine - Free
Analyzed
Cl2 by Certified Correct
OFF-SPECS IEM 2 : SPB - Ca+Mg, Na2SO4; Depleted brine - Free Cl2, NaClO3 (Original copy signed) (Original copy signed)

Others : Instrument Air - dewpoint; Effluents - S8(pH), S9(Color) NEY/ANB/RGD OVA


MVC-QF-TECH-004 (13)
Effectivity Date: August 5, 2014

MABUHAY VINYL CORPORATION PRODUCT TRANSFER CLEARANCE


Assumption Heights, Iligan City

Date : 04/20/17 [ ] IEM 1 [ ] IEM 2 [ ] Mktg [ ] QC file


IEM 1
HYDROCHLORIC ACID LIQUID CAUSTIC SODA SODIUM HYPOCHLORITE
Tk # % HCl SG @ 30”C Color Tk # 50% 32%. Tk # % NaOCl % NaOH SG @ 30”C
1 NA A NA NA 1 NA 0.00 0.000
2 NA B NA NA 2 NA 0.00 0.000
3 NA 3 NA 0.00 0.000
4 NA 6 NA 0.00 0.000
5 NA 7 NA 0.00 0.000
IEM 2 SPECIFICATIONS
HYDROCHLORIC ACID LIQUID CAUSTIC SODA HYDROCHLORIC ACID
Tk # % HCl SG @ 30”C Color Tk # 50% 32%. % HCl 32.00 - 33.50
CTA 1 NA 9 NA - SG @ 30”C, min 1.152
CTA 2 NA 8 - NA Color, max #3
CTA 3 NA LIQUID CAUSTIC SODA
CTB 1 NA 50% 32%
CTB 2 NA % NaOH 48.0-50.0 30.0 - 32.0
Remarks: % NaCl 0.10 0.10
WITHIN SPECS, OK for transfer ppm Fe, max 10 10
SODIUM HYPOCHLORITE
Analyzed by Certified Correct % NaOCl 7.40 - 8.00
(Original copy signed) (Original copy signed)
% excess NaOH 0.40 - 1.00
ANB OVA SG @ 30”C, min 1.108
MVC-QF-TECH-008(24) QUALITY CONTROL DAILY ANALYSIS REPORT
Effectivity Date: October 1, 2016 MABUHAY VINYL CORPORATION
Date : 04/21/17 Time : 11:30 AM [ ]QC [ ]Technical [ ]IEM1/IEM2 [ ]AVP-Mfg
IEM 1 IEM 2
50 % CAUSTIC SODA 50 % CAUSTIC SODA Specs
Online Tk – A Tk - B Online Tk - 9
% NaOH NA NA NA 48.00-50.00
32 % CAUSTIC SODA 32 % CAUSTIC SODA
Online Tk – A Tk - B Online Tk - 8
% NaOH NA NA NA 30.00-32.00
HYDROCHLORIC ACID HYDROCHLORIC ACID
Online Tk- Tk- Online CTA 2
% HCl NA 32.00-33.50
Color # 3, max
POLISHED BRINE(After Precoat) POLISHED BRINE(After Precoat)
Ca+Mg, ppm + NA = + NA = 5.0 ppm,max.
SPB (After Headtank) SPB (After Headtank)
Ca+Mg, ppb nil + nil = nil nil + nil = nil 20 ppb, max.
NaCl, gpl NA NA 290 gpl,min.
Na2SO4,gpl NA NA 7 gpl, max.
NaClO3,gpl NA NA 20 gpl,max.
DEPLETED BRINE DEPLETED BRINE
NaCl, gpl 200 gpl, min.
Free Cl2 negative negative Negative
NaClO3,gpl NA NA 20 gpl, max.
pH NA NA 2.0, max
S O D I U M H Y P O C H L O R I T E PLANT
Tank No. 1 2 3 6 7
% NaOCl NA NA NA NA NA 7.40-8.00
% NaOH 0.40-1.00
Sp. Gravity 1.108, min
LI Q U I D C H LO R I N E PLAN T
Specs
Source LCP Tk.# Cl2 Feed LCP Tk # Cl2 Feed SULFURIC ACID
% Cl2 NA NA 99.5% min 91.0% min Source % H2SO4 Specs
% H2 NA NA NA NA LCP Comp. NA 97.0% min
UTILITIES
INSTRUMENT AIR @ AM Specs BOILER WATER Specs
Dew Point, °C ≤3.8 °C SiO2, ppm NA 150 ppm, max.
GAS ANALYSIS
IEM 1 IEM 2 FLUE GAS
% Cl2 % H2 O2 + CO2 % Cl2 % H2 O2 + CO2 % CO % CO2 % O2
Line A NA NA NA
Line B
POLLUTION C O N T R O L - EFFLUENTS
pH OIL Hg TDS TSS Color COD
Source 6AM 7PM (+ or -) ppb ppm mg/L Pt-Co Units mg/L
S-2 - NA NA NA NA NA
S-5 NA - NA NA NA NA NA
S-8 NA - NA NA NA NA NA
S-9 NA - NA NA NA NA NA
Lagoon NA NA NA NA NA NA NA
Source pH gpl NaOH Source pH SPECIFICATIONS
JBC NA S-3 NA pH = 6-9 COD = 100 mg/li, max Hg = 4 ppb, max.
Evap Canal S-4 Oil = Negative TDS = 1000 ppm, max TSS = 100 mg/li, max
Total Canal S-7 Color = 150 Pt-Co units, max.

Remarks: IEM 1 : NaOH- online(50%); SPB - Ca+Mg, NaCl; Depleted brine - Free
Analyzed
Cl2 by Certified Correct
OFF-SPECS IEM 2 : SPB - Ca+Mg, Na2SO4; Depleted brine - Free Cl2, NaClO3 (Original copy signed) (Original copy signed)

Others : Instrument Air - dewpoint; Effluents - S8(pH), S9(Color) NEY/ANB/RGD OVA


MVC-QF-TECH-004 (13)
Effectivity Date: August 5, 2014

MABUHAY VINYL CORPORATION PRODUCT TRANSFER CLEARANCE


Assumption Heights, Iligan City

Date : 04/21/17 [ ] IEM 1 [ ] IEM 2 [ ] Mktg [ ] QC file


IEM 1
HYDROCHLORIC ACID LIQUID CAUSTIC SODA SODIUM HYPOCHLORITE
Tk # % HCl SG @ 30”C Color Tk # 50% 32%. Tk # % NaOCl % NaOH SG @ 30”C
1 NA A NA NA 1 NA 0.00 0.000
2 NA B NA NA 2 NA 0.00 0.000
3 NA 3 NA 0.00 0.000
4 NA 6 NA 0.00 0.000
5 NA 7 NA 0.00 0.000
IEM 2 SPECIFICATIONS
HYDROCHLORIC ACID LIQUID CAUSTIC SODA HYDROCHLORIC ACID
Tk # % HCl SG @ 30”C Color Tk # 50% 32%. % HCl 32.00 - 33.50
CTA 1 NA 9 NA - SG @ 30”C, min 1.152
CTA 2 NA 8 - NA Color, max #3
CTA 3 NA LIQUID CAUSTIC SODA
CTB 1 NA 50% 32%
CTB 2 NA % NaOH 48.0-50.0 30.0 - 32.0
Remarks: % NaCl 0.10 0.10
WITHIN SPECS, OK for transfer ppm Fe, max 10 10
SODIUM HYPOCHLORITE
Analyzed by Certified Correct % NaOCl 7.40 - 8.00
(Original copy signed) (Original copy signed)
% excess NaOH 0.40 - 1.00
ANB OVA SG @ 30”C, min 1.108
MVC-QF-TECH-008(24) QUALITY CONTROL DAILY ANALYSIS REPORT
Effectivity Date: October 1, 2016 MABUHAY VINYL CORPORATION
Date : 04/22/17 Time : 11:30 AM [ ]QC [ ]Technical [ ]IEM1/IEM2 [ ]AVP-Mfg
IEM 1 IEM 2
50 % CAUSTIC SODA 50 % CAUSTIC SODA Specs
Online Tk – A Tk - B Online Tk - 9
% NaOH NA NA NA 48.00-50.00
32 % CAUSTIC SODA 32 % CAUSTIC SODA
Online Tk – A Tk - B Online Tk - 8
% NaOH NA NA NA 30.00-32.00
HYDROCHLORIC ACID HYDROCHLORIC ACID
Online Tk- Tk- Online CTA 2
% HCl NA 32.00-33.50
Color # 3, max
POLISHED BRINE(After Precoat) POLISHED BRINE(After Precoat)
Ca+Mg, ppm + NA = + NA = 5.0 ppm,max.
SPB (After Headtank) SPB (After Headtank)
Ca+Mg, ppb nil + nil = nil nil + nil = nil 20 ppb, max.
NaCl, gpl NA NA 290 gpl,min.
Na2SO4,gpl NA NA 7 gpl, max.
NaClO3,gpl NA NA 20 gpl,max.
DEPLETED BRINE DEPLETED BRINE
NaCl, gpl 200 gpl, min.
Free Cl2 negative negative Negative
NaClO3,gpl NA NA 20 gpl, max.
pH NA NA 2.0, max
S O D I U M H Y P O C H L O R I T E PLANT
Tank No. 1 2 3 6 7
% NaOCl NA NA NA NA NA 7.40-8.00
% NaOH 0.40-1.00
Sp. Gravity 1.108, min
LI Q U I D C H LO R I N E PLAN T
Specs
Source LCP Tk.# Cl2 Feed LCP Tk # Cl2 Feed SULFURIC ACID
% Cl2 NA NA 99.5% min 91.0% min Source % H2SO4 Specs
% H2 NA NA NA NA LCP Comp. NA 97.0% min
UTILITIES
INSTRUMENT AIR @ AM Specs BOILER WATER Specs
Dew Point, °C ≤3.8 °C SiO2, ppm NA 150 ppm, max.
GAS ANALYSIS
IEM 1 IEM 2 FLUE GAS
% Cl2 % H2 O2 + CO2 % Cl2 % H2 O2 + CO2 % CO % CO2 % O2
Line A NA NA NA
Line B
POLLUTION C O N T R O L - EFFLUENTS
pH OIL Hg TDS TSS Color COD
Source 6AM 7PM (+ or -) ppb ppm mg/L Pt-Co Units mg/L
S-2 - NA NA NA NA NA
S-5 NA - NA NA NA NA NA
S-8 NA - NA NA NA NA NA
S-9 NA - NA NA NA NA NA
Lagoon NA NA NA NA NA NA NA
Source pH gpl NaOH Source pH SPECIFICATIONS
JBC NA S-3 NA pH = 6-9 COD = 100 mg/li, max Hg = 4 ppb, max.
Evap Canal S-4 Oil = Negative TDS = 1000 ppm, max TSS = 100 mg/li, max
Total Canal S-7 Color = 150 Pt-Co units, max.

Remarks: IEM 1 : NaOH- online(50%); SPB - Ca+Mg, NaCl; Depleted brine - Free
Analyzed
Cl2 by Certified Correct
OFF-SPECS IEM 2 : SPB - Ca+Mg, Na2SO4; Depleted brine - Free Cl2, NaClO3 (Original copy signed) (Original copy signed)

Others : Instrument Air - dewpoint; Effluents - S8(pH), S9(Color) NEY/ANB/RGD OVA


MVC-QF-TECH-004 (13)
Effectivity Date: August 5, 2014

MABUHAY VINYL CORPORATION PRODUCT TRANSFER CLEARANCE


Assumption Heights, Iligan City

Date : 04/22/17 [ ] IEM 1 [ ] IEM 2 [ ] Mktg [ ] QC file


IEM 1
HYDROCHLORIC ACID LIQUID CAUSTIC SODA SODIUM HYPOCHLORITE
Tk # % HCl SG @ 30”C Color Tk # 50% 32%. Tk # % NaOCl % NaOH SG @ 30”C
1 NA A NA NA 1 NA 0.00 0.000
2 NA B NA NA 2 NA 0.00 0.000
3 NA 3 NA 0.00 0.000
4 NA 6 NA 0.00 0.000
5 NA 7 NA 0.00 0.000
IEM 2 SPECIFICATIONS
HYDROCHLORIC ACID LIQUID CAUSTIC SODA HYDROCHLORIC ACID
Tk # % HCl SG @ 30”C Color Tk # 50% 32%. % HCl 32.00 - 33.50
CTA 1 NA 9 NA - SG @ 30”C, min 1.152
CTA 2 NA 8 - NA Color, max #3
CTA 3 NA LIQUID CAUSTIC SODA
CTB 1 NA 50% 32%
CTB 2 NA % NaOH 48.0-50.0 30.0 - 32.0
Remarks: % NaCl 0.10 0.10
WITHIN SPECS, OK for transfer ppm Fe, max 10 10
SODIUM HYPOCHLORITE
Analyzed by Certified Correct % NaOCl 7.40 - 8.00
(Original copy signed) (Original copy signed)
% excess NaOH 0.40 - 1.00
ANB OVA SG @ 30”C, min 1.108
MVC-QF-TECH-008(24) QUALITY CONTROL DAILY ANALYSIS REPORT
Effectivity Date: October 1, 2016 MABUHAY VINYL CORPORATION
Date : 04/23/17 Time : 11:30 AM [ ]QC [ ]Technical [ ]IEM1/IEM2 [ ]AVP-Mfg
IEM 1 IEM 2
50 % CAUSTIC SODA 50 % CAUSTIC SODA Specs
Online Tk – A Tk - B Online Tk - 9
% NaOH NA NA NA 48.00-50.00
32 % CAUSTIC SODA 32 % CAUSTIC SODA
Online Tk – A Tk - B Online Tk - 8
% NaOH NA NA NA 30.00-32.00
HYDROCHLORIC ACID HYDROCHLORIC ACID
Online Tk- Tk- Online CTA 2
% HCl NA 32.00-33.50
Color # 3, max
POLISHED BRINE(After Precoat) POLISHED BRINE(After Precoat)
Ca+Mg, ppm + NA = + NA = 5.0 ppm,max.
SPB (After Headtank) SPB (After Headtank)
Ca+Mg, ppb nil + nil = nil nil + nil = nil 20 ppb, max.
NaCl, gpl NA NA 290 gpl,min.
Na2SO4,gpl NA NA 7 gpl, max.
NaClO3,gpl NA NA 20 gpl,max.
DEPLETED BRINE DEPLETED BRINE
NaCl, gpl 200 gpl, min.
Free Cl2 negative negative Negative
NaClO3,gpl NA NA 20 gpl, max.
pH NA NA 2.0, max
S O D I U M H Y P O C H L O R I T E PLANT
Tank No. 1 2 3 6 7
% NaOCl NA NA NA NA NA 7.40-8.00
% NaOH 0.40-1.00
Sp. Gravity 1.108, min
LI Q U I D C H LO R I N E PLAN T
Specs
Source LCP Tk.# Cl2 Feed LCP Tk # Cl2 Feed SULFURIC ACID
% Cl2 NA NA 99.5% min 91.0% min Source % H2SO4 Specs
% H2 NA NA NA NA LCP Comp. NA 97.0% min
UTILITIES
INSTRUMENT AIR @ AM Specs BOILER WATER Specs
Dew Point, °C ≤3.8 °C SiO2, ppm NA 150 ppm, max.
GAS ANALYSIS
IEM 1 IEM 2 FLUE GAS
% Cl2 % H2 O2 + CO2 % Cl2 % H2 O2 + CO2 % CO % CO2 % O2
Line A NA NA NA
Line B
POLLUTION C O N T R O L - EFFLUENTS
pH OIL Hg TDS TSS Color COD
Source 6AM 7PM (+ or -) ppb ppm mg/L Pt-Co Units mg/L
S-2 - NA NA NA NA NA
S-5 NA - NA NA NA NA NA
S-8 NA - NA NA NA NA NA
S-9 NA - NA NA NA NA NA
Lagoon NA NA NA NA NA NA NA
Source pH gpl NaOH Source pH SPECIFICATIONS
JBC NA S-3 NA pH = 6-9 COD = 100 mg/li, max Hg = 4 ppb, max.
Evap Canal S-4 Oil = Negative TDS = 1000 ppm, max TSS = 100 mg/li, max
Total Canal S-7 Color = 150 Pt-Co units, max.

Remarks: IEM 1 : NaOH- online(50%); SPB - Ca+Mg, NaCl; Depleted brine - Free
Analyzed
Cl2 by Certified Correct
OFF-SPECS IEM 2 : SPB - Ca+Mg, Na2SO4; Depleted brine - Free Cl2, NaClO3 (Original copy signed) (Original copy signed)

Others : Instrument Air - dewpoint; Effluents - S8(pH), S9(Color) NEY/ANB/RGD OVA


MVC-QF-TECH-004 (13)
Effectivity Date: August 5, 2014

MABUHAY VINYL CORPORATION PRODUCT TRANSFER CLEARANCE


Assumption Heights, Iligan City

Date : 04/23/17 [ ] IEM 1 [ ] IEM 2 [ ] Mktg [ ] QC file


IEM 1
HYDROCHLORIC ACID LIQUID CAUSTIC SODA SODIUM HYPOCHLORITE
Tk # % HCl SG @ 30”C Color Tk # 50% 32%. Tk # % NaOCl % NaOH SG @ 30”C
1 NA A NA NA 1 NA 0.00 0.000
2 NA B NA NA 2 NA 0.00 0.000
3 NA 3 NA 0.00 0.000
4 NA 6 NA 0.00 0.000
5 NA 7 NA 0.00 0.000
IEM 2 SPECIFICATIONS
HYDROCHLORIC ACID LIQUID CAUSTIC SODA HYDROCHLORIC ACID
Tk # % HCl SG @ 30”C Color Tk # 50% 32%. % HCl 32.00 - 33.50
CTA 1 NA 9 NA - SG @ 30”C, min 1.152
CTA 2 NA 8 - NA Color, max #3
CTA 3 NA LIQUID CAUSTIC SODA
CTB 1 NA 50% 32%
CTB 2 NA % NaOH 48.0-50.0 30.0 - 32.0
Remarks: % NaCl 0.10 0.10
WITHIN SPECS, OK for transfer ppm Fe, max 10 10
SODIUM HYPOCHLORITE
Analyzed by Certified Correct % NaOCl 7.40 - 8.00
(Original copy signed) (Original copy signed)
% excess NaOH 0.40 - 1.00
ANB OVA SG @ 30”C, min 1.108
MVC-QF-TECH-008(24) QUALITY CONTROL DAILY ANALYSIS REPORT
Effectivity Date: October 1, 2016 MABUHAY VINYL CORPORATION
Date : 04/24/17 Time : 11:30 AM [ ]QC [ ]Technical [ ]IEM1/IEM2 [ ]AVP-Mfg
IEM 1 IEM 2
50 % CAUSTIC SODA 50 % CAUSTIC SODA Specs
Online Tk – A Tk - B Online Tk - 9
% NaOH NA NA NA 48.00-50.00
32 % CAUSTIC SODA 32 % CAUSTIC SODA
Online Tk – A Tk - B Online Tk - 8
% NaOH NA NA NA 30.00-32.00
HYDROCHLORIC ACID HYDROCHLORIC ACID
Online Tk- Tk- Online CTA 2
% HCl NA 32.00-33.50
Color # 3, max
POLISHED BRINE(After Precoat) POLISHED BRINE(After Precoat)
Ca+Mg, ppm + NA = + NA = 5.0 ppm,max.
SPB (After Headtank) SPB (After Headtank)
Ca+Mg, ppb nil + nil = nil nil + nil = nil 20 ppb, max.
NaCl, gpl NA NA 290 gpl,min.
Na2SO4,gpl NA NA 7 gpl, max.
NaClO3,gpl NA NA 20 gpl,max.
DEPLETED BRINE DEPLETED BRINE
NaCl, gpl 200 gpl, min.
Free Cl2 negative negative Negative
NaClO3,gpl NA NA 20 gpl, max.
pH NA NA 2.0, max
S O D I U M H Y P O C H L O R I T E PLANT
Tank No. 1 2 3 6 7
% NaOCl NA NA NA NA NA 7.40-8.00
% NaOH 0.40-1.00
Sp. Gravity 1.108, min
LI Q U I D C H LO R I N E PLAN T
Specs
Source LCP Tk.# Cl2 Feed LCP Tk # Cl2 Feed SULFURIC ACID
% Cl2 NA NA 99.5% min 91.0% min Source % H2SO4 Specs
% H2 NA NA NA NA LCP Comp. NA 97.0% min
UTILITIES
INSTRUMENT AIR @ AM Specs BOILER WATER Specs
Dew Point, °C ≤3.8 °C SiO2, ppm NA 150 ppm, max.
GAS ANALYSIS
IEM 1 IEM 2 FLUE GAS
% Cl2 % H2 O2 + CO2 % Cl2 % H2 O2 + CO2 % CO % CO2 % O2
Line A NA NA NA
Line B
POLLUTION C O N T R O L - EFFLUENTS
pH OIL Hg TDS TSS Color COD
Source 6AM 7PM (+ or -) ppb ppm mg/L Pt-Co Units mg/L
S-2 - NA NA NA NA NA
S-5 NA - NA NA NA NA NA
S-8 NA - NA NA NA NA NA
S-9 NA - NA NA NA NA NA
Lagoon NA NA NA NA NA NA NA
Source pH gpl NaOH Source pH SPECIFICATIONS
JBC NA S-3 NA pH = 6-9 COD = 100 mg/li, max Hg = 4 ppb, max.
Evap Canal S-4 Oil = Negative TDS = 1000 ppm, max TSS = 100 mg/li, max
Total Canal S-7 Color = 150 Pt-Co units, max.

Remarks: IEM 1 : NaOH- online(50%); SPB - Ca+Mg, NaCl; Depleted brine - Free
Analyzed
Cl2 by Certified Correct
OFF-SPECS IEM 2 : SPB - Ca+Mg, Na2SO4; Depleted brine - Free Cl2, NaClO3 (Original copy signed) (Original copy signed)

Others : Instrument Air - dewpoint; Effluents - S8(pH), S9(Color) NEY/ANB/RGD OVA


MVC-QF-TECH-004 (13)
Effectivity Date: August 5, 2014

MABUHAY VINYL CORPORATION PRODUCT TRANSFER CLEARANCE


Assumption Heights, Iligan City

Date : 04/24/17 [ ] IEM 1 [ ] IEM 2 [ ] Mktg [ ] QC file


IEM 1
HYDROCHLORIC ACID LIQUID CAUSTIC SODA SODIUM HYPOCHLORITE
Tk # % HCl SG @ 30”C Color Tk # 50% 32%. Tk # % NaOCl % NaOH SG @ 30”C
1 NA A NA NA 1 NA 0.00 0.000
2 NA B NA NA 2 NA 0.00 0.000
3 NA 3 NA 0.00 0.000
4 NA 6 NA 0.00 0.000
5 NA 7 NA 0.00 0.000
IEM 2 SPECIFICATIONS
HYDROCHLORIC ACID LIQUID CAUSTIC SODA HYDROCHLORIC ACID
Tk # % HCl SG @ 30”C Color Tk # 50% 32%. % HCl 32.00 - 33.50
CTA 1 NA 9 NA - SG @ 30”C, min 1.152
CTA 2 NA 8 - NA Color, max #3
CTA 3 NA LIQUID CAUSTIC SODA
CTB 1 NA 50% 32%
CTB 2 NA % NaOH 48.0-50.0 30.0 - 32.0
Remarks: % NaCl 0.10 0.10
WITHIN SPECS, OK for transfer ppm Fe, max 10 10
SODIUM HYPOCHLORITE
Analyzed by Certified Correct % NaOCl 7.40 - 8.00
(Original copy signed) (Original copy signed)
% excess NaOH 0.40 - 1.00
ANB OVA SG @ 30”C, min 1.108
MVC-QF-TECH-008(24) QUALITY CONTROL DAILY ANALYSIS REPORT
Effectivity Date: October 1, 2016 MABUHAY VINYL CORPORATION
Date : 04/25/17 Time : 11:30 AM [ ]QC [ ]Technical [ ]IEM1/IEM2 [ ]AVP-Mfg
IEM 1 IEM 2
50 % CAUSTIC SODA 50 % CAUSTIC SODA Specs
Online Tk – A Tk - B Online Tk - 9
% NaOH NA NA NA 48.00-50.00
32 % CAUSTIC SODA 32 % CAUSTIC SODA
Online Tk – A Tk - B Online Tk - 8
% NaOH NA NA NA 30.00-32.00
HYDROCHLORIC ACID HYDROCHLORIC ACID
Online Tk- Tk- Online CTA 2
% HCl NA 32.00-33.50
Color # 3, max
POLISHED BRINE(After Precoat) POLISHED BRINE(After Precoat)
Ca+Mg, ppm + NA = + NA = 5.0 ppm,max.
SPB (After Headtank) SPB (After Headtank)
Ca+Mg, ppb nil + nil = nil nil + nil = nil 20 ppb, max.
NaCl, gpl NA NA 290 gpl,min.
Na2SO4,gpl NA NA 7 gpl, max.
NaClO3,gpl NA NA 20 gpl,max.
DEPLETED BRINE DEPLETED BRINE
NaCl, gpl 200 gpl, min.
Free Cl2 negative negative Negative
NaClO3,gpl NA NA 20 gpl, max.
pH NA NA 2.0, max
S O D I U M H Y P O C H L O R I T E PLANT
Tank No. 1 2 3 6 7
% NaOCl NA NA NA NA NA 7.40-8.00
% NaOH 0.40-1.00
Sp. Gravity 1.108, min
LI Q U I D C H LO R I N E PLAN T
Specs
Source LCP Tk.# Cl2 Feed LCP Tk # Cl2 Feed SULFURIC ACID
% Cl2 NA NA 99.5% min 91.0% min Source % H2SO4 Specs
% H2 NA NA NA NA LCP Comp. NA 97.0% min
UTILITIES
INSTRUMENT AIR @ AM Specs BOILER WATER Specs
Dew Point, °C ≤3.8 °C SiO2, ppm NA 150 ppm, max.
GAS ANALYSIS
IEM 1 IEM 2 FLUE GAS
% Cl2 % H2 O2 + CO2 % Cl2 % H2 O2 + CO2 % CO % CO2 % O2
Line A NA NA NA
Line B
POLLUTION C O N T R O L - EFFLUENTS
pH OIL Hg TDS TSS Color COD
Source 6AM 7PM (+ or -) ppb ppm mg/L Pt-Co Units mg/L
S-2 - NA NA NA NA NA
S-5 NA - NA NA NA NA NA
S-8 NA - NA NA NA NA NA
S-9 NA - NA NA NA NA NA
Lagoon NA NA NA NA NA NA NA
Source pH gpl NaOH Source pH SPECIFICATIONS
JBC NA S-3 NA pH = 6-9 COD = 100 mg/li, max Hg = 4 ppb, max.
Evap Canal S-4 Oil = Negative TDS = 1000 ppm, max TSS = 100 mg/li, max
Total Canal S-7 Color = 150 Pt-Co units, max.

Remarks: IEM 1 : NaOH- online(50%); SPB - Ca+Mg, NaCl; Depleted brine - Free
Analyzed
Cl2 by Certified Correct
OFF-SPECS IEM 2 : SPB - Ca+Mg, Na2SO4; Depleted brine - Free Cl2, NaClO3 (Original copy signed) (Original copy signed)

Others : Instrument Air - dewpoint; Effluents - S8(pH), S9(Color) NEY/ANB/RGD OVA


MVC-QF-TECH-004 (13)
Effectivity Date: August 5, 2014

MABUHAY VINYL CORPORATION PRODUCT TRANSFER CLEARANCE


Assumption Heights, Iligan City

Date : 04/25/17 [ ] IEM 1 [ ] IEM 2 [ ] Mktg [ ] QC file


IEM 1
HYDROCHLORIC ACID LIQUID CAUSTIC SODA SODIUM HYPOCHLORITE
Tk # % HCl SG @ 30”C Color Tk # 50% 32%. Tk # % NaOCl % NaOH SG @ 30”C
1 NA A NA NA 1 NA 0.00 0.000
2 NA B NA NA 2 NA 0.00 0.000
3 NA 3 NA 0.00 0.000
4 NA 6 NA 0.00 0.000
5 NA 7 NA 0.00 0.000
IEM 2 SPECIFICATIONS
HYDROCHLORIC ACID LIQUID CAUSTIC SODA HYDROCHLORIC ACID
Tk # % HCl SG @ 30”C Color Tk # 50% 32%. % HCl 32.00 - 33.50
CTA 1 NA 9 NA - SG @ 30”C, min 1.152
CTA 2 NA 8 - NA Color, max #3
CTA 3 NA LIQUID CAUSTIC SODA
CTB 1 NA 50% 32%
CTB 2 NA % NaOH 48.0-50.0 30.0 - 32.0
Remarks: % NaCl 0.10 0.10
WITHIN SPECS, OK for transfer ppm Fe, max 10 10
SODIUM HYPOCHLORITE
Analyzed by Certified Correct % NaOCl 7.40 - 8.00
(Original copy signed) (Original copy signed)
% excess NaOH 0.40 - 1.00
ANB OVA SG @ 30”C, min 1.108
MVC-QF-TECH-008(24) QUALITY CONTROL DAILY ANALYSIS REPORT
Effectivity Date: October 1, 2016 MABUHAY VINYL CORPORATION
Date : 04/26/17 Time : 11:30 AM [ ]QC [ ]Technical [ ]IEM1/IEM2 [ ]AVP-Mfg
IEM 1 IEM 2
50 % CAUSTIC SODA 50 % CAUSTIC SODA Specs
Online Tk – A Tk - B Online Tk - 9
% NaOH NA NA NA 48.00-50.00
32 % CAUSTIC SODA 32 % CAUSTIC SODA
Online Tk – A Tk - B Online Tk - 8
% NaOH NA NA NA 30.00-32.00
HYDROCHLORIC ACID HYDROCHLORIC ACID
Online Tk- Tk- Online CTA 2
% HCl NA 32.00-33.50
Color # 3, max
POLISHED BRINE(After Precoat) POLISHED BRINE(After Precoat)
Ca+Mg, ppm + NA = + NA = 5.0 ppm,max.
SPB (After Headtank) SPB (After Headtank)
Ca+Mg, ppb nil + nil = nil nil + nil = nil 20 ppb, max.
NaCl, gpl NA NA 290 gpl,min.
Na2SO4,gpl NA NA 7 gpl, max.
NaClO3,gpl NA NA 20 gpl,max.
DEPLETED BRINE DEPLETED BRINE
NaCl, gpl 200 gpl, min.
Free Cl2 negative negative Negative
NaClO3,gpl NA NA 20 gpl, max.
pH NA NA 2.0, max
S O D I U M H Y P O C H L O R I T E PLANT
Tank No. 1 2 3 6 7
% NaOCl NA NA NA NA NA 7.40-8.00
% NaOH 0.40-1.00
Sp. Gravity 1.108, min
LI Q U I D C H LO R I N E PLAN T
Specs
Source LCP Tk.# Cl2 Feed LCP Tk # Cl2 Feed SULFURIC ACID
% Cl2 NA NA 99.5% min 91.0% min Source % H2SO4 Specs
% H2 NA NA NA NA LCP Comp. NA 97.0% min
UTILITIES
INSTRUMENT AIR @ AM Specs BOILER WATER Specs
Dew Point, °C ≤3.8 °C SiO2, ppm NA 150 ppm, max.
GAS ANALYSIS
IEM 1 IEM 2 FLUE GAS
% Cl2 % H2 O2 + CO2 % Cl2 % H2 O2 + CO2 % CO % CO2 % O2
Line A NA NA NA
Line B
POLLUTION C O N T R O L - EFFLUENTS
pH OIL Hg TDS TSS Color COD
Source 6AM 7PM (+ or -) ppb ppm mg/L Pt-Co Units mg/L
S-2 - NA NA NA NA NA
S-5 NA - NA NA NA NA NA
S-8 NA - NA NA NA NA NA
S-9 NA - NA NA NA NA NA
Lagoon NA NA NA NA NA NA NA
Source pH gpl NaOH Source pH SPECIFICATIONS
JBC NA S-3 NA pH = 6-9 COD = 100 mg/li, max Hg = 4 ppb, max.
Evap Canal S-4 Oil = Negative TDS = 1000 ppm, max TSS = 100 mg/li, max
Total Canal S-7 Color = 150 Pt-Co units, max.

Remarks: IEM 1 : NaOH- online(50%); SPB - Ca+Mg, NaCl; Depleted brine - Free
Analyzed
Cl2 by Certified Correct
OFF-SPECS IEM 2 : SPB - Ca+Mg, Na2SO4; Depleted brine - Free Cl2, NaClO3 (Original copy signed) (Original copy signed)

Others : Instrument Air - dewpoint; Effluents - S8(pH), S9(Color) NEY/ANB/RGD OVA


MVC-QF-TECH-004 (13)
Effectivity Date: August 5, 2014

MABUHAY VINYL CORPORATION PRODUCT TRANSFER CLEARANCE


Assumption Heights, Iligan City

Date : 04/26/17 [ ] IEM 1 [ ] IEM 2 [ ] Mktg [ ] QC file


IEM 1
HYDROCHLORIC ACID LIQUID CAUSTIC SODA SODIUM HYPOCHLORITE
Tk # % HCl SG @ 30”C Color Tk # 50% 32%. Tk # % NaOCl % NaOH SG @ 30”C
1 NA A NA NA 1 NA 0.00 0.000
2 NA B NA NA 2 NA 0.00 0.000
3 NA 3 NA 0.00 0.000
4 NA 6 NA 0.00 0.000
5 NA 7 NA 0.00 0.000
IEM 2 SPECIFICATIONS
HYDROCHLORIC ACID LIQUID CAUSTIC SODA HYDROCHLORIC ACID
Tk # % HCl SG @ 30”C Color Tk # 50% 32%. % HCl 32.00 - 33.50
CTA 1 NA 9 NA - SG @ 30”C, min 1.152
CTA 2 NA 8 - NA Color, max #3
CTA 3 NA LIQUID CAUSTIC SODA
CTB 1 NA 50% 32%
CTB 2 NA % NaOH 48.0-50.0 30.0 - 32.0
Remarks: % NaCl 0.10 0.10
WITHIN SPECS, OK for transfer ppm Fe, max 10 10
SODIUM HYPOCHLORITE
Analyzed by Certified Correct % NaOCl 7.40 - 8.00
(Original copy signed) (Original copy signed)
% excess NaOH 0.40 - 1.00
ANB OVA SG @ 30”C, min 1.108
MVC-QF-TECH-008(24) QUALITY CONTROL DAILY ANALYSIS REPORT
Effectivity Date: October 1, 2016 MABUHAY VINYL CORPORATION
Date : 04/27/17 Time : 11:30 AM [ ]QC [ ]Technical [ ]IEM1/IEM2 [ ]AVP-Mfg
IEM 1 IEM 2
50 % CAUSTIC SODA 50 % CAUSTIC SODA Specs
Online Tk – A Tk - B Online Tk - 9
% NaOH NA NA NA 48.00-50.00
32 % CAUSTIC SODA 32 % CAUSTIC SODA
Online Tk – A Tk - B Online Tk - 8
% NaOH NA NA NA 30.00-32.00
HYDROCHLORIC ACID HYDROCHLORIC ACID
Online Tk- Tk- Online CTA 2
% HCl NA 32.00-33.50
Color # 3, max
POLISHED BRINE(After Precoat) POLISHED BRINE(After Precoat)
Ca+Mg, ppm + NA = + NA = 5.0 ppm,max.
SPB (After Headtank) SPB (After Headtank)
Ca+Mg, ppb nil + nil = nil nil + nil = nil 20 ppb, max.
NaCl, gpl NA NA 290 gpl,min.
Na2SO4,gpl NA NA 7 gpl, max.
NaClO3,gpl NA NA 20 gpl,max.
DEPLETED BRINE DEPLETED BRINE
NaCl, gpl 200 gpl, min.
Free Cl2 negative negative Negative
NaClO3,gpl NA NA 20 gpl, max.
pH NA NA 2.0, max
S O D I U M H Y P O C H L O R I T E PLANT
Tank No. 1 2 3 6 7
% NaOCl NA NA NA NA NA 7.40-8.00
% NaOH 0.40-1.00
Sp. Gravity 1.108, min
LI Q U I D C H LO R I N E PLAN T
Specs
Source LCP Tk.# Cl2 Feed LCP Tk # Cl2 Feed SULFURIC ACID
% Cl2 NA NA 99.5% min 91.0% min Source % H2SO4 Specs
% H2 NA NA NA NA LCP Comp. NA 97.0% min
UTILITIES
INSTRUMENT AIR @ AM Specs BOILER WATER Specs
Dew Point, °C ≤3.8 °C SiO2, ppm NA 150 ppm, max.
GAS ANALYSIS
IEM 1 IEM 2 FLUE GAS
% Cl2 % H2 O2 + CO2 % Cl2 % H2 O2 + CO2 % CO % CO2 % O2
Line A NA NA NA
Line B
POLLUTION C O N T R O L - EFFLUENTS
pH OIL Hg TDS TSS Color COD
Source 6AM 7PM (+ or -) ppb ppm mg/L Pt-Co Units mg/L
S-2 - NA NA NA NA NA
S-5 NA - NA NA NA NA NA
S-8 NA - NA NA NA NA NA
S-9 NA - NA NA NA NA NA
Lagoon NA NA NA NA NA NA NA
Source pH gpl NaOH Source pH SPECIFICATIONS
JBC NA S-3 NA pH = 6-9 COD = 100 mg/li, max Hg = 4 ppb, max.
Evap Canal S-4 Oil = Negative TDS = 1000 ppm, max TSS = 100 mg/li, max
Total Canal S-7 Color = 150 Pt-Co units, max.

Remarks: IEM 1 : NaOH- online(50%); SPB - Ca+Mg, NaCl; Depleted brine - Free
Analyzed
Cl2 by Certified Correct
OFF-SPECS IEM 2 : SPB - Ca+Mg, Na2SO4; Depleted brine - Free Cl2, NaClO3 (Original copy signed) (Original copy signed)

Others : Instrument Air - dewpoint; Effluents - S8(pH), S9(Color) NEY/ANB/RGD OVA


MVC-QF-TECH-004 (13)
Effectivity Date: August 5, 2014

MABUHAY VINYL CORPORATION PRODUCT TRANSFER CLEARANCE


Assumption Heights, Iligan City

Date : 04/27/17 [ ] IEM 1 [ ] IEM 2 [ ] Mktg [ ] QC file


IEM 1
HYDROCHLORIC ACID LIQUID CAUSTIC SODA SODIUM HYPOCHLORITE
Tk # % HCl SG @ 30”C Color Tk # 50% 32%. Tk # % NaOCl % NaOH SG @ 30”C
1 NA A NA NA 1 NA 0.00 0.000
2 NA B NA NA 2 NA 0.00 0.000
3 NA 3 NA 0.00 0.000
4 NA 6 NA 0.00 0.000
5 NA 7 NA 0.00 0.000
IEM 2 SPECIFICATIONS
HYDROCHLORIC ACID LIQUID CAUSTIC SODA HYDROCHLORIC ACID
Tk # % HCl SG @ 30”C Color Tk # 50% 32%. % HCl 32.00 - 33.50
CTA 1 NA 9 NA - SG @ 30”C, min 1.152
CTA 2 NA 8 - NA Color, max #3
CTA 3 NA LIQUID CAUSTIC SODA
CTB 1 NA 50% 32%
CTB 2 NA % NaOH 48.0-50.0 30.0 - 32.0
Remarks: % NaCl 0.10 0.10
WITHIN SPECS, OK for transfer ppm Fe, max 10 10
SODIUM HYPOCHLORITE
Analyzed by Certified Correct % NaOCl 7.40 - 8.00
(Original copy signed) (Original copy signed)
% excess NaOH 0.40 - 1.00
ANB OVA SG @ 30”C, min 1.108
MVC-QF-TECH-008(24) QUALITY CONTROL DAILY ANALYSIS REPORT
Effectivity Date: October 1, 2016 MABUHAY VINYL CORPORATION
Date : 04/28/17 Time : 11:30 AM [ ]QC [ ]Technical [ ]IEM1/IEM2 [ ]AVP-Mfg
IEM 1 IEM 2
50 % CAUSTIC SODA 50 % CAUSTIC SODA Specs
Online Tk – A Tk - B Online Tk - 9
% NaOH NA NA NA 48.00-50.00
32 % CAUSTIC SODA 32 % CAUSTIC SODA
Online Tk – A Tk - B Online Tk - 8
% NaOH NA NA NA 30.00-32.00
HYDROCHLORIC ACID HYDROCHLORIC ACID
Online Tk- Tk- Online CTA 2
% HCl NA 32.00-33.50
Color # 3, max
POLISHED BRINE(After Precoat) POLISHED BRINE(After Precoat)
Ca+Mg, ppm + NA = + NA = 5.0 ppm,max.
SPB (After Headtank) SPB (After Headtank)
Ca+Mg, ppb nil + nil = nil nil + nil = nil 20 ppb, max.
NaCl, gpl NA NA 290 gpl,min.
Na2SO4,gpl NA NA 7 gpl, max.
NaClO3,gpl NA NA 20 gpl,max.
DEPLETED BRINE DEPLETED BRINE
NaCl, gpl 200 gpl, min.
Free Cl2 negative negative Negative
NaClO3,gpl NA NA 20 gpl, max.
pH NA NA 2.0, max
S O D I U M H Y P O C H L O R I T E PLANT
Tank No. 1 2 3 6 7
% NaOCl NA NA NA NA NA 7.40-8.00
% NaOH 0.40-1.00
Sp. Gravity 1.108, min
LI Q U I D C H LO R I N E PLAN T
Specs
Source LCP Tk.# Cl2 Feed LCP Tk # Cl2 Feed SULFURIC ACID
% Cl2 NA NA 99.5% min 91.0% min Source % H2SO4 Specs
% H2 NA NA NA NA LCP Comp. NA 97.0% min
UTILITIES
INSTRUMENT AIR @ AM Specs BOILER WATER Specs
Dew Point, °C ≤3.8 °C SiO2, ppm NA 150 ppm, max.
GAS ANALYSIS
IEM 1 IEM 2 FLUE GAS
% Cl2 % H2 O2 + CO2 % Cl2 % H2 O2 + CO2 % CO % CO2 % O2
Line A NA NA NA
Line B
POLLUTION C O N T R O L - EFFLUENTS
pH OIL Hg TDS TSS Color COD
Source 6AM 7PM (+ or -) ppb ppm mg/L Pt-Co Units mg/L
S-2 - NA NA NA NA NA
S-5 NA - NA NA NA NA NA
S-8 NA - NA NA NA NA NA
S-9 NA - NA NA NA NA NA
Lagoon NA NA NA NA NA NA NA
Source pH gpl NaOH Source pH SPECIFICATIONS
JBC NA S-3 NA pH = 6-9 COD = 100 mg/li, max Hg = 4 ppb, max.
Evap Canal S-4 Oil = Negative TDS = 1000 ppm, max TSS = 100 mg/li, max
Total Canal S-7 Color = 150 Pt-Co units, max.

Remarks: IEM 1 : NaOH- online(50%); SPB - Ca+Mg, NaCl; Depleted brine - Free
Analyzed
Cl2 by Certified Correct
OFF-SPECS IEM 2 : SPB - Ca+Mg, Na2SO4; Depleted brine - Free Cl2, NaClO3 (Original copy signed) (Original copy signed)

Others : Instrument Air - dewpoint; Effluents - S8(pH), S9(Color) NEY/ANB/RGD OVA


MVC-QF-TECH-004 (13)
Effectivity Date: August 5, 2014

MABUHAY VINYL CORPORATION PRODUCT TRANSFER CLEARANCE


Assumption Heights, Iligan City

Date : 04/28/17 [ ] IEM 1 [ ] IEM 2 [ ] Mktg [ ] QC file


IEM 1
HYDROCHLORIC ACID LIQUID CAUSTIC SODA SODIUM HYPOCHLORITE
Tk # % HCl SG @ 30”C Color Tk # 50% 32%. Tk # % NaOCl % NaOH SG @ 30”C
1 NA A NA NA 1 NA 0.00 0.000
2 NA B NA NA 2 NA 0.00 0.000
3 NA 3 NA 0.00 0.000
4 NA 6 NA 0.00 0.000
5 NA 7 NA 0.00 0.000
IEM 2 SPECIFICATIONS
HYDROCHLORIC ACID LIQUID CAUSTIC SODA HYDROCHLORIC ACID
Tk # % HCl SG @ 30”C Color Tk # 50% 32%. % HCl 32.00 - 33.50
CTA 1 NA 9 NA - SG @ 30”C, min 1.152
CTA 2 NA 8 - NA Color, max #3
CTA 3 NA LIQUID CAUSTIC SODA
CTB 1 NA 50% 32%
CTB 2 NA % NaOH 48.0-50.0 30.0 - 32.0
Remarks: % NaCl 0.10 0.10
WITHIN SPECS, OK for transfer ppm Fe, max 10 10
SODIUM HYPOCHLORITE
Analyzed by Certified Correct % NaOCl 7.40 - 8.00
(Original copy signed) (Original copy signed)
% excess NaOH 0.40 - 1.00
ANB OVA SG @ 30”C, min 1.108
MVC-QF-TECH-008(24) QUALITY CONTROL DAILY ANALYSIS REPORT
Effectivity Date: October 1, 2016 MABUHAY VINYL CORPORATION
Date : 04/29/17 Time : 11:30 AM [ ]QC [ ]Technical [ ]IEM1/IEM2 [ ]AVP-Mfg
IEM 1 IEM 2
50 % CAUSTIC SODA 50 % CAUSTIC SODA Specs
Online Tk – A Tk - B Online Tk - 9
% NaOH NA NA NA 48.00-50.00
32 % CAUSTIC SODA 32 % CAUSTIC SODA
Online Tk – A Tk - B Online Tk - 8
% NaOH NA NA NA 30.00-32.00
HYDROCHLORIC ACID HYDROCHLORIC ACID
Online Tk- Tk- Online CTA 2
% HCl NA 32.00-33.50
Color # 3, max
POLISHED BRINE(After Precoat) POLISHED BRINE(After Precoat)
Ca+Mg, ppm + NA = + NA = 5.0 ppm,max.
SPB (After Headtank) SPB (After Headtank)
Ca+Mg, ppb nil + nil = nil nil + nil = nil 20 ppb, max.
NaCl, gpl NA NA 290 gpl,min.
Na2SO4,gpl NA NA 7 gpl, max.
NaClO3,gpl NA NA 20 gpl,max.
DEPLETED BRINE DEPLETED BRINE
NaCl, gpl 200 gpl, min.
Free Cl2 negative negative Negative
NaClO3,gpl NA NA 20 gpl, max.
pH NA NA 2.0, max
S O D I U M H Y P O C H L O R I T E PLANT
Tank No. 1 2 3 6 7
% NaOCl NA NA NA NA NA 7.40-8.00
% NaOH 0.40-1.00
Sp. Gravity 1.108, min
LI Q U I D C H LO R I N E PLAN T
Specs
Source LCP Tk.# Cl2 Feed LCP Tk # Cl2 Feed SULFURIC ACID
% Cl2 NA NA 99.5% min 91.0% min Source % H2SO4 Specs
% H2 NA NA NA NA LCP Comp. NA 97.0% min
UTILITIES
INSTRUMENT AIR @ AM Specs BOILER WATER Specs
Dew Point, °C ≤3.8 °C SiO2, ppm NA 150 ppm, max.
GAS ANALYSIS
IEM 1 IEM 2 FLUE GAS
% Cl2 % H2 O2 + CO2 % Cl2 % H2 O2 + CO2 % CO % CO2 % O2
Line A NA NA NA
Line B
POLLUTION C O N T R O L - EFFLUENTS
pH OIL Hg TDS TSS Color COD
Source 6AM 7PM (+ or -) ppb ppm mg/L Pt-Co Units mg/L
S-2 - NA NA NA NA NA
S-5 NA - NA NA NA NA NA
S-8 NA - NA NA NA NA NA
S-9 NA - NA NA NA NA NA
Lagoon NA NA NA NA NA NA NA
Source pH gpl NaOH Source pH SPECIFICATIONS
JBC NA S-3 NA pH = 6-9 COD = 100 mg/li, max Hg = 4 ppb, max.
Evap Canal S-4 Oil = Negative TDS = 1000 ppm, max TSS = 100 mg/li, max
Total Canal S-7 Color = 150 Pt-Co units, max.

Remarks: IEM 1 : NaOH- online(50%); SPB - Ca+Mg, NaCl; Depleted brine - Free
Analyzed
Cl2 by Certified Correct
OFF-SPECS IEM 2 : SPB - Ca+Mg, Na2SO4; Depleted brine - Free Cl2, NaClO3 (Original copy signed) (Original copy signed)

Others : Instrument Air - dewpoint; Effluents - S8(pH), S9(Color) NEY/ANB/RGD OVA


MVC-QF-TECH-004 (13)
Effectivity Date: August 5, 2014

MABUHAY VINYL CORPORATION PRODUCT TRANSFER CLEARANCE


Assumption Heights, Iligan City

Date : 04/29/17 [ ] IEM 1 [ ] IEM 2 [ ] Mktg [ ] QC file


IEM 1
HYDROCHLORIC ACID LIQUID CAUSTIC SODA SODIUM HYPOCHLORITE
Tk # % HCl SG @ 30”C Color Tk # 50% 32%. Tk # % NaOCl % NaOH SG @ 30”C
1 NA A NA NA 1 NA 0.00 0.000
2 NA B NA NA 2 NA 0.00 0.000
3 NA 3 NA 0.00 0.000
4 NA 6 NA 0.00 0.000
5 NA 7 NA 0.00 0.000
IEM 2 SPECIFICATIONS
HYDROCHLORIC ACID LIQUID CAUSTIC SODA HYDROCHLORIC ACID
Tk # % HCl SG @ 30”C Color Tk # 50% 32%. % HCl 32.00 - 33.50
CTA 1 NA 9 NA - SG @ 30”C, min 1.152
CTA 2 NA 8 - NA Color, max #3
CTA 3 NA LIQUID CAUSTIC SODA
CTB 1 NA 50% 32%
CTB 2 NA % NaOH 48.0-50.0 30.0 - 32.0
Remarks: % NaCl 0.10 0.10
WITHIN SPECS, OK for transfer ppm Fe, max 10 10
SODIUM HYPOCHLORITE
Analyzed by Certified Correct % NaOCl 7.40 - 8.00
(Original copy signed) (Original copy signed)
% excess NaOH 0.40 - 1.00
ANB OVA SG @ 30”C, min 1.108
MVC-QF-TECH-008(24) QUALITY CONTROL DAILY ANALYSIS REPORT
Effectivity Date: October 1, 2016 MABUHAY VINYL CORPORATION
Date : 04/30/17 Time : 11:30 AM [ ]QC [ ]Technical [ ]IEM1/IEM2 [ ]AVP-Mfg
IEM 1 IEM 2
50 % CAUSTIC SODA 50 % CAUSTIC SODA Specs
Online Tk – A Tk - B Online Tk - 9
% NaOH NA NA NA 48.00-50.00
32 % CAUSTIC SODA 32 % CAUSTIC SODA
Online Tk – A Tk - B Online Tk - 8
% NaOH NA NA NA 30.00-32.00
HYDROCHLORIC ACID HYDROCHLORIC ACID
Online Tk- Tk- Online CTA 2
% HCl NA 32.00-33.50
Color # 3, max
POLISHED BRINE(After Precoat) POLISHED BRINE(After Precoat)
Ca+Mg, ppm + NA = + NA = 5.0 ppm,max.
SPB (After Headtank) SPB (After Headtank)
Ca+Mg, ppb nil + nil = nil nil + nil = nil 20 ppb, max.
NaCl, gpl NA NA 290 gpl,min.
Na2SO4,gpl NA NA 7 gpl, max.
NaClO3,gpl NA NA 20 gpl,max.
DEPLETED BRINE DEPLETED BRINE
NaCl, gpl 200 gpl, min.
Free Cl2 negative negative Negative
NaClO3,gpl NA NA 20 gpl, max.
pH NA NA 2.0, max
S O D I U M H Y P O C H L O R I T E PLANT
Tank No. 1 2 3 6 7
% NaOCl NA NA NA NA NA 7.40-8.00
% NaOH 0.40-1.00
Sp. Gravity 1.108, min
LI Q U I D C H LO R I N E PLAN T
Specs
Source LCP Tk.# Cl2 Feed LCP Tk # Cl2 Feed SULFURIC ACID
% Cl2 NA NA 99.5% min 91.0% min Source % H2SO4 Specs
% H2 NA NA NA NA LCP Comp. NA 97.0% min
UTILITIES
INSTRUMENT AIR @ AM Specs BOILER WATER Specs
Dew Point, °C ≤3.8 °C SiO2, ppm NA 150 ppm, max.
GAS ANALYSIS
IEM 1 IEM 2 FLUE GAS
% Cl2 % H2 O2 + CO2 % Cl2 % H2 O2 + CO2 % CO % CO2 % O2
Line A NA NA NA
Line B
POLLUTION C O N T R O L - EFFLUENTS
pH OIL Hg TDS TSS Color COD
Source 6AM 7PM (+ or -) ppb ppm mg/L Pt-Co Units mg/L
S-2 - NA NA NA NA NA
S-5 NA - NA NA NA NA NA
S-8 NA - NA NA NA NA NA
S-9 NA - NA NA NA NA NA
Lagoon NA NA NA NA NA NA NA
Source pH gpl NaOH Source pH SPECIFICATIONS
JBC NA S-3 NA pH = 6-9 COD = 100 mg/li, max Hg = 4 ppb, max.
Evap Canal S-4 Oil = Negative TDS = 1000 ppm, max TSS = 100 mg/li, max
Total Canal S-7 Color = 150 Pt-Co units, max.

Remarks: IEM 1 : NaOH- online(50%); SPB - Ca+Mg, NaCl; Depleted brine - Free
Analyzed
Cl2 by Certified Correct
OFF-SPECS IEM 2 : SPB - Ca+Mg, Na2SO4; Depleted brine - Free Cl2, NaClO3 (Original copy signed) (Original copy signed)

Others : Instrument Air - dewpoint; Effluents - S8(pH), S9(Color) NEY/ANB/RGD OVA


MVC-QF-TECH-004 (13)
Effectivity Date: August 5, 2014

MABUHAY VINYL CORPORATION PRODUCT TRANSFER CLEARANCE


Assumption Heights, Iligan City

Date : 04/30/17 [ ] IEM 1 [ ] IEM 2 [ ] Mktg [ ] QC file


IEM 1
HYDROCHLORIC ACID LIQUID CAUSTIC SODA SODIUM HYPOCHLORITE
Tk # % HCl SG @ 30”C Color Tk # 50% 32%. Tk # % NaOCl % NaOH SG @ 30”C
1 NA A NA NA 1 NA 0.00 0.000
2 NA B NA NA 2 NA 0.00 0.000
3 NA 3 NA 0.00 0.000
4 NA 6 NA 0.00 0.000
5 NA 7 NA 0.00 0.000
IEM 2 SPECIFICATIONS
HYDROCHLORIC ACID LIQUID CAUSTIC SODA HYDROCHLORIC ACID
Tk # % HCl SG @ 30”C Color Tk # 50% 32%. % HCl 32.00 - 33.50
CTA 1 NA 9 NA - SG @ 30”C, min 1.152
CTA 2 NA 8 - NA Color, max #3
CTA 3 NA LIQUID CAUSTIC SODA
CTB 1 NA 50% 32%
CTB 2 NA % NaOH 48.0-50.0 30.0 - 32.0
Remarks: % NaCl 0.10 0.10
WITHIN SPECS, OK for transfer ppm Fe, max 10 10
SODIUM HYPOCHLORITE
Analyzed by Certified Correct % NaOCl 7.40 - 8.00
(Original copy signed) (Original copy signed)
% excess NaOH 0.40 - 1.00
ANB OVA SG @ 30”C, min 1.108
MVC-QF-TECH-008(24) QUALITY CONTROL DAILY ANALYSIS REPORT
Effectivity Date: October 1, 2016 MABUHAY VINYL CORPORATION
Date : 05/01/17 Time : 11:30 AM [ ]QC [ ]Technical [ ]IEM1/IEM2 [ ]AVP-Mfg
IEM 1 IEM 2
50 % CAUSTIC SODA 50 % CAUSTIC SODA Specs
Online Tk – A Tk - B Online Tk - 9
% NaOH NA NA NA 48.00-50.00
32 % CAUSTIC SODA 32 % CAUSTIC SODA
Online Tk – A Tk - B Online Tk - 8
% NaOH NA NA NA 30.00-32.00
HYDROCHLORIC ACID HYDROCHLORIC ACID
Online Tk- Tk- Online CTA 2
% HCl NA 32.00-33.50
Color # 3, max
POLISHED BRINE(After Precoat) POLISHED BRINE(After Precoat)
Ca+Mg, ppm + NA = + NA = 5.0 ppm,max.
SPB (After Headtank) SPB (After Headtank)
Ca+Mg, ppb nil + nil = nil nil + nil = nil 20 ppb, max.
NaCl, gpl NA NA 290 gpl,min.
Na2SO4,gpl NA NA 7 gpl, max.
NaClO3,gpl NA NA 20 gpl,max.
DEPLETED BRINE DEPLETED BRINE
NaCl, gpl 200 gpl, min.
Free Cl2 negative negative Negative
NaClO3,gpl NA NA 20 gpl, max.
pH NA NA 2.0, max
S O D I U M H Y P O C H L O R I T E PLANT
Tank No. 1 2 3 6 7
% NaOCl NA NA NA NA NA 7.40-8.00
% NaOH 0.40-1.00
Sp. Gravity 1.108, min
LI Q U I D C H LO R I N E PLAN T
Specs
Source LCP Tk.# Cl2 Feed LCP Tk # Cl2 Feed SULFURIC ACID
% Cl2 NA NA 99.5% min 91.0% min Source % H2SO4 Specs
% H2 NA NA NA NA LCP Comp. NA 97.0% min
UTILITIES
INSTRUMENT AIR @ AM Specs BOILER WATER Specs
Dew Point, °C ≤3.8 °C SiO2, ppm NA 150 ppm, max.
GAS ANALYSIS
IEM 1 IEM 2 FLUE GAS
% Cl2 % H2 O2 + CO2 % Cl2 % H2 O2 + CO2 % CO % CO2 % O2
Line A NA NA NA
Line B
POLLUTION C O N T R O L - EFFLUENTS
pH OIL Hg TDS TSS Color COD
Source 6AM 7PM (+ or -) ppb ppm mg/L Pt-Co Units mg/L
S-2 - NA NA NA NA NA
S-5 NA - NA NA NA NA NA
S-8 NA - NA NA NA NA NA
S-9 NA - NA NA NA NA NA
Lagoon NA NA NA NA NA NA NA
Source pH gpl NaOH Source pH SPECIFICATIONS
JBC NA S-3 NA pH = 6-9 COD = 100 mg/li, max Hg = 4 ppb, max.
Evap Canal S-4 Oil = Negative TDS = 1000 ppm, max TSS = 100 mg/li, max
Total Canal S-7 Color = 150 Pt-Co units, max.

Remarks: IEM 1 : NaOH- online(50%); SPB - Ca+Mg, NaCl; Depleted brine - Free
Analyzed
Cl2 by Certified Correct
OFF-SPECS IEM 2 : SPB - Ca+Mg, Na2SO4; Depleted brine - Free Cl2, NaClO3 (Original copy signed) (Original copy signed)

Others : Instrument Air - dewpoint; Effluents - S8(pH), S9(Color) NEY/ANB/RGD OVA


MVC-QF-TECH-004 (13)
Effectivity Date: August 5, 2014

MABUHAY VINYL CORPORATION PRODUCT TRANSFER CLEARANCE


Assumption Heights, Iligan City

Date : 05/01/17 [ ] IEM 1 [ ] IEM 2 [ ] Mktg [ ] QC file


IEM 1
HYDROCHLORIC ACID LIQUID CAUSTIC SODA SODIUM HYPOCHLORITE
Tk # % HCl SG @ 30”C Color Tk # 50% 32%. Tk # % NaOCl % NaOH SG @ 30”C
1 NA A NA NA 1 NA 0.00 0.000
2 NA B NA NA 2 NA 0.00 0.000
3 NA 3 NA 0.00 0.000
4 NA 6 NA 0.00 0.000
5 NA 7 NA 0.00 0.000
IEM 2 SPECIFICATIONS
HYDROCHLORIC ACID LIQUID CAUSTIC SODA HYDROCHLORIC ACID
Tk # % HCl SG @ 30”C Color Tk # 50% 32%. % HCl 32.00 - 33.50
CTA 1 NA 9 NA - SG @ 30”C, min 1.152
CTA 2 NA 8 - NA Color, max #3
CTA 3 NA LIQUID CAUSTIC SODA
CTB 1 NA 50% 32%
CTB 2 NA % NaOH 48.0-50.0 30.0 - 32.0
Remarks: % NaCl 0.10 0.10
WITHIN SPECS, OK for transfer ppm Fe, max 10 10
SODIUM HYPOCHLORITE
Analyzed by Certified Correct % NaOCl 7.40 - 8.00
(Original copy signed) (Original copy signed)
% excess NaOH 0.40 - 1.00
ANB OVA SG @ 30”C, min 1.108
MVC-QF-TECH-008(24) QUALITY CONTROL DAILY ANALYSIS REPORT
Effectivity Date: October 1, 2016 MABUHAY VINYL CORPORATION
Date : 05/02/17 Time : 11:30 AM [ ]QC [ ]Technical [ ]IEM1/IEM2 [ ]AVP-Mfg
IEM 1 IEM 2
50 % CAUSTIC SODA 50 % CAUSTIC SODA Specs
Online Tk – A Tk - B Online Tk - 9
% NaOH NA NA NA 48.00-50.00
32 % CAUSTIC SODA 32 % CAUSTIC SODA
Online Tk – A Tk - B Online Tk - 8
% NaOH NA NA NA 30.00-32.00
HYDROCHLORIC ACID HYDROCHLORIC ACID
Online Tk- Tk- Online CTA 2
% HCl NA 32.00-33.50
Color # 3, max
POLISHED BRINE(After Precoat) POLISHED BRINE(After Precoat)
Ca+Mg, ppm + NA = + NA = 5.0 ppm,max.
SPB (After Headtank) SPB (After Headtank)
Ca+Mg, ppb nil + nil = nil nil + nil = nil 20 ppb, max.
NaCl, gpl NA NA 290 gpl,min.
Na2SO4,gpl NA NA 7 gpl, max.
NaClO3,gpl NA NA 20 gpl,max.
DEPLETED BRINE DEPLETED BRINE
NaCl, gpl 200 gpl, min.
Free Cl2 negative negative Negative
NaClO3,gpl NA NA 20 gpl, max.
pH NA NA 2.0, max
S O D I U M H Y P O C H L O R I T E PLANT
Tank No. 1 2 3 6 7
% NaOCl NA NA NA NA NA 7.40-8.00
% NaOH 0.40-1.00
Sp. Gravity 1.108, min
LI Q U I D C H LO R I N E PLAN T
Specs
Source LCP Tk.# Cl2 Feed LCP Tk # Cl2 Feed SULFURIC ACID
% Cl2 NA NA 99.5% min 91.0% min Source % H2SO4 Specs
% H2 NA NA NA NA LCP Comp. NA 97.0% min
UTILITIES
INSTRUMENT AIR @ AM Specs BOILER WATER Specs
Dew Point, °C ≤3.8 °C SiO2, ppm NA 150 ppm, max.
GAS ANALYSIS
IEM 1 IEM 2 FLUE GAS
% Cl2 % H2 O2 + CO2 % Cl2 % H2 O2 + CO2 % CO % CO2 % O2
Line A NA NA NA
Line B
POLLUTION C O N T R O L - EFFLUENTS
pH OIL Hg TDS TSS Color COD
Source 6AM 7PM (+ or -) ppb ppm mg/L Pt-Co Units mg/L
S-2 - NA NA NA NA NA
S-5 NA - NA NA NA NA NA
S-8 NA - NA NA NA NA NA
S-9 NA - NA NA NA NA NA
Lagoon NA NA NA NA NA NA NA
Source pH gpl NaOH Source pH SPECIFICATIONS
JBC NA S-3 NA pH = 6-9 COD = 100 mg/li, max Hg = 4 ppb, max.
Evap Canal S-4 Oil = Negative TDS = 1000 ppm, max TSS = 100 mg/li, max
Total Canal S-7 Color = 150 Pt-Co units, max.

Remarks: IEM 1 : NaOH- online(50%); SPB - Ca+Mg, NaCl; Depleted brine - Free
Analyzed
Cl2 by Certified Correct
OFF-SPECS IEM 2 : SPB - Ca+Mg, Na2SO4; Depleted brine - Free Cl2, NaClO3 (Original copy signed) (Original copy signed)

Others : Instrument Air - dewpoint; Effluents - S8(pH), S9(Color) NEY/ANB/RGD OVA


MVC-QF-TECH-004 (13)
Effectivity Date: August 5, 2014

MABUHAY VINYL CORPORATION PRODUCT TRANSFER CLEARANCE


Assumption Heights, Iligan City

Date : 05/02/17 [ ] IEM 1 [ ] IEM 2 [ ] Mktg [ ] QC file


IEM 1
HYDROCHLORIC ACID LIQUID CAUSTIC SODA SODIUM HYPOCHLORITE
Tk # % HCl SG @ 30”C Color Tk # 50% 32%. Tk # % NaOCl % NaOH SG @ 30”C
1 NA A NA NA 1 NA 0.00 0.000
2 NA B NA NA 2 NA 0.00 0.000
3 NA 3 NA 0.00 0.000
4 NA 6 NA 0.00 0.000
5 NA 7 NA 0.00 0.000
IEM 2 SPECIFICATIONS
HYDROCHLORIC ACID LIQUID CAUSTIC SODA HYDROCHLORIC ACID
Tk # % HCl SG @ 30”C Color Tk # 50% 32%. % HCl 32.00 - 33.50
CTA 1 NA 9 NA - SG @ 30”C, min 1.152
CTA 2 NA 8 - NA Color, max #3
CTA 3 NA LIQUID CAUSTIC SODA
CTB 1 NA 50% 32%
CTB 2 NA % NaOH 48.0-50.0 30.0 - 32.0
Remarks: % NaCl 0.10 0.10
WITHIN SPECS, OK for transfer ppm Fe, max 10 10
SODIUM HYPOCHLORITE
Analyzed by Certified Correct % NaOCl 7.40 - 8.00
(Original copy signed) (Original copy signed)
% excess NaOH 0.40 - 1.00
ANB OVA SG @ 30”C, min 1.108
MVC-QF-TECH-008(24) QUALITY CONTROL DAILY ANALYSIS REPORT
Effectivity Date: October 1, 2016 MABUHAY VINYL CORPORATION
Date : 05/03/17 Time : 11:30 AM [ ]QC [ ]Technical [ ]IEM1/IEM2 [ ]AVP-Mfg
IEM 1 IEM 2
50 % CAUSTIC SODA 50 % CAUSTIC SODA Specs
Online Tk – A Tk - B Online Tk - 9
% NaOH NA NA NA 48.00-50.00
32 % CAUSTIC SODA 32 % CAUSTIC SODA
Online Tk – A Tk - B Online Tk - 8
% NaOH NA NA NA 30.00-32.00
HYDROCHLORIC ACID HYDROCHLORIC ACID
Online Tk- Tk- Online CTA 2
% HCl NA 32.00-33.50
Color # 3, max
POLISHED BRINE(After Precoat) POLISHED BRINE(After Precoat)
Ca+Mg, ppm + NA = + NA = 5.0 ppm,max.
SPB (After Headtank) SPB (After Headtank)
Ca+Mg, ppb nil + nil = nil nil + nil = nil 20 ppb, max.
NaCl, gpl NA NA 290 gpl,min.
Na2SO4,gpl NA NA 7 gpl, max.
NaClO3,gpl NA NA 20 gpl,max.
DEPLETED BRINE DEPLETED BRINE
NaCl, gpl 200 gpl, min.
Free Cl2 negative negative Negative
NaClO3,gpl NA NA 20 gpl, max.
pH NA NA 2.0, max
S O D I U M H Y P O C H L O R I T E PLANT
Tank No. 1 2 3 6 7
% NaOCl NA NA NA NA NA 7.40-8.00
% NaOH 0.40-1.00
Sp. Gravity 1.108, min
LI Q U I D C H LO R I N E PLAN T
Specs
Source LCP Tk.# Cl2 Feed LCP Tk # Cl2 Feed SULFURIC ACID
% Cl2 NA NA 99.5% min 91.0% min Source % H2SO4 Specs
% H2 NA NA NA NA LCP Comp. NA 97.0% min
UTILITIES
INSTRUMENT AIR @ AM Specs BOILER WATER Specs
Dew Point, °C ≤3.8 °C SiO2, ppm NA 150 ppm, max.
GAS ANALYSIS
IEM 1 IEM 2 FLUE GAS
% Cl2 % H2 O2 + CO2 % Cl2 % H2 O2 + CO2 % CO % CO2 % O2
Line A NA NA NA
Line B
POLLUTION C O N T R O L - EFFLUENTS
pH OIL Hg TDS TSS Color COD
Source 6AM 7PM (+ or -) ppb ppm mg/L Pt-Co Units mg/L
S-2 - NA NA NA NA NA
S-5 NA - NA NA NA NA NA
S-8 NA - NA NA NA NA NA
S-9 NA - NA NA NA NA NA
Lagoon NA NA NA NA NA NA NA
Source pH gpl NaOH Source pH SPECIFICATIONS
JBC NA S-3 NA pH = 6-9 COD = 100 mg/li, max Hg = 4 ppb, max.
Evap Canal S-4 Oil = Negative TDS = 1000 ppm, max TSS = 100 mg/li, max
Total Canal S-7 Color = 150 Pt-Co units, max.

Remarks: IEM 1 : NaOH- online(50%); SPB - Ca+Mg, NaCl; Depleted brine - Free
Analyzed
Cl2 by Certified Correct
OFF-SPECS IEM 2 : SPB - Ca+Mg, Na2SO4; Depleted brine - Free Cl2, NaClO3 (Original copy signed) (Original copy signed)

Others : Instrument Air - dewpoint; Effluents - S8(pH), S9(Color) NEY/ANB/RGD OVA


MVC-QF-TECH-004 (13)
Effectivity Date: August 5, 2014

MABUHAY VINYL CORPORATION PRODUCT TRANSFER CLEARANCE


Assumption Heights, Iligan City

Date : 05/03/17 [ ] IEM 1 [ ] IEM 2 [ ] Mktg [ ] QC file


IEM 1
HYDROCHLORIC ACID LIQUID CAUSTIC SODA SODIUM HYPOCHLORITE
Tk # % HCl SG @ 30”C Color Tk # 50% 32%. Tk # % NaOCl % NaOH SG @ 30”C
1 NA A NA NA 1 NA 0.00 0.000
2 NA B NA NA 2 NA 0.00 0.000
3 NA 3 NA 0.00 0.000
4 NA 6 NA 0.00 0.000
5 NA 7 NA 0.00 0.000
IEM 2 SPECIFICATIONS
HYDROCHLORIC ACID LIQUID CAUSTIC SODA HYDROCHLORIC ACID
Tk # % HCl SG @ 30”C Color Tk # 50% 32%. % HCl 32.00 - 33.50
CTA 1 NA 9 NA - SG @ 30”C, min 1.152
CTA 2 NA 8 - NA Color, max #3
CTA 3 NA LIQUID CAUSTIC SODA
CTB 1 NA 50% 32%
CTB 2 NA % NaOH 48.0-50.0 30.0 - 32.0
Remarks: % NaCl 0.10 0.10
WITHIN SPECS, OK for transfer ppm Fe, max 10 10
SODIUM HYPOCHLORITE
Analyzed by Certified Correct % NaOCl 7.40 - 8.00
(Original copy signed) (Original copy signed)
% excess NaOH 0.40 - 1.00
ANB OVA SG @ 30”C, min 1.108
MVC-QF-TECH-008(24) QUALITY CONTROL DAILY ANALYSIS REPORT
Effectivity Date: October 1, 2016 MABUHAY VINYL CORPORATION
Date : 05/04/17 Time : 11:30 AM [ ]QC [ ]Technical [ ]IEM1/IEM2 [ ]AVP-Mfg
IEM 1 IEM 2
50 % CAUSTIC SODA 50 % CAUSTIC SODA Specs
Online Tk – A Tk - B Online Tk - 9
% NaOH NA NA NA 48.00-50.00
32 % CAUSTIC SODA 32 % CAUSTIC SODA
Online Tk – A Tk - B Online Tk - 8
% NaOH NA NA NA 30.00-32.00
HYDROCHLORIC ACID HYDROCHLORIC ACID
Online Tk- Tk- Online CTA 2
% HCl NA 32.00-33.50
Color # 3, max
POLISHED BRINE(After Precoat) POLISHED BRINE(After Precoat)
Ca+Mg, ppm + NA = + NA = 5.0 ppm,max.
SPB (After Headtank) SPB (After Headtank)
Ca+Mg, ppb nil + nil = nil nil + nil = nil 20 ppb, max.
NaCl, gpl NA NA 290 gpl,min.
Na2SO4,gpl NA NA 7 gpl, max.
NaClO3,gpl NA NA 20 gpl,max.
DEPLETED BRINE DEPLETED BRINE
NaCl, gpl 200 gpl, min.
Free Cl2 negative negative Negative
NaClO3,gpl NA NA 20 gpl, max.
pH NA NA 2.0, max
S O D I U M H Y P O C H L O R I T E PLANT
Tank No. 1 2 3 6 7
% NaOCl NA NA NA NA NA 7.40-8.00
% NaOH 0.40-1.00
Sp. Gravity 1.108, min
LI Q U I D C H LO R I N E PLAN T
Specs
Source LCP Tk.# Cl2 Feed LCP Tk # Cl2 Feed SULFURIC ACID
% Cl2 NA NA 99.5% min 91.0% min Source % H2SO4 Specs
% H2 NA NA NA NA LCP Comp. NA 97.0% min
UTILITIES
INSTRUMENT AIR @ AM Specs BOILER WATER Specs
Dew Point, °C ≤3.8 °C SiO2, ppm NA 150 ppm, max.
GAS ANALYSIS
IEM 1 IEM 2 FLUE GAS
% Cl2 % H2 O2 + CO2 % Cl2 % H2 O2 + CO2 % CO % CO2 % O2
Line A NA NA NA
Line B
POLLUTION C O N T R O L - EFFLUENTS
pH OIL Hg TDS TSS Color COD
Source 6AM 7PM (+ or -) ppb ppm mg/L Pt-Co Units mg/L
S-2 - NA NA NA NA NA
S-5 NA - NA NA NA NA NA
S-8 NA - NA NA NA NA NA
S-9 NA - NA NA NA NA NA
Lagoon NA NA NA NA NA NA NA
Source pH gpl NaOH Source pH SPECIFICATIONS
JBC NA S-3 NA pH = 6-9 COD = 100 mg/li, max Hg = 4 ppb, max.
Evap Canal S-4 Oil = Negative TDS = 1000 ppm, max TSS = 100 mg/li, max
Total Canal S-7 Color = 150 Pt-Co units, max.

Remarks: IEM 1 : NaOH- online(50%); SPB - Ca+Mg, NaCl; Depleted brine - Free
Analyzed
Cl2 by Certified Correct
OFF-SPECS IEM 2 : SPB - Ca+Mg, Na2SO4; Depleted brine - Free Cl2, NaClO3 (Original copy signed) (Original copy signed)

Others : Instrument Air - dewpoint; Effluents - S8(pH), S9(Color) NEY/ANB/RGD OVA


MVC-QF-TECH-004 (13)
Effectivity Date: August 5, 2014

MABUHAY VINYL CORPORATION PRODUCT TRANSFER CLEARANCE


Assumption Heights, Iligan City

Date : 05/04/17 [ ] IEM 1 [ ] IEM 2 [ ] Mktg [ ] QC file


IEM 1
HYDROCHLORIC ACID LIQUID CAUSTIC SODA SODIUM HYPOCHLORITE
Tk # % HCl SG @ 30”C Color Tk # 50% 32%. Tk # % NaOCl % NaOH SG @ 30”C
1 NA A NA NA 1 NA 0.00 0.000
2 NA B NA NA 2 NA 0.00 0.000
3 NA 3 NA 0.00 0.000
4 NA 6 NA 0.00 0.000
5 NA 7 NA 0.00 0.000
IEM 2 SPECIFICATIONS
HYDROCHLORIC ACID LIQUID CAUSTIC SODA HYDROCHLORIC ACID
Tk # % HCl SG @ 30”C Color Tk # 50% 32%. % HCl 32.00 - 33.50
CTA 1 NA 9 NA - SG @ 30”C, min 1.152
CTA 2 NA 8 - NA Color, max #3
CTA 3 NA LIQUID CAUSTIC SODA
CTB 1 NA 50% 32%
CTB 2 NA % NaOH 48.0-50.0 30.0 - 32.0
Remarks: % NaCl 0.10 0.10
WITHIN SPECS, OK for transfer ppm Fe, max 10 10
SODIUM HYPOCHLORITE
Analyzed by Certified Correct % NaOCl 7.40 - 8.00
(Original copy signed) (Original copy signed)
% excess NaOH 0.40 - 1.00
ANB OVA SG @ 30”C, min 1.108
MVC-QF-TECH-008(24) QUALITY CONTROL DAILY ANALYSIS REPORT
Effectivity Date: October 1, 2016 MABUHAY VINYL CORPORATION
Date : 05/05/17 Time : 11:30 AM [ ]QC [ ]Technical [ ]IEM1/IEM2 [ ]AVP-Mfg
IEM 1 IEM 2
50 % CAUSTIC SODA 50 % CAUSTIC SODA Specs
Online Tk – A Tk - B Online Tk - 9
% NaOH NA NA NA 48.00-50.00
32 % CAUSTIC SODA 32 % CAUSTIC SODA
Online Tk – A Tk - B Online Tk - 8
% NaOH NA NA NA 30.00-32.00
HYDROCHLORIC ACID HYDROCHLORIC ACID
Online Tk- Tk- Online CTA 2
% HCl NA 32.00-33.50
Color # 3, max
POLISHED BRINE(After Precoat) POLISHED BRINE(After Precoat)
Ca+Mg, ppm + NA = + NA = 5.0 ppm,max.
SPB (After Headtank) SPB (After Headtank)
Ca+Mg, ppb nil + nil = nil nil + nil = nil 20 ppb, max.
NaCl, gpl NA NA 290 gpl,min.
Na2SO4,gpl NA NA 7 gpl, max.
NaClO3,gpl NA NA 20 gpl,max.
DEPLETED BRINE DEPLETED BRINE
NaCl, gpl 200 gpl, min.
Free Cl2 negative negative Negative
NaClO3,gpl NA NA 20 gpl, max.
pH NA NA 2.0, max
S O D I U M H Y P O C H L O R I T E PLANT
Tank No. 1 2 3 6 7
% NaOCl NA NA NA NA NA 7.40-8.00
% NaOH 0.40-1.00
Sp. Gravity 1.108, min
LI Q U I D C H LO R I N E PLAN T
Specs
Source LCP Tk.# Cl2 Feed LCP Tk # Cl2 Feed SULFURIC ACID
% Cl2 NA NA 99.5% min 91.0% min Source % H2SO4 Specs
% H2 NA NA NA NA LCP Comp. NA 97.0% min
UTILITIES
INSTRUMENT AIR @ AM Specs BOILER WATER Specs
Dew Point, °C ≤3.8 °C SiO2, ppm NA 150 ppm, max.
GAS ANALYSIS
IEM 1 IEM 2 FLUE GAS
% Cl2 % H2 O2 + CO2 % Cl2 % H2 O2 + CO2 % CO % CO2 % O2
Line A NA NA NA
Line B
POLLUTION C O N T R O L - EFFLUENTS
pH OIL Hg TDS TSS Color COD
Source 6AM 7PM (+ or -) ppb ppm mg/L Pt-Co Units mg/L
S-2 - NA NA NA NA NA
S-5 NA - NA NA NA NA NA
S-8 NA - NA NA NA NA NA
S-9 NA - NA NA NA NA NA
Lagoon NA NA NA NA NA NA NA
Source pH gpl NaOH Source pH SPECIFICATIONS
JBC NA S-3 NA pH = 6-9 COD = 100 mg/li, max Hg = 4 ppb, max.
Evap Canal S-4 Oil = Negative TDS = 1000 ppm, max TSS = 100 mg/li, max
Total Canal S-7 Color = 150 Pt-Co units, max.

Remarks: IEM 1 : NaOH- online(50%); SPB - Ca+Mg, NaCl; Depleted brine - Free
Analyzed
Cl2 by Certified Correct
OFF-SPECS IEM 2 : SPB - Ca+Mg, Na2SO4; Depleted brine - Free Cl2, NaClO3 (Original copy signed) (Original copy signed)

Others : Instrument Air - dewpoint; Effluents - S8(pH), S9(Color) NEY/ANB/RGD OVA


MVC-QF-TECH-004 (13)
Effectivity Date: August 5, 2014

MABUHAY VINYL CORPORATION PRODUCT TRANSFER CLEARANCE


Assumption Heights, Iligan City

Date : 05/05/17 [ ] IEM 1 [ ] IEM 2 [ ] Mktg [ ] QC file


IEM 1
HYDROCHLORIC ACID LIQUID CAUSTIC SODA SODIUM HYPOCHLORITE
Tk # % HCl SG @ 30”C Color Tk # 50% 32%. Tk # % NaOCl % NaOH SG @ 30”C
1 NA A NA NA 1 NA 0.00 0.000
2 NA B NA NA 2 NA 0.00 0.000
3 NA 3 NA 0.00 0.000
4 NA 6 NA 0.00 0.000
5 NA 7 NA 0.00 0.000
IEM 2 SPECIFICATIONS
HYDROCHLORIC ACID LIQUID CAUSTIC SODA HYDROCHLORIC ACID
Tk # % HCl SG @ 30”C Color Tk # 50% 32%. % HCl 32.00 - 33.50
CTA 1 NA 9 NA - SG @ 30”C, min 1.152
CTA 2 NA 8 - NA Color, max #3
CTA 3 NA LIQUID CAUSTIC SODA
CTB 1 NA 50% 32%
CTB 2 NA % NaOH 48.0-50.0 30.0 - 32.0
Remarks: % NaCl 0.10 0.10
WITHIN SPECS, OK for transfer ppm Fe, max 10 10
SODIUM HYPOCHLORITE
Analyzed by Certified Correct % NaOCl 7.40 - 8.00
(Original copy signed) (Original copy signed)
% excess NaOH 0.40 - 1.00
ANB OVA SG @ 30”C, min 1.108
MVC-QF-TECH-008(24) QUALITY CONTROL DAILY ANALYSIS REPORT
Effectivity Date: October 1, 2016 MABUHAY VINYL CORPORATION
Date : 05/06/17 Time : 11:30 AM [ ]QC [ ]Technical [ ]IEM1/IEM2 [ ]AVP-Mfg
IEM 1 IEM 2
50 % CAUSTIC SODA 50 % CAUSTIC SODA Specs
Online Tk – A Tk - B Online Tk - 9
% NaOH NA NA NA 48.00-50.00
32 % CAUSTIC SODA 32 % CAUSTIC SODA
Online Tk – A Tk - B Online Tk - 8
% NaOH NA NA NA 30.00-32.00
HYDROCHLORIC ACID HYDROCHLORIC ACID
Online Tk- Tk- Online CTA 2
% HCl NA 32.00-33.50
Color # 3, max
POLISHED BRINE(After Precoat) POLISHED BRINE(After Precoat)
Ca+Mg, ppm + NA = + NA = 5.0 ppm,max.
SPB (After Headtank) SPB (After Headtank)
Ca+Mg, ppb nil + nil = nil nil + nil = nil 20 ppb, max.
NaCl, gpl NA NA 290 gpl,min.
Na2SO4,gpl NA NA 7 gpl, max.
NaClO3,gpl NA NA 20 gpl,max.
DEPLETED BRINE DEPLETED BRINE
NaCl, gpl 200 gpl, min.
Free Cl2 negative negative Negative
NaClO3,gpl NA NA 20 gpl, max.
pH NA NA 2.0, max
S O D I U M H Y P O C H L O R I T E PLANT
Tank No. 1 2 3 6 7
% NaOCl NA NA NA NA NA 7.40-8.00
% NaOH 0.40-1.00
Sp. Gravity 1.108, min
LI Q U I D C H LO R I N E PLAN T
Specs
Source LCP Tk.# Cl2 Feed LCP Tk # Cl2 Feed SULFURIC ACID
% Cl2 NA NA 99.5% min 91.0% min Source % H2SO4 Specs
% H2 NA NA NA NA LCP Comp. NA 97.0% min
UTILITIES
INSTRUMENT AIR @ AM Specs BOILER WATER Specs
Dew Point, °C ≤3.8 °C SiO2, ppm NA 150 ppm, max.
GAS ANALYSIS
IEM 1 IEM 2 FLUE GAS
% Cl2 % H2 O2 + CO2 % Cl2 % H2 O2 + CO2 % CO % CO2 % O2
Line A NA NA NA
Line B
POLLUTION C O N T R O L - EFFLUENTS
pH OIL Hg TDS TSS Color COD
Source 6AM 7PM (+ or -) ppb ppm mg/L Pt-Co Units mg/L
S-2 - NA NA NA NA NA
S-5 NA - NA NA NA NA NA
S-8 NA - NA NA NA NA NA
S-9 NA - NA NA NA NA NA
Lagoon NA NA NA NA NA NA NA
Source pH gpl NaOH Source pH SPECIFICATIONS
JBC NA S-3 NA pH = 6-9 COD = 100 mg/li, max Hg = 4 ppb, max.
Evap Canal S-4 Oil = Negative TDS = 1000 ppm, max TSS = 100 mg/li, max
Total Canal S-7 Color = 150 Pt-Co units, max.

Remarks: IEM 1 : NaOH- online(50%); SPB - Ca+Mg, NaCl; Depleted brine - Free
Analyzed
Cl2 by Certified Correct
OFF-SPECS IEM 2 : SPB - Ca+Mg, Na2SO4; Depleted brine - Free Cl2, NaClO3 (Original copy signed) (Original copy signed)

Others : Instrument Air - dewpoint; Effluents - S8(pH), S9(Color) NEY/ANB/RGD OVA


MVC-QF-TECH-004 (13)
Effectivity Date: August 5, 2014

MABUHAY VINYL CORPORATION PRODUCT TRANSFER CLEARANCE


Assumption Heights, Iligan City

Date : 05/06/17 [ ] IEM 1 [ ] IEM 2 [ ] Mktg [ ] QC file


IEM 1
HYDROCHLORIC ACID LIQUID CAUSTIC SODA SODIUM HYPOCHLORITE
Tk # % HCl SG @ 30”C Color Tk # 50% 32%. Tk # % NaOCl % NaOH SG @ 30”C
1 NA A NA NA 1 NA 0.00 0.000
2 NA B NA NA 2 NA 0.00 0.000
3 NA 3 NA 0.00 0.000
4 NA 6 NA 0.00 0.000
5 NA 7 NA 0.00 0.000
IEM 2 SPECIFICATIONS
HYDROCHLORIC ACID LIQUID CAUSTIC SODA HYDROCHLORIC ACID
Tk # % HCl SG @ 30”C Color Tk # 50% 32%. % HCl 32.00 - 33.50
CTA 1 NA 9 NA - SG @ 30”C, min 1.152
CTA 2 NA 8 - NA Color, max #3
CTA 3 NA LIQUID CAUSTIC SODA
CTB 1 NA 50% 32%
CTB 2 NA % NaOH 48.0-50.0 30.0 - 32.0
Remarks: % NaCl 0.10 0.10
WITHIN SPECS, OK for transfer ppm Fe, max 10 10
SODIUM HYPOCHLORITE
Analyzed by Certified Correct % NaOCl 7.40 - 8.00
(Original copy signed) (Original copy signed)
% excess NaOH 0.40 - 1.00
ANB OVA SG @ 30”C, min 1.108
MVC-QF-TECH-008(24) QUALITY CONTROL DAILY ANALYSIS REPORT
Effectivity Date: October 1, 2016 MABUHAY VINYL CORPORATION
Date : 05/07/17 Time : 11:30 AM [ ]QC [ ]Technical [ ]IEM1/IEM2 [ ]AVP-Mfg
IEM 1 IEM 2
50 % CAUSTIC SODA 50 % CAUSTIC SODA Specs
Online Tk – A Tk - B Online Tk - 9
% NaOH NA NA NA 48.00-50.00
32 % CAUSTIC SODA 32 % CAUSTIC SODA
Online Tk – A Tk - B Online Tk - 8
% NaOH NA NA NA 30.00-32.00
HYDROCHLORIC ACID HYDROCHLORIC ACID
Online Tk- Tk- Online CTA 2
% HCl NA 32.00-33.50
Color # 3, max
POLISHED BRINE(After Precoat) POLISHED BRINE(After Precoat)
Ca+Mg, ppm + NA = + NA = 5.0 ppm,max.
SPB (After Headtank) SPB (After Headtank)
Ca+Mg, ppb nil + nil = nil nil + nil = nil 20 ppb, max.
NaCl, gpl NA NA 290 gpl,min.
Na2SO4,gpl NA NA 7 gpl, max.
NaClO3,gpl NA NA 20 gpl,max.
DEPLETED BRINE DEPLETED BRINE
NaCl, gpl 200 gpl, min.
Free Cl2 negative negative Negative
NaClO3,gpl NA NA 20 gpl, max.
pH NA NA 2.0, max
S O D I U M H Y P O C H L O R I T E PLANT
Tank No. 1 2 3 6 7
% NaOCl NA NA NA NA NA 7.40-8.00
% NaOH 0.40-1.00
Sp. Gravity 1.108, min
LI Q U I D C H LO R I N E PLAN T
Specs
Source LCP Tk.# Cl2 Feed LCP Tk # Cl2 Feed SULFURIC ACID
% Cl2 NA NA 99.5% min 91.0% min Source % H2SO4 Specs
% H2 NA NA NA NA LCP Comp. NA 97.0% min
UTILITIES
INSTRUMENT AIR @ AM Specs BOILER WATER Specs
Dew Point, °C ≤3.8 °C SiO2, ppm NA 150 ppm, max.
GAS ANALYSIS
IEM 1 IEM 2 FLUE GAS
% Cl2 % H2 O2 + CO2 % Cl2 % H2 O2 + CO2 % CO % CO2 % O2
Line A NA NA NA
Line B
POLLUTION C O N T R O L - EFFLUENTS
pH OIL Hg TDS TSS Color COD
Source 6AM 7PM (+ or -) ppb ppm mg/L Pt-Co Units mg/L
S-2 - NA NA NA NA NA
S-5 NA - NA NA NA NA NA
S-8 NA - NA NA NA NA NA
S-9 NA - NA NA NA NA NA
Lagoon NA NA NA NA NA NA NA
Source pH gpl NaOH Source pH SPECIFICATIONS
JBC NA S-3 NA pH = 6-9 COD = 100 mg/li, max Hg = 4 ppb, max.
Evap Canal S-4 Oil = Negative TDS = 1000 ppm, max TSS = 100 mg/li, max
Total Canal S-7 Color = 150 Pt-Co units, max.

Remarks: IEM 1 : NaOH- online(50%); SPB - Ca+Mg, NaCl; Depleted brine - Free
Analyzed
Cl2 by Certified Correct
OFF-SPECS IEM 2 : SPB - Ca+Mg, Na2SO4; Depleted brine - Free Cl2, NaClO3 (Original copy signed) (Original copy signed)

Others : Instrument Air - dewpoint; Effluents - S8(pH), S9(Color) NEY/ANB/RGD OVA


MVC-QF-TECH-004 (13)
Effectivity Date: August 5, 2014

MABUHAY VINYL CORPORATION PRODUCT TRANSFER CLEARANCE


Assumption Heights, Iligan City

Date : 05/07/17 [ ] IEM 1 [ ] IEM 2 [ ] Mktg [ ] QC file


IEM 1
HYDROCHLORIC ACID LIQUID CAUSTIC SODA SODIUM HYPOCHLORITE
Tk # % HCl SG @ 30”C Color Tk # 50% 32%. Tk # % NaOCl % NaOH SG @ 30”C
1 NA A NA NA 1 NA 0.00 0.000
2 NA B NA NA 2 NA 0.00 0.000
3 NA 3 NA 0.00 0.000
4 NA 6 NA 0.00 0.000
5 NA 7 NA 0.00 0.000
IEM 2 SPECIFICATIONS
HYDROCHLORIC ACID LIQUID CAUSTIC SODA HYDROCHLORIC ACID
Tk # % HCl SG @ 30”C Color Tk # 50% 32%. % HCl 32.00 - 33.50
CTA 1 NA 9 NA - SG @ 30”C, min 1.152
CTA 2 NA 8 - NA Color, max #3
CTA 3 NA LIQUID CAUSTIC SODA
CTB 1 NA 50% 32%
CTB 2 NA % NaOH 48.0-50.0 30.0 - 32.0
Remarks: % NaCl 0.10 0.10
WITHIN SPECS, OK for transfer ppm Fe, max 10 10
SODIUM HYPOCHLORITE
Analyzed by Certified Correct % NaOCl 7.40 - 8.00
(Original copy signed) (Original copy signed)
% excess NaOH 0.40 - 1.00
ANB OVA SG @ 30”C, min 1.108
MVC-QF-TECH-008(24) QUALITY CONTROL DAILY ANALYSIS REPORT
Effectivity Date: October 1, 2016 MABUHAY VINYL CORPORATION
Date : 05/08/17 Time : 11:30 AM [ ]QC [ ]Technical [ ]IEM1/IEM2 [ ]AVP-Mfg
IEM 1 IEM 2
50 % CAUSTIC SODA 50 % CAUSTIC SODA Specs
Online Tk – A Tk - B Online Tk - 9
% NaOH NA NA NA 48.00-50.00
32 % CAUSTIC SODA 32 % CAUSTIC SODA
Online Tk – A Tk - B Online Tk - 8
% NaOH NA NA NA 30.00-32.00
HYDROCHLORIC ACID HYDROCHLORIC ACID
Online Tk- Tk- Online CTA 2
% HCl NA 32.00-33.50
Color # 3, max
POLISHED BRINE(After Precoat) POLISHED BRINE(After Precoat)
Ca+Mg, ppm + NA = + NA = 5.0 ppm,max.
SPB (After Headtank) SPB (After Headtank)
Ca+Mg, ppb nil + nil = nil nil + nil = nil 20 ppb, max.
NaCl, gpl NA NA 290 gpl,min.
Na2SO4,gpl NA NA 7 gpl, max.
NaClO3,gpl NA NA 20 gpl,max.
DEPLETED BRINE DEPLETED BRINE
NaCl, gpl 200 gpl, min.
Free Cl2 negative negative Negative
NaClO3,gpl NA NA 20 gpl, max.
pH NA NA 2.0, max
S O D I U M H Y P O C H L O R I T E PLANT
Tank No. 1 2 3 6 7
% NaOCl NA NA NA NA NA 7.40-8.00
% NaOH 0.40-1.00
Sp. Gravity 1.108, min
LI Q U I D C H LO R I N E PLAN T
Specs
Source LCP Tk.# Cl2 Feed LCP Tk # Cl2 Feed SULFURIC ACID
% Cl2 NA NA 99.5% min 91.0% min Source % H2SO4 Specs
% H2 NA NA NA NA LCP Comp. NA 97.0% min
UTILITIES
INSTRUMENT AIR @ AM Specs BOILER WATER Specs
Dew Point, °C ≤3.8 °C SiO2, ppm NA 150 ppm, max.
GAS ANALYSIS
IEM 1 IEM 2 FLUE GAS
% Cl2 % H2 O2 + CO2 % Cl2 % H2 O2 + CO2 % CO % CO2 % O2
Line A NA NA NA
Line B
POLLUTION C O N T R O L - EFFLUENTS
pH OIL Hg TDS TSS Color COD
Source 6AM 7PM (+ or -) ppb ppm mg/L Pt-Co Units mg/L
S-2 - NA NA NA NA NA
S-5 NA - NA NA NA NA NA
S-8 NA - NA NA NA NA NA
S-9 NA - NA NA NA NA NA
Lagoon NA NA NA NA NA NA NA
Source pH gpl NaOH Source pH SPECIFICATIONS
JBC NA S-3 NA pH = 6-9 COD = 100 mg/li, max Hg = 4 ppb, max.
Evap Canal S-4 Oil = Negative TDS = 1000 ppm, max TSS = 100 mg/li, max
Total Canal S-7 Color = 150 Pt-Co units, max.

Remarks: IEM 1 : NaOH- online(50%); SPB - Ca+Mg, NaCl; Depleted brine - Free
Analyzed
Cl2 by Certified Correct
OFF-SPECS IEM 2 : SPB - Ca+Mg, Na2SO4; Depleted brine - Free Cl2, NaClO3 (Original copy signed) (Original copy signed)

Others : Instrument Air - dewpoint; Effluents - S8(pH), S9(Color) NEY/ANB/RGD OVA


MVC-QF-TECH-004 (13)
Effectivity Date: August 5, 2014

MABUHAY VINYL CORPORATION PRODUCT TRANSFER CLEARANCE


Assumption Heights, Iligan City

Date : 05/08/17 [ ] IEM 1 [ ] IEM 2 [ ] Mktg [ ] QC file


IEM 1
HYDROCHLORIC ACID LIQUID CAUSTIC SODA SODIUM HYPOCHLORITE
Tk # % HCl SG @ 30”C Color Tk # 50% 32%. Tk # % NaOCl % NaOH SG @ 30”C
1 NA A NA NA 1 NA 0.00 0.000
2 NA B NA NA 2 NA 0.00 0.000
3 NA 3 NA 0.00 0.000
4 NA 6 NA 0.00 0.000
5 NA 7 NA 0.00 0.000
IEM 2 SPECIFICATIONS
HYDROCHLORIC ACID LIQUID CAUSTIC SODA HYDROCHLORIC ACID
Tk # % HCl SG @ 30”C Color Tk # 50% 32%. % HCl 32.00 - 33.50
CTA 1 NA 9 NA - SG @ 30”C, min 1.152
CTA 2 NA 8 - NA Color, max #3
CTA 3 NA LIQUID CAUSTIC SODA
CTB 1 NA 50% 32%
CTB 2 NA % NaOH 48.0-50.0 30.0 - 32.0
Remarks: % NaCl 0.10 0.10
WITHIN SPECS, OK for transfer ppm Fe, max 10 10
SODIUM HYPOCHLORITE
Analyzed by Certified Correct % NaOCl 7.40 - 8.00
(Original copy signed) (Original copy signed)
% excess NaOH 0.40 - 1.00
ANB OVA SG @ 30”C, min 1.108
MVC-QF-TECH-008(24) QUALITY CONTROL DAILY ANALYSIS REPORT
Effectivity Date: October 1, 2016 MABUHAY VINYL CORPORATION
Date : 05/09/17 Time : 11:30 AM [ ]QC [ ]Technical [ ]IEM1/IEM2 [ ]AVP-Mfg
IEM 1 IEM 2
50 % CAUSTIC SODA 50 % CAUSTIC SODA Specs
Online Tk – A Tk - B Online Tk - 9
% NaOH NA NA NA 48.00-50.00
32 % CAUSTIC SODA 32 % CAUSTIC SODA
Online Tk – A Tk - B Online Tk - 8
% NaOH NA NA NA 30.00-32.00
HYDROCHLORIC ACID HYDROCHLORIC ACID
Online Tk- Tk- Online CTA 2
% HCl NA 32.00-33.50
Color # 3, max
POLISHED BRINE(After Precoat) POLISHED BRINE(After Precoat)
Ca+Mg, ppm + NA = + NA = 5.0 ppm,max.
SPB (After Headtank) SPB (After Headtank)
Ca+Mg, ppb nil + nil = nil nil + nil = nil 20 ppb, max.
NaCl, gpl NA NA 290 gpl,min.
Na2SO4,gpl NA NA 7 gpl, max.
NaClO3,gpl NA NA 20 gpl,max.
DEPLETED BRINE DEPLETED BRINE
NaCl, gpl 200 gpl, min.
Free Cl2 negative negative Negative
NaClO3,gpl NA NA 20 gpl, max.
pH NA NA 2.0, max
S O D I U M H Y P O C H L O R I T E PLANT
Tank No. 1 2 3 6 7
% NaOCl NA NA NA NA NA 7.40-8.00
% NaOH 0.40-1.00
Sp. Gravity 1.108, min
LI Q U I D C H LO R I N E PLAN T
Specs
Source LCP Tk.# Cl2 Feed LCP Tk # Cl2 Feed SULFURIC ACID
% Cl2 NA NA 99.5% min 91.0% min Source % H2SO4 Specs
% H2 NA NA NA NA LCP Comp. NA 97.0% min
UTILITIES
INSTRUMENT AIR @ AM Specs BOILER WATER Specs
Dew Point, °C ≤3.8 °C SiO2, ppm NA 150 ppm, max.
GAS ANALYSIS
IEM 1 IEM 2 FLUE GAS
% Cl2 % H2 O2 + CO2 % Cl2 % H2 O2 + CO2 % CO % CO2 % O2
Line A NA NA NA
Line B
POLLUTION C O N T R O L - EFFLUENTS
pH OIL Hg TDS TSS Color COD
Source 6AM 7PM (+ or -) ppb ppm mg/L Pt-Co Units mg/L
S-2 - NA NA NA NA NA
S-5 NA - NA NA NA NA NA
S-8 NA - NA NA NA NA NA
S-9 NA - NA NA NA NA NA
Lagoon NA NA NA NA NA NA NA
Source pH gpl NaOH Source pH SPECIFICATIONS
JBC NA S-3 NA pH = 6-9 COD = 100 mg/li, max Hg = 4 ppb, max.
Evap Canal S-4 Oil = Negative TDS = 1000 ppm, max TSS = 100 mg/li, max
Total Canal S-7 Color = 150 Pt-Co units, max.

Remarks: IEM 1 : NaOH- online(50%); SPB - Ca+Mg, NaCl; Depleted brine - Free
Analyzed
Cl2 by Certified Correct
OFF-SPECS IEM 2 : SPB - Ca+Mg, Na2SO4; Depleted brine - Free Cl2, NaClO3 (Original copy signed) (Original copy signed)

Others : Instrument Air - dewpoint; Effluents - S8(pH), S9(Color) NEY/ANB/RGD OVA


MVC-QF-TECH-004 (13)
Effectivity Date: August 5, 2014

MABUHAY VINYL CORPORATION PRODUCT TRANSFER CLEARANCE


Assumption Heights, Iligan City

Date : 05/09/17 [ ] IEM 1 [ ] IEM 2 [ ] Mktg [ ] QC file


IEM 1
HYDROCHLORIC ACID LIQUID CAUSTIC SODA SODIUM HYPOCHLORITE
Tk # % HCl SG @ 30”C Color Tk # 50% 32%. Tk # % NaOCl % NaOH SG @ 30”C
1 NA A NA NA 1 NA 0.00 0.000
2 NA B NA NA 2 NA 0.00 0.000
3 NA 3 NA 0.00 0.000
4 NA 6 NA 0.00 0.000
5 NA 7 NA 0.00 0.000
IEM 2 SPECIFICATIONS
HYDROCHLORIC ACID LIQUID CAUSTIC SODA HYDROCHLORIC ACID
Tk # % HCl SG @ 30”C Color Tk # 50% 32%. % HCl 32.00 - 33.50
CTA 1 NA 9 NA - SG @ 30”C, min 1.152
CTA 2 NA 8 - NA Color, max #3
CTA 3 NA LIQUID CAUSTIC SODA
CTB 1 NA 50% 32%
CTB 2 NA % NaOH 48.0-50.0 30.0 - 32.0
Remarks: % NaCl 0.10 0.10
WITHIN SPECS, OK for transfer ppm Fe, max 10 10
SODIUM HYPOCHLORITE
Analyzed by Certified Correct % NaOCl 7.40 - 8.00
(Original copy signed) (Original copy signed)
% excess NaOH 0.40 - 1.00
ANB OVA SG @ 30”C, min 1.108
50% NaOH 32% NaOH
IEM 1 IEM 2 IEM 1
WEEK DAY DATE Online Tk A Tk B Online Tank 9 Online Tk A
Wed 29-Mar 49.98 49.92 NA 49.59 NA NA NA
Thu 30-Mar 49.73 NA NA SD NA 31.15 NA
Fri 31-Mar 49.64 50.00 NA 51.59 48.26 30.07 NA
Sat 1-Apr 49.28 49.71 NA 49.09 NA 30.44 NA
Sun 2-Apr 49.81 49.87 NA SD NA 30.17 NA
Mon 3-Apr 0.00 NA NA 0.00 NA 0.00 NA
1 Tue 4-Apr 49.49 NA NA 51.50 48.83 30.45 NA
Wed 5-Apr 48.96 49.76 30.77
Thu 6-Apr 49.27 50.04 29.66
Fri 7-Apr 49.70
Sat 8-Apr 49.87 49.56 49.83 30.76
Sun 9-Apr 49.70 46.88 30.78
Mon 10-Apr 50.35 49.35 30.08
2 Tue 11-Apr 50.14 49.67 29.53
Wed 12-Apr 48.77 30.29
Thu 13-Apr 49.38 29.66
Fri 14-Apr 50.14 49.66 50.27 29.88
Sat 15-Apr 49.70 49.63 30.59
Sun 16-Apr 48.49 49.40 48.67 30.13
Mon 17-Apr 49.94 49.37 48.44 48.44 29.45
3 Tue 18-Apr 48.28
Wed 19-Apr 0.00 NA NA 0.00 NA 0.00 NA
Thu 20-Apr 0.00 NA NA 0.00 NA 0.00 NA
Fri 21-Apr 0.00 NA NA 0.00 NA 0.00 NA
Sat 22-Apr 0.00 NA NA 0.00 NA 0.00 NA
Sun 23-Apr 0.00 NA NA 0.00 NA 0.00 NA
Mon 24-Apr 0.00 NA NA 0.00 NA 0.00 NA
4 Tue 25-Apr 0.00 NA NA 0.00 NA 0.00 NA
Wed 26-Apr 0.00 NA NA 0.00 NA 0.00 NA
Thu 27-Apr 0.00 NA NA 0.00 NA 0.00 NA
Fri 28-Apr 0.00 NA NA 0.00 NA 0.00 NA
Sat 29-Apr 0.00 NA NA 0.00 NA 0.00 NA
Sun 30-Apr 0.00 NA NA 0.00 NA 0.00 NA
Mon 1-May 0.00 NA NA 0.00 NA 0.00 NA
5 Tue 2-May 0.00 NA NA 0.00 NA 0.00 NA
Wed 3-May 0.00 NA NA 0.00 NA 0.00 NA
Thu 4-May 0.00 NA NA 0.00 NA 0.00 NA
Fri 5-May 0.00 NA NA 0.00 NA 0.00 NA
Sat 6-May 0.00 NA NA 0.00 NA 0.00 NA
Sun 7-May 0.00 NA NA 0.00 NA 0.00 NA
Mon 8-May 0.00 NA NA 0.00 NA 0.00 NA
6 Tue 9-May 0.00 NA NA 0.00 NA 0.00 NA
Average 22.32 49.69 15.48 48.71 13.18 #DIV/0!
Minimum 0.00 49.37 0.00 48.26 0.00 0.00
Maximum 50.35 50.00 51.59 49.35 31.15 0.00
32% NaOH HYDROCHLORIC ACID
IEM 1 IEM 2 IEM 1
Tk B Online Tank 9 Online Tank 1 Tank 2 Tank 3 Tank 4 Tank 5 Online
NA 31.13 30.98 SD NA NA NA NA NA 33.01
NA 31.72 30.79 SD NA NA NA NA NA 33.07
NA 31.09 NA SD NA NA NA NA NA 33.31
NA 31.13 NA NA NA NA NA NA NA 32.39
NA 30.91 30.90 NA NA NA NA NA NA 33.09
NA 0.00 NA NA NA NA NA NA NA 0.00
NA 31.42 NA NA NA NA NA NA NA 33.42
30.82 30.88 33.15
31.05 31.04 33.20
30.86 31.30 34.05
31.15 32.68 33.20 33.57
30.56 33.50 32.87 33.50
33.03 32.82
31.22 32.59
30.37 32.34 32.51 32.59
30.52 30.41 32.16 33.19
31.27 33.56
31.01 33.87
30.76 33.73
30.64 32.07
30.76 30.68 32.86
NA 0.00 NA NA NA NA NA NA NA 0.00
NA 0.00 NA NA NA NA NA NA NA 0.00
NA 0.00 NA NA NA NA NA NA NA 0.00
NA 0.00 NA NA NA NA NA NA NA 0.00
NA 0.00 NA NA NA NA NA NA NA 0.00
NA 0.00 NA NA NA NA NA NA NA 0.00
NA 0.00 NA NA NA NA NA NA NA 0.00
NA 0.00 NA NA NA NA NA NA NA 0.00
NA 0.00 NA NA NA NA NA NA NA 0.00
NA 0.00 NA NA NA NA NA NA NA 0.00
NA 0.00 NA NA NA NA NA NA NA 0.00
NA 0.00 NA NA NA NA NA NA NA 0.00
NA 0.00 NA NA NA NA NA NA NA 0.00
NA 0.00 NA NA NA NA NA NA NA 0.00
NA 0.00 NA NA NA NA NA NA NA 0.00
NA 0.00 NA NA NA NA NA NA NA 0.00
NA 0.00 NA NA NA NA NA NA NA 0.00
NA 0.00 NA NA NA NA NA NA NA 0.00
NA 0.00 NA NA NA NA NA NA NA 0.00
NA 0.00 NA NA NA NA NA NA NA 0.00
NA 0.00 NA NA NA NA NA NA NA 0.00
#DIV/0! 13.93 30.91 32.83 32.71 14.94
0.00 0.00 30.41 32.34 32.16 0.00
0.00 31.72 31.30 33.50 33.20 34.05
HLORIC ACID
IEM 2 NaOCl
CTA 1 CTA 2 CTA 3 CTB 1 CTB 2 Tk 1 Tk 2 Tk 3 Tk 4 Tk 5
NA NA NA 32.54 NA NA NA NA 7.77 NA
NA NA NA NA 32.96 NA NA NA NA 7.78
NA 33.25 NA NA 33.10 NA NA NA 7.57 NA
NA NA NA 33.27 NA NA NA NA NA 7.97
NA 33.16 NA NA NA NA NA NA 7.89 NA
NA NA NA NA NA NA NA NA NA NA
NA 32.54 NA 33.33 NA NA NA NA 7.48 NA
33.37 7.55
33.33 7.54
33.30 33.44
32.88 7.80 7.61
33.41 8.70
33.18 7.80 7.72
7.68
33.39 7.61
33.38 7.80

33.45 33.13 7.56 7.77


33.45 7.45
33.19 32.67 7.96
33.16 7.68
NA NA NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA NA NA
33.17 7.75
32.54 7.45
33.45 8.70
SODIUM HYPOCHLORITE
Excess NaOH SG
Tk 1 Tk 2 Tk 3 Tk 4 Tk 5 Tk 1 Tk 2 Tk 3 Tk 4 Tk 5
0.00 0.00 0.00 0.82 0.00 0.00 0.00 0.00 1.13 0.00
0.00 0.00 0.00 0.00 0.57 0.00 0.00 0.00 0.00 1.14
0.00 0.00 0.00 0.65 0.00 0.00 0.00 0.00 1.13 0.00
0.00 0.00 0.00 0.00 0.53 0.00 0.00 0.00 0.00 1.14
0.00 0.00 0.00 0.72 0.00 0.00 0.00 0.00 1.13 0.00
0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00
0.00 0.00 0.00 0.72 0.00 0.00 0.00 0.00 1.13 0.00
0.70 1.13
0.75 1.13

0.81 0.82 1.13 1.15


0.91 1.13
0.75 0.73 1.14 1.13
0.68 1.13
0.70 1.13
0.64 1.14

0.60 0.53 1.13 1.14


0.72 1.13
0.74 1.14
0.79 1.14
0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00
0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00
0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00
0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00
0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00
0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00
0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00
0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00
0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00
0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00
0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00
0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00
0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00
0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00
0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00
0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00
0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00
0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00
0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00
0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00
0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00
0.10 0.15
0.00 0.00
0.91 1.15
Polished brine
LIQUID CHLORINE Ca+Mg Ca + Mg in SPB Na2SO4 in SPB
Tank Feed % H2 IEM 1 IEM 2 IEM 1 IEM 2 IEM 1 IEM 2
NA NA NA 0.00 0.00 14 8 NA NA
NA NA NA 3.56 5.34 34 4 2.96 4.74
NA NA NA 0.00 0.00 14 20 NA NA
NA NA NA 0.00 0.00 68 nil NA NA
NA NA NA 0.00 0.00 0 0 0.00 0.00
NA NA NA 0.00 0.00 nil nil NA NA
NA NA NA 0.00 0.00 12 12 NA NA
25 4
18 0 2.81 5.48
25 0
5 0

34 2.22
4.00 2 2.22 0.00
12 10
2.67 1.78 30 2 2.22 4.14

36 2

2.67 7.12 12 0 2.52 4.14


4
NA NA NA 0.00 0.00 nil nil NA NA
NA NA NA 0.00 0.00 nil nil NA NA
NA NA NA 0.00 0.00 nil nil NA NA
NA NA NA 0.00 0.00 nil nil NA NA
NA NA NA 0.00 0.00 nil nil NA NA
NA NA NA 0.00 0.00 nil nil NA NA
NA NA NA 0.00 0.00 nil nil NA NA
NA NA NA 0.00 0.00 nil nil NA NA
NA NA NA 0.00 0.00 nil nil NA NA
NA NA NA 0.00 0.00 nil nil NA NA
NA NA NA 0.00 0.00 nil nil NA NA
NA NA 0.00 0.00 0.00 nil nil NA NA
NA NA NA 0.00 0.00 nil nil NA NA
NA NA NA 0.00 0.00 nil nil NA NA
NA NA NA 0.00 0.00 nil nil NA NA
NA NA NA 0.00 0.00 nil nil NA NA
NA NA NA 0.00 0.00 nil nil NA NA
NA NA NA 0.00 0.00 nil nil NA NA
NA NA NA 0.00 0.00 nil nil NA NA
NA NA NA 0.00 0.00 nil nil NA NA
NA NA NA 0.00 0.00 nil nil NA NA
#DIV/0! #DIV/0! 0.00 0.42 0.47 21.31 4.71 2.14 3.08
0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00
0.00 0.00 0.00 4.00 7.12 68.00 20.00 2.96 5.48
CHLORATE Depleted brine
SPB Depleted brine NaCl Free Cl2 pH
IEM 1 IEM 2 IEM 1 IEM 2 IEM 1 IEM 2 IEM 1 IEM 2 IEM 2
NA NA NA NA 196 226 negative negative NA
5.96 25.76 11.57 37.51 197 227 negative negative 1.83
NA NA NA NA 202 225 negative negative NA
NA NA NA NA 204 222 positive negative NA
0.00 0.00 0.00 0.00 NA NA 0 0 0.00
NA NA NA NA 0 0 negative negative NA
NA NA NA NA 228 240 negative negative NA
209 226 negative negative
209 226 negative negative
25.41 34.97 226 negative 2.89
207 222 negative negative

198 positive
3.51 8.06 181 positive
183 184 negative negative
4.82 18.84 8.33 29.36 183 215 negative negative

188 244 negative negative

4.38 18.49 9.46 28.39 182 211 negative negative 2.11


212 negative
NA NA NA NA 0 0 negative negative NA
NA NA NA NA 0 0 negative negative NA
NA NA NA NA 0 0 negative negative NA
NA NA NA NA 0 0 negative negative NA
NA NA NA NA 0 0 negative negative NA
NA NA NA NA 0 0 negative negative NA
NA NA NA NA 0 0 negative negative NA
NA NA NA NA 0 0 negative negative NA
NA NA NA NA 0 0 negative negative NA
NA NA NA NA 0 0 negative negative NA
NA NA NA NA 0 0 negative negative NA
NA NA NA NA 0 0 negative negative NA
NA NA NA NA 0 0 negative negative NA
NA NA NA NA 0 0 negative negative NA
NA NA NA NA 0 0 negative negative NA
NA NA NA NA 0 0 negative negative NA
NA NA NA NA 0 0 negative negative NA
NA NA NA NA 0 0 negative negative NA
NA NA NA NA 0 0 negative negative NA
NA NA NA NA 0 0 negative negative NA
NA NA NA NA 0 0 negative negative NA
3.73 17.70 7.48 26.05 76.86 86.28 negative negative 1.71
positive positive
0.00 0.00 0.00 0.00 0.00 0.00 3 0 0.00
negative negative
5.96 25.76 11.57 37.51 228.00 244.00 33 36 2.89
positive negative
GAS ANALYSIS - IEM 1
Instrument Line A Line B
H2SO4 Air SiO2 Cl2 H2 O2+CO2 Cl2 H2 O2+CO2
NA 0.0 NA NA 0 0 0 0 0
NA UNDER REPAIR 130 NA 0 0 0 0 0
NA UNDER REPAIR NA NA 0 0 0 0 0
NA for repair NA NA 0 0 0 0 0
NA NA NA NA 0 0 0 0 0
NA 0.0 NA NA 0 0 0 0 0
NA for repair NA NA 0 0 0 0 0
for repair
for repair
for repair
5.7

8.6
7.6
5.6
8.6

7.1

97.22 6.5
6.5
NA 0.0 NA NA 0 0 0 0 0
NA 0.0 NA NA 0 0 0 0 0
NA 0.0 NA NA 0 0 0 0 0
NA 0.0 NA NA 0 0 0 0 0
NA 0.0 NA NA 0 0 0 0 0
NA 0.0 NA NA 0 0 0 0 0
NA 0.0 NA NA 0 0 0 0 0
NA 0.0 NA NA 0 0 0 0 0
NA 0.0 NA NA 0 0 0 0 0
NA 0.0 NA NA 0 0 0 0 0
NA 0.0 NA NA 0 0 0 0 0
NA 0.0 NA NA 0 0 0 0 0
NA 0.0 NA NA 0 0 0 0 0
NA 0.0 NA NA 0 0 0 0 0
NA 0.0 NA NA 0 0 0 0 0
NA 0.0 NA NA 0 0 0 0 0
NA 0.0 NA NA 0 0 0 0 0
NA 0.0 NA NA 0 0 0 0 0
NA 0.0 NA NA 0 0 0 0 0
NA 0.0 NA NA 0 0 0 0 0
NA 0.0 NA NA 0 0 0 0 0
97.22 1.81 130.00 #DIV/0! 0.00 0.00 0.00 0.00 0.00
positive
97.22 0.00 130.00 0.00 0.00 0.00 0.00 0.00 0.00
negative
97.22 8.60 130.00 0.00 0.00 0.00 0.00 0.00 0.00
GAS ANALYSIS - IEM 2
Line A Line B GAS ANALYSIS - FLUE GAS pH
Cl2 H2 O2+CO2 Cl2 H2 O2+CO2 CO CO2 O2 6:00 AM
NA 0 0 0 0 0 NA 0 0 8.66
NA 0 0 0 0 0 NA 0 0 8.63
NA 0 0 0 0 0 NA 0 0 8.58
NA 0 0 0 0 0 NA 0 0 8.56
NA 0 0 0 0 0 NA 0 0 NA
NA 0 0 0 0 0 NA 0 0 0.00
NA 0 0 0 0 0 NA 0 0 8.55
8.54
8.55
8.68
8.68

8.68
8.88
8.85
8.70

8.58

8.78
8.60
NA 0 0 0 0 0 NA 0 0 0.00
NA 0 0 0 0 0 NA 0 0 0.00
NA 0 0 0 0 0 NA 0 0 0.00
NA 0 0 0 0 0 NA 0 0 0.00
NA 0 0 0 0 0 NA 0 0 0.00
NA 0 0 0 0 0 NA 0 0 0.00
NA 0 0 0 0 0 NA 0 0 0.00
NA 0 0 0 0 0 NA 0 0 0.00
NA 0 0 0 0 0 NA 0 0 0.00
NA 0 0 0 0 0 NA 0 0 0.00
NA 0 0 0 0 0 NA 0 0 0.00
NA 0 0 0 0 0 NA 0 0 0.00
NA 0 0 0 0 0 NA 0 0 0.00
NA 0 0 0 0 0 NA 0 0 0.00
NA 0 0 0 0 0 NA 0 0 0.00
NA 0 0 0 0 0 NA 0 0 0.00
NA 0 0 0 0 0 NA 0 0 0.00
NA 0 0 0 0 0 NA 0 0 0.00
NA 0 0 0 0 0 NA 0 0 0.00
NA 0 0 0 0 0 NA 0 0 0.00
NA 0 0 0 0 0 NA 0 0 0.00
#DIV/0! 0.00 0.00 0.00 0.00 0.00 #DIV/0! 0.00 0.00 3.64
0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00
0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 8.88
S-2 S-5
pH
7:00 PM Hg, ppb TDS TSS Color COD pH Hg, ppb TDS TSS
8.58 NA NA NA NA NA 8.66 NA NA NA
8.54 0.056 204 4 40 NA 8.61 0.168 263 2
8.52 NA NA NA NA NA 8.67 NA NA NA
8.66 NA NA NA NA NA 9.20 NA NA NA
0.00 NA NA NA NA NA NA NA NA NA
0.00 NA NA NA NA NA NA NA NA NA
9.23 NA NA NA NA NA 8.68 NA NA NA
8.52 8.83
8.44 8.63
8.61 8.62
8.48 0.056 256 6 43 8.62 0.335 368 3

8.64 8.62
8.62 8.53
8.79 0.112 3800 5 35 8.70 0.224 251 2
8.65 8.63

8.63 8.67

8.71 8.65
8.57 8.62
0.00 NA NA NA NA NA NA NA NA NA
0.00 NA NA NA NA NA NA NA NA NA
0.00 NA NA NA NA NA NA NA NA NA
0.00 NA NA NA NA NA NA NA NA NA
0.00 NA NA NA NA NA NA NA NA NA
0.00 NA NA NA NA NA NA NA NA NA
0.00 NA NA NA NA NA NA NA NA NA
0.00 NA NA NA NA NA NA NA NA NA
0.00 NA NA NA NA NA NA NA NA NA
0.00 NA NA NA NA NA NA NA NA NA
0.00 NA NA NA NA NA NA NA NA NA
0.00 NA NA NA NA NA NA NA NA NA
0.00 NA NA NA NA NA NA NA NA NA
0.00 NA NA NA NA NA NA NA NA NA
0.00 NA NA NA NA NA NA NA NA NA
0.00 NA NA NA NA NA NA NA NA NA
0.00 NA NA NA NA NA NA NA NA NA
0.00 NA NA NA NA NA NA NA NA NA
0.00 NA NA NA NA NA NA NA NA NA
0.00 NA NA NA NA NA NA NA NA NA
0.00 NA NA NA NA NA NA NA NA NA
3.54 0.07 1420.00 5.00 39.33 #DIV/0! 8.68 0.24 294.00 2.33
0.00 0.06 204.00 4.00 35.00 0.00 8.53 0.17 251.00 2.00
9.23 0.11 3800.00 6.00 43.00 0.00 9.20 0.34 368.00 3.00
S-5 S-8(Sludge Pond Outlet 1) S-9(Sludge Po

Color COD pH Hg, ppb TDS TSS Color COD pH Hg, ppb
NA NA 6.52 NA NA 38 152 nil 8.21 NA
17 NA 6.87 NA NA 22 98 NA 8.25 NA
NA NA 7.07 NA NA 16 96 NA 8.28 NA
NA NA 7.33 NA NA 7 75 NA 8.25 NA
NA NA NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA NA NA
NA NA 7.97 NA NA 9 43 NA 8.43 NA
7.40 16 104 8.62
7.83 17 89 8.33
7.78 11 73 8.36
24 7.63 9 110 8.42

7.67 12 116 8.32


7.27 7 14 25 8.28
17 7.23 7 8 8.68

7.50 2 14 8.77

7.49 12 16 15 8.44
7.57 5 15 8.26
NA NA NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA NA NA
19.33 #DIV/0! 7.41 #DIV/0! #DIV/0! 12.67 68.20 20.00 8.39 #DIV/0!
17.00 0.00 6.52 0.00 0.00 2.00 8.00 15.00 8.21 0.00
24.00 0.00 7.97 0.00 0.00 38.00 152.00 25.00 8.77 0.00
S-9(Sludge Pond Outlet 2) LAGOON

TDS TSS Color COD pH Hg, ppb TDS TSS Color COD
NA 1 16 nil NA NA NA NA NA NA
NA 1 8 NA NA NA NA NA NA NA
NA 2 8 NA NA NA NA NA NA NA
NA 2 0 NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA NA NA
NA 2 7 NA NA NA NA NA NA NA
1 11
3 25
3 11
11 15 8.26 0.056 159 4 28

4 12
2 2 10
3 4 8.28 0.056 280 5 30

4 12

5 6 4
3 15
NA NA NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA NA NA
#DIV/0! 3.13 10.13 7.00 8.27 0.06 219.50 4.50 29.00 #DIV/0!
0.00 1.00 0.00 4.00 8.26 0.06 159.00 4.00 28.00 0.00
0.00 11.00 25.00 10.00 8.28 0.06 280.00 5.00 30.00 0.00
JBC Evap Canal Total Canal

pH gpl NaOH pH gpl NaOH pH gpl NaOH S-3 S-4 S-7


NA 0.00 0.00 0.00 0.00 0.00 NA 0.00 0.00
8.23 ND 8.31 ND 8.07 ND 7.63 8.85 7.84
NA 0.00 0.00 0.00 0.00 0.00 NA 0.00 0.00
NA 0.00 0.00 0.00 0.00 0.00 NA 0.00 0.00
NA 0.00 0.00 0.00 0.00 0.00 NA 0.00 0.00
NA 0.00 0.00 0.00 0.00 0.00 NA 0.00 0.00
NA 0.00 0.00 0.00 0.00 0.00 NA 0.00 0.00

8.17 ND 8.34 ND 8.03 ND 8.25 8.82 8.48

7.78 0.00 2.12 0.00 6.12 0.00 7.95 .8.78 9.68

NA 0.00 0.00 0.00 0.00 0.00 NA 0.00 0.00


NA 0.00 0.00 0.00 0.00 0.00 NA 0.00 0.00
NA 0.00 0.00 0.00 0.00 0.00 NA 0.00 0.00
NA 0.00 0.00 0.00 0.00 0.00 NA 0.00 0.00
NA 0.00 0.00 0.00 0.00 0.00 NA 0.00 0.00
NA 0.00 0.00 0.00 0.00 0.00 NA 0.00 0.00
NA 0.00 0.00 0.00 0.00 0.00 NA 0.00 0.00
NA 0.00 0.00 0.00 0.00 0.00 NA 0.00 0.00
NA 0.00 0.00 0.00 0.00 0.00 NA 0.00 0.00
NA 0.00 0.00 0.00 0.00 0.00 NA 0.00 0.00
NA 0.00 0.00 0.00 0.00 0.00 NA 0.00 0.00
NA 0.00 0.00 0.00 0.00 0.00 NA 0.00 0.00
NA 0.00 0.00 0.00 0.00 0.00 NA 0.00 0.00
NA 0.00 0.00 0.00 0.00 0.00 NA 0.00 0.00
NA 0.00 0.00 0.00 0.00 0.00 NA 0.00 0.00
NA 0.00 0.00 0.00 0.00 0.00 NA 0.00 0.00
NA 0.00 0.00 0.00 0.00 0.00 NA 0.00 0.00
NA 0.00 0.00 0.00 0.00 0.00 NA 0.00 0.00
NA 0.00 0.00 0.00 0.00 0.00 NA 0.00 0.00
NA 0.00 0.00 0.00 0.00 0.00 NA 0.00 0.00
NA 0.00 0.00 0.00 0.00 0.00 NA 0.00 0.00
8.06 0.00 0.63 0.00 0.74 0.00 7.94 0.61 0.87
7.78 0.00 0.00 0.00 0.00 0.00 7.63 0.00 0.00
8.23 0.00 8.34 0.00 8.07 0.00 8.25 8.85 9.68
50% NaOH 32% NaOH
IEM 1 IEM 2 IEM 1
WEEK DAY DATE Online Tk A Tk B Online Tank 9 Online Tk A
Wed 29-Mar 49.98 49.92 NA 49.59 NA NA NA
Thu 30-Mar 49.73 NA NA SD NA 31.15 NA
Fri 31-Mar 49.64 50.00 NA 51.59 48.26 30.07 NA
Sat 1-Apr 49.28 49.71 NA 49.09 NA 30.44 NA
Sun 2-Apr 49.81 49.87 NA SD NA 30.17 NA
Mon 3-Apr 0.00 NA NA 0.00 NA 0.00 NA
1 Tue 4-Apr 49.49 NA NA 51.50 48.83 30.45 NA
Average 42.56 49.88 40.35 48.55 25.38 #DIV/0!
Minimum 0.00 49.71 0.00 48.26 0.00 0.00
Maximum 49.98 50.00 51.59 48.83 31.15 0.00
32% NaOH HYDROCHLORIC ACID
IEM 1 IEM 2 IEM 1
Tk B Online Tank 9 Online Tank 1 Tank 2 Tank 3 Tank 4 Tank 5 Online
NA 31.13 30.98 SD NA NA NA NA NA 33.01
NA 31.72 30.79 SD NA NA NA NA NA 33.07
NA 31.09 NA SD NA NA NA NA NA 33.31
NA 31.13 NA NA NA NA NA NA NA 32.39
NA 30.91 30.90 NA NA NA NA NA NA 33.09
NA 0.00 NA NA NA NA NA NA NA 0.00
NA 31.42 NA NA NA NA NA NA NA 33.42
#DIV/0! 26.77 30.89 #DIV/0! #DIV/0! 28.33
0.00 0.00 30.79 0.00 0.00 0.00
0.00 31.72 30.98 0.00 0.00 33.42
HLORIC ACID
IEM 2 NaOCl
CTA 1 CTA 2 CTA 3 CTB 1 CTB 2 Tk 1 Tk 2 Tk 3 Tk 4 Tk 5
NA NA NA 32.54 NA NA NA NA 7.77 NA
NA NA NA NA 32.96 NA NA NA NA 7.78
NA 33.25 NA NA 33.10 NA NA NA 7.57 NA
NA NA NA 33.27 NA NA NA NA NA 7.97
NA 33.16 NA NA NA NA NA NA 7.89 NA
NA NA NA NA NA NA NA NA NA NA
NA 32.54 NA 33.33 NA NA NA NA 7.48 NA
33.02 7.74
32.54 7.48
33.33 7.97
SODIUM HYPOCHLORITE
Excess NaOH SG
Tk 1 Tk 2 Tk 3 Tk 4 Tk 5 Tk 1 Tk 2 Tk 3 Tk 4 Tk 5
0.00 0.00 0.00 0.82 0.00 0.00 0.00 0.00 1.13 0.00
0.00 0.00 0.00 0.00 0.57 0.00 0.00 0.00 0.00 1.14
0.00 0.00 0.00 0.65 0.00 0.00 0.00 0.00 1.13 0.00
0.00 0.00 0.00 0.00 0.53 0.00 0.00 0.00 0.00 1.14
0.00 0.00 0.00 0.72 0.00 0.00 0.00 0.00 1.13 0.00
0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00
0.00 0.00 0.00 0.72 0.00 0.00 0.00 0.00 1.13 0.00
0.11 0.19
0.00 0.00
0.82 1.14
Polished brine
LIQUID CHLORINE Ca+Mg Ca + Mg in SPB Na2SO4 in SPB
Tank Feed % H2 IEM 1 IEM 2 IEM 1 IEM 2 IEM 1 IEM 2
NA NA NA 0.00 0.00 14 8 NA NA
NA NA NA 3.56 5.34 34 4 2.96 4.74
NA NA NA 0.00 0.00 14 20 NA NA
NA NA NA 0.00 0.00 68 nil NA NA
NA NA NA 0.00 0.00 0 0 0.00 0.00
NA NA NA 0.00 0.00 nil nil NA NA
NA NA NA 0.00 0.00 12 12 NA NA
#DIV/0! #DIV/0! #DIV/0! 0.51 0.76 23.67 8.80 1.48 2.37
0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00
0.00 0.00 0.00 3.56 5.34 68.00 20.00 2.96 4.74
CHLORATE Depleted brine
SPB Depleted brine NaCl Free Cl2 pH
IEM 1 IEM 2 IEM 1 IEM 2 IEM 1 IEM 2 IEM 1 IEM 2 IEM 2
NA NA NA NA 196 226 negative negative NA
5.96 25.76 11.57 37.51 197 227 negative negative 1.83
NA NA NA NA 202 225 negative negative NA
NA NA NA NA 204 222 positive negative NA
0.00 0.00 0.00 0.00 NA NA 0 0 0.00
NA NA NA NA 0 0 negative negative NA
NA NA NA NA 228 240 negative negative NA
2.98 12.88 5.79 18.76 171.17 190.00 negative negative 0.92
positive positive
0.00 0.00 0.00 0.00 0.00 0.00 1 0 0.00
negative negative
5.96 25.76 11.57 37.51 228.00 240.00 5 6 1.83

positive negative
GAS ANALYSIS - IEM 1
Instrument Line A Line B
H2SO4 Air SiO2 Cl2 H2 O2+CO2 Cl2 H2 O2+CO2
NA 0.0 NA NA 0 0 0 0 0
NA UNDER REPAIR 130 NA 0 0 0 0 0
NA UNDER REPAIR NA NA 0 0 0 0 0
NA for repair NA NA 0 0 0 0 0
NA NA NA NA 0 0 0 0 0
NA 0.0 NA NA 0 0 0 0 0
NA for repair NA NA 0 0 0 0 0
#DIV/0! 0.00 130.00 #DIV/0! 0.00 0.00 0.00 0.00 0.00
positive
0.00 0.00 130.00 0.00 0.00 0.00 0.00 0.00 0.00
negative
0.00 0.00 130.00 0.00 0.00 0.00 0.00 0.00 0.00
GAS ANALYSIS - IEM 2
Line A Line B GAS ANALYSIS - FLUE GAS pH
Cl2 H2 O2+CO2 Cl2 H2 O2+CO2 CO CO2 O2 6:00 AM
NA 0 0 0 0 0 NA 0 0 8.66
NA 0 0 0 0 0 NA 0 0 8.63
NA 0 0 0 0 0 NA 0 0 8.58
NA 0 0 0 0 0 NA 0 0 8.56
NA 0 0 0 0 0 NA 0 0 NA
NA 0 0 0 0 0 NA 0 0 0.00
NA 0 0 0 0 0 NA 0 0 8.55
#DIV/0! 0.00 0.00 0.00 0.00 0.00 #DIV/0! 0.00 0.00 7.16
0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00
0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 8.66
S-2 S-5
pH
7:00 PM Hg, ppb TDS TSS Color COD pH Hg, ppb TDS TSS
8.58 NA NA NA NA NA 8.66 NA NA NA
8.54 0.056 204 4 40 NA 8.61 0.168 263 2
8.52 NA NA NA NA NA 8.67 NA NA NA
8.66 NA NA NA NA NA 9.20 NA NA NA
0.00 NA NA NA NA NA NA NA NA NA
0.00 NA NA NA NA NA NA NA NA NA
9.23 NA NA NA NA NA 8.68 NA NA NA
6.22 0.06 204.00 4.00 40.00 #DIV/0! 8.76 0.17 263.00 2.00
0.00 0.06 204.00 4.00 40.00 0.00 8.61 0.17 263.00 2.00
9.23 0.06 204.00 4.00 40.00 0.00 9.20 0.17 263.00 2.00
S-5 S-8(Sludge Pond Outlet 1) S-9(Sludge Po

Color COD pH Hg, ppb TDS TSS Color COD pH Hg, ppb
NA NA 6.52 NA NA 38 152 nil 8.21 NA
17 NA 6.87 NA NA 22 98 NA 8.25 NA
NA NA 7.07 NA NA 16 96 NA 8.28 NA
NA NA 7.33 NA NA 7 75 NA 8.25 NA
NA NA NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA NA NA
NA NA 7.97 NA NA 9 43 NA 8.43 NA
17.00 #DIV/0! 7.15 #DIV/0! #DIV/0! 18.40 92.80 #DIV/0! 8.28 #DIV/0!
17.00 0.00 6.52 0.00 0.00 7.00 43.00 0.00 8.21 0.00
17.00 0.00 7.97 0.00 0.00 38.00 152.00 0.00 8.43 0.00
S-9(Sludge Pond Outlet 2) LAGOON

TDS TSS Color COD pH Hg, ppb TDS TSS Color COD
NA 1 16 nil NA NA NA NA NA NA
NA 1 8 NA NA NA NA NA NA NA
NA 2 8 NA NA NA NA NA NA NA
NA 2 0 NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA NA NA
NA 2 7 NA NA NA NA NA NA NA
#DIV/0! 1.60 7.80 #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0!
0.00 1.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00
0.00 2.00 16.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00
JBC Evap Canal Total Canal

pH gpl NaOH pH gpl NaOH pH gpl NaOH S-3 S-4 S-7


NA 0.00 0.00 0.00 0.00 0.00 NA 0.00 0.00
8.23 ND 8.31 ND 8.07 ND 7.63 8.85 7.84
NA 0.00 0.00 0.00 0.00 0.00 NA 0.00 0.00
NA 0.00 0.00 0.00 0.00 0.00 NA 0.00 0.00
NA 0.00 0.00 0.00 0.00 0.00 NA 0.00 0.00
NA 0.00 0.00 0.00 0.00 0.00 NA 0.00 0.00
NA 0.00 0.00 0.00 0.00 0.00 NA 0.00 0.00
8.23 0.00 1.19 0.00 1.15 0.00 7.63 1.26 1.12
8.23 0.00 0.00 0.00 0.00 0.00 7.63 0.00 0.00
8.23 0.00 8.31 0.00 8.07 0.00 7.63 8.85 7.84
50% NaOH 32% NaOH
IEM 1 IEM 2 IEM 1
WEEK DAY DATE Online Tk A Tk B Online Tank 9 Online Tk A
Wed 5-Apr 48.96 49.76 30.77
Thu 6-Apr 49.27 50.04 29.66
Fri 7-Apr 49.70
Sat 8-Apr 49.87 49.56 49.83 30.76
Sun 9-Apr 49.70 46.88 30.78
Mon 10-Apr 50.35 49.35 30.08
2 Tue 11-Apr 50.14 49.67 29.53
Average 49.72 49.67 48.92 49.35 30.26 #DIV/0!
Minimum 48.96 49.56 46.88 49.35 29.53 0.00
Maximum 50.35 49.76 50.04 49.35 30.78 0.00
32% NaOH HYDROCHLORIC ACID
IEM 1 IEM 2 IEM 1
Tk B Online Tank 9 Online Tank 1 Tank 2 Tank 3 Tank 4 Tank 5 Online
30.82 30.88 33.15
31.05 31.04 33.20
30.86 31.30 34.05
31.15 32.68 33.20 33.57
30.56 33.50 32.87 33.50
33.03 32.82
31.22 32.59
#DIV/0! 30.89 31.11 32.95 32.96 33.49
0.00 30.56 30.88 32.59 32.82 33.15
0.00 31.15 31.30 33.50 33.20 34.05
HLORIC ACID
IEM 2 NaOCl
CTA 1 CTA 2 CTA 3 CTB 1 CTB 2 Tk 1 Tk 2 Tk 3 Tk 4 Tk 5
33.37 7.55
33.33 7.54
33.30 33.44
32.88 7.80 7.61
33.41 8.70
33.18 7.80 7.72
7.68
33.27 7.80
32.88 7.54
33.44 8.70
SODIUM HYPOCHLORITE
Excess NaOH SG
Tk 1 Tk 2 Tk 3 Tk 4 Tk 5 Tk 1 Tk 2 Tk 3 Tk 4 Tk 5
0.70 1.13
0.75 1.13

0.81 0.82 1.13 1.15


0.91 1.13
0.75 0.73 1.14 1.13
0.68 1.13
0.77 1.14
0.68 1.13
0.91 1.15
Polished brine
LIQUID CHLORINE Ca+Mg Ca + Mg in SPB Na2SO4 in SPB
Tank Feed % H2 IEM 1 IEM 2 IEM 1 IEM 2 IEM 1 IEM 2
25 4
18 0 2.81 5.48
25 0
5 0

34 2.22
4.00 2 2.22 0.00
#DIV/0! #DIV/0! #DIV/0! 4.00 #DIV/0! 18.17 1.00 2.42 2.74
0.00 0.00 0.00 4.00 0.00 2.00 0.00 2.22 0.00
0.00 0.00 0.00 4.00 0.00 34.00 4.00 2.81 5.48
CHLORATE Depleted brine
SPB Depleted brine NaCl Free Cl2 pH
IEM 1 IEM 2 IEM 1 IEM 2 IEM 1 IEM 2 IEM 1 IEM 2 IEM 2
209 226 negative negative
209 226 negative negative
25.41 34.97 226 negative 2.89
207 222 negative negative

198 positive
3.51 8.06 181 positive
3.51 25.41 8.06 34.97 200.80 225.00 negative negative 2.89
positive positive
3.51 25.41 8.06 34.97 181.00 222.00 2 0 2.89
negative negative
3.51 25.41 8.06 34.97 209.00 226.00 3 4 2.89

positive negative
GAS ANALYSIS - IEM 1
Instrument Line A Line B
H2SO4 Air SiO2 Cl2 H2 O2+CO2 Cl2 H2 O2+CO2
for repair
for repair
for repair
5.7

8.6
7.6
#DIV/0! 7.30 #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0!
positive
0.00 5.70 0.00 0.00 0.00 0.00 0.00 0.00 0.00
negative
0.00 8.60 0.00 0.00 0.00 0.00 0.00 0.00 0.00
GAS ANALYSIS - IEM 2
Line A Line B GAS ANALYSIS - FLUE GAS pH
Cl2 H2 O2+CO2 Cl2 H2 O2+CO2 CO CO2 O2 6:00 AM
8.54
8.55
8.68
8.68

8.68
8.88
#DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! 8.67
0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 8.54
0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 8.88
S-2 S-5
pH
7:00 PM Hg, ppb TDS TSS Color COD pH Hg, ppb TDS TSS
8.52 8.83
8.44 8.63
8.61 8.62
8.48 0.056 256 6 43 8.62 0.335 368 3

8.64 8.62
8.62 8.53
8.55 0.06 256.00 6.00 43.00 #DIV/0! 8.64 0.34 368.00 3.00
8.44 0.06 256.00 6.00 43.00 0.00 8.53 0.34 368.00 3.00
8.64 0.06 256.00 6.00 43.00 0.00 8.83 0.34 368.00 3.00
S-5 S-8(Sludge Pond Outlet 1) S-9(Sludge Po

Color COD pH Hg, ppb TDS TSS Color COD pH Hg, ppb
7.40 16 104 8.62
7.83 17 89 8.33
7.78 11 73 8.36
24 7.63 9 110 8.42

7.67 12 116 8.32


7.27 7 14 25 8.28
24.00 #DIV/0! 7.60 #DIV/0! #DIV/0! 12.00 84.33 25.00 8.39 #DIV/0!
24.00 0.00 7.27 0.00 0.00 7.00 14.00 25.00 8.28 0.00
24.00 0.00 7.83 0.00 0.00 17.00 116.00 25.00 8.62 0.00
S-9(Sludge Pond Outlet 2) LAGOON

TDS TSS Color COD pH Hg, ppb TDS TSS Color COD
1 11
3 25
3 11
11 15 8.26 0.056 159 4 28

4 12
2 2 10
#DIV/0! 4.00 12.67 10.00 8.26 0.06 159.00 4.00 28.00 #DIV/0!
0.00 1.00 2.00 10.00 8.26 0.06 159.00 4.00 28.00 0.00
0.00 11.00 25.00 10.00 8.26 0.06 159.00 4.00 28.00 0.00
JBC Evap Canal Total Canal

pH gpl NaOH pH gpl NaOH pH gpl NaOH S-3 S-4 S-7

8.17 ND 8.34 ND 8.03 ND 8.25 8.82 8.48

8.17 #DIV/0! 8.34 #DIV/0! 8.03 #DIV/0! 8.25 8.82 8.48


8.17 0.00 8.34 0.00 8.03 0.00 8.25 8.82 8.48
8.17 0.00 8.34 0.00 8.03 0.00 8.25 8.82 8.48
50% NaOH 32% NaOH
IEM 1 IEM 2 IEM 1
WEEK DAY DATE Online Tk A Tk B Online Tank 9 Online Tk A
Wed 12-Apr 48.77 30.29
Thu 13-Apr 49.38 29.66
Fri 14-Apr 50.14 49.66 50.27 29.88
Sat 15-Apr 49.70 49.63 30.59
Sun 16-Apr 48.49 49.40 48.67 30.13
Mon 17-Apr 49.94 49.37 48.44 48.44 29.45
3 Tue 18-Apr 48.28
Average 49.40 49.52 49.00 48.56 30.00 #DIV/0!
Minimum 48.49 49.37 48.28 48.44 29.45 0.00
Maximum 50.14 49.66 50.27 48.67 30.59 0.00
32% NaOH HYDROCHLORIC ACID
IEM 1 IEM 2 IEM 1
Tk B Online Tank 9 Online Tank 1 Tank 2 Tank 3 Tank 4 Tank 5 Online
30.37 32.34 32.51 32.59
30.52 30.41 32.16 33.19
31.27 33.56
31.01 33.87
30.76 33.73
30.64 32.07
30.76 30.68 32.86
#DIV/0! 30.76 30.55 32.34 32.34 33.12
0.00 30.37 30.41 32.34 32.16 32.07
0.00 31.27 30.68 32.34 32.51 33.87
HLORIC ACID
IEM 2 NaOCl
CTA 1 CTA 2 CTA 3 CTB 1 CTB 2 Tk 1 Tk 2 Tk 3 Tk 4 Tk 5
33.39 7.61
33.38 7.80

33.45 33.13 7.56 7.77


33.45 7.45
33.19 32.67 7.96
33.16 7.68
33.23 7.69
32.67 7.45
33.45 7.96
SODIUM HYPOCHLORITE
Excess NaOH SG
Tk 1 Tk 2 Tk 3 Tk 4 Tk 5 Tk 1 Tk 2 Tk 3 Tk 4 Tk 5
0.70 1.13
0.64 1.14

0.60 0.53 1.13 1.14


0.72 1.13
0.74 1.14
0.79 1.14
0.67 1.14
0.53 1.13
0.79 1.14
Polished brine
LIQUID CHLORINE Ca+Mg Ca + Mg in SPB Na2SO4 in SPB
Tank Feed % H2 IEM 1 IEM 2 IEM 1 IEM 2 IEM 1 IEM 2
12 10
2.67 1.78 30 2 2.22 4.14

36 2

2.67 7.12 12 0 2.52 4.14


4
#DIV/0! #DIV/0! #DIV/0! 2.67 4.45 22.50 3.60 2.37 4.14
0.00 0.00 0.00 2.67 1.78 12.00 0.00 2.22 4.14
0.00 0.00 0.00 2.67 7.12 36.00 10.00 2.52 4.14
CHLORATE Depleted brine
SPB Depleted brine NaCl Free Cl2 pH
IEM 1 IEM 2 IEM 1 IEM 2 IEM 1 IEM 2 IEM 1 IEM 2 IEM 2
183 184 negative negative
4.82 18.84 8.33 29.36 183 215 negative negative

188 244 negative negative

4.38 18.49 9.46 28.39 182 211 negative negative 2.11


212 negative
4.60 18.67 8.90 28.88 184.00 213.20 negative negative 2.11
positive positive
4.38 18.49 8.33 28.39 182.00 184.00 0 0 2.11
negative negative
4.82 18.84 9.46 29.36 188.00 244.00 4 5 2.11

positive negative
GAS ANALYSIS - IEM 1
Instrument Line A Line B
H2SO4 Air SiO2 Cl2 H2 O2+CO2 Cl2 H2 O2+CO2
5.6
8.6

7.1

97.22 6.5
6.5
97.22 6.86 #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0!
positive
97.22 5.60 0.00 0.00 0.00 0.00 0.00 0.00 0.00
negative
97.22 8.60 0.00 0.00 0.00 0.00 0.00 0.00 0.00
GAS ANALYSIS - IEM 2
Line A Line B GAS ANALYSIS - FLUE GAS pH
Cl2 H2 O2+CO2 Cl2 H2 O2+CO2 CO CO2 O2 6:00 AM
8.85
8.70

8.58

8.78
8.60
#DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! 8.70
0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 8.58
0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 8.85
S-2 S-5
pH
7:00 PM Hg, ppb TDS TSS Color COD pH Hg, ppb TDS TSS
8.79 0.112 3800 5 35 8.70 0.224 251 2
8.65 8.63

8.63 8.67

8.71 8.65
8.57 8.62
8.67 0.11 3800.00 5.00 35.00 #DIV/0! 8.65 0.22 251.00 2.00
8.57 0.11 3800.00 5.00 35.00 0.00 8.62 0.22 251.00 2.00
8.79 0.11 3800.00 5.00 35.00 0.00 8.70 0.22 251.00 2.00
S-5 S-8(Sludge Pond Outlet 1) S-9(Sludge Po

Color COD pH Hg, ppb TDS TSS Color COD pH Hg, ppb
17 7.23 7 8 8.68

7.50 2 14 8.77

7.49 12 16 15 8.44
7.57 5 15 8.26
17.00 #DIV/0! 7.45 #DIV/0! #DIV/0! 6.50 13.25 15.00 8.54 #DIV/0!
17.00 0.00 7.23 0.00 0.00 2.00 8.00 15.00 8.26 0.00
17.00 0.00 7.57 0.00 0.00 12.00 16.00 15.00 8.77 0.00
S-9(Sludge Pond Outlet 2) LAGOON

TDS TSS Color COD pH Hg, ppb TDS TSS Color COD
3 4 8.28 0.056 280 5 30

4 12

5 6 4
3 15
#DIV/0! 3.75 9.25 4.00 8.28 0.06 280.00 5.00 30.00 #DIV/0!
0.00 3.00 4.00 4.00 8.28 0.06 280.00 5.00 30.00 0.00
0.00 5.00 15.00 4.00 8.28 0.06 280.00 5.00 30.00 0.00
JBC Evap Canal Total Canal

pH gpl NaOH pH gpl NaOH pH gpl NaOH S-3 S-4 S-7


7.78 0.00 2.12 0.00 6.12 0.00 7.95 .8.78 9.68

7.78 0.00 2.12 0.00 6.12 0.00 7.95 #DIV/0! 9.68


7.78 0.00 2.12 0.00 6.12 0.00 7.95 0.00 9.68
7.78 0.00 2.12 0.00 6.12 0.00 7.95 0.00 9.68
50% NaOH 32% NaOH
IEM 1 IEM 2 IEM 1
WEEK DAY DATE Online Tk A Tk B Online Tank 9 Online Tk A
Wed 19-Apr 0.00 NA NA 0.00 NA 0.00 NA
Thu 20-Apr 0.00 NA NA 0.00 NA 0.00 NA
Fri 21-Apr 0.00 NA NA 0.00 NA 0.00 NA
Sat 22-Apr 0.00 NA NA 0.00 NA 0.00 NA
Sun 23-Apr 0.00 NA NA 0.00 NA 0.00 NA
Mon 24-Apr 0.00 NA NA 0.00 NA 0.00 NA
4 Tue 25-Apr 0.00 NA NA 0.00 NA 0.00 NA
Average 0.00 #DIV/0! 0.00 #DIV/0! 0.00 #DIV/0!
Minimum 0.00 0.00 0.00 0.00 0.00 0.00
Maximum 0.00 0.00 0.00 0.00 0.00 0.00
32% NaOH HYDROCHLORIC ACID
IEM 1 IEM 2 IEM 1
Tk B Online Tank 9 Online Tank 1 Tank 2 Tank 3 Tank 4 Tank 5 Online
NA 0.00 NA NA NA NA NA NA NA 0.00
NA 0.00 NA NA NA NA NA NA NA 0.00
NA 0.00 NA NA NA NA NA NA NA 0.00
NA 0.00 NA NA NA NA NA NA NA 0.00
NA 0.00 NA NA NA NA NA NA NA 0.00
NA 0.00 NA NA NA NA NA NA NA 0.00
NA 0.00 NA NA NA NA NA NA NA 0.00
#DIV/0! 0.00 #DIV/0! #DIV/0! #DIV/0! 0.00
0.00 0.00 0.00 0.00 0.00 0.00
0.00 0.00 0.00 0.00 0.00 0.00
HLORIC ACID
IEM 2 NaOCl
CTA 1 CTA 2 CTA 3 CTB 1 CTB 2 Tk 1 Tk 2 Tk 3 Tk 4 Tk 5
NA NA NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA NA NA
#DIV/0! #DIV/0!
0.00 0.00
0.00 0.00
SODIUM HYPOCHLORITE
Excess NaOH SG
Tk 1 Tk 2 Tk 3 Tk 4 Tk 5 Tk 1 Tk 2 Tk 3 Tk 4 Tk 5
0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00
0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00
0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00
0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00
0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00
0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00
0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00
0.00 0.00
0.00 0.00
0.00 0.00
Polished brine
LIQUID CHLORINE Ca+Mg Ca + Mg in SPB Na2SO4 in SPB
Tank Feed % H2 IEM 1 IEM 2 IEM 1 IEM 2 IEM 1 IEM 2
NA NA NA 0.00 0.00 nil nil NA NA
NA NA NA 0.00 0.00 nil nil NA NA
NA NA NA 0.00 0.00 nil nil NA NA
NA NA NA 0.00 0.00 nil nil NA NA
NA NA NA 0.00 0.00 nil nil NA NA
NA NA NA 0.00 0.00 nil nil NA NA
NA NA NA 0.00 0.00 nil nil NA NA
#DIV/0! #DIV/0! #DIV/0! 0.00 0.00 #DIV/0! #DIV/0! #DIV/0! #DIV/0!
0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00
0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00
CHLORATE Depleted brine
SPB Depleted brine NaCl Free Cl2 pH
IEM 1 IEM 2 IEM 1 IEM 2 IEM 1 IEM 2 IEM 1 IEM 2 IEM 2
NA NA NA NA 0 0 negative negative NA
NA NA NA NA 0 0 negative negative NA
NA NA NA NA 0 0 negative negative NA
NA NA NA NA 0 0 negative negative NA
NA NA NA NA 0 0 negative negative NA
NA NA NA NA 0 0 negative negative NA
NA NA NA NA 0 0 negative negative NA
#DIV/0! #DIV/0! #DIV/0! #DIV/0! 0.00 0.00 negative negative #DIV/0!
positive positive
0.00 0.00 0.00 0.00 0.00 0.00 0 0 0.00
negative negative
0.00 0.00 0.00 0.00 0.00 0.00 7 7 0.00

positive negative
GAS ANALYSIS - IEM 1
Instrument Line A Line B
H2SO4 Air SiO2 Cl2 H2 O2+CO2 Cl2 H2 O2+CO2
NA 0.0 NA NA 0 0 0 0 0
NA 0.0 NA NA 0 0 0 0 0
NA 0.0 NA NA 0 0 0 0 0
NA 0.0 NA NA 0 0 0 0 0
NA 0.0 NA NA 0 0 0 0 0
NA 0.0 NA NA 0 0 0 0 0
NA 0.0 NA NA 0 0 0 0 0
#DIV/0! 0.00 #DIV/0! #DIV/0! 0.00 0.00 0.00 0.00 0.00
positive
0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00
negative
0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00
GAS ANALYSIS - IEM 2
Line A Line B GAS ANALYSIS - FLUE GAS pH
Cl2 H2 O2+CO2 Cl2 H2 O2+CO2 CO CO2 O2 6:00 AM
NA 0 0 0 0 0 NA 0 0 0.00
NA 0 0 0 0 0 NA 0 0 0.00
NA 0 0 0 0 0 NA 0 0 0.00
NA 0 0 0 0 0 NA 0 0 0.00
NA 0 0 0 0 0 NA 0 0 0.00
NA 0 0 0 0 0 NA 0 0 0.00
NA 0 0 0 0 0 NA 0 0 0.00
#DIV/0! 0.00 0.00 0.00 0.00 0.00 #DIV/0! 0.00 0.00 0.00
0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00
0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00
S-2 S-5
pH
7:00 PM Hg, ppb TDS TSS Color COD pH Hg, ppb TDS TSS
0.00 NA NA NA NA NA NA NA NA NA
0.00 NA NA NA NA NA NA NA NA NA
0.00 NA NA NA NA NA NA NA NA NA
0.00 NA NA NA NA NA NA NA NA NA
0.00 NA NA NA NA NA NA NA NA NA
0.00 NA NA NA NA NA NA NA NA NA
0.00 NA NA NA NA NA NA NA NA NA
0.00 #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0!
0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00
0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00
S-5 S-8(Sludge Pond Outlet 1) S-9(Sludge Po

Color COD pH Hg, ppb TDS TSS Color COD pH Hg, ppb
NA NA NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA NA NA
#DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0!
0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00
0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00
S-9(Sludge Pond Outlet 2) LAGOON

TDS TSS Color COD pH Hg, ppb TDS TSS Color COD
NA NA NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA NA NA
#DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0!
0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00
0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00
JBC Evap Canal Total Canal

pH gpl NaOH pH gpl NaOH pH gpl NaOH S-3 S-4 S-7


NA 0.00 0.00 0.00 0.00 0.00 NA 0.00 0.00
NA 0.00 0.00 0.00 0.00 0.00 NA 0.00 0.00
NA 0.00 0.00 0.00 0.00 0.00 NA 0.00 0.00
NA 0.00 0.00 0.00 0.00 0.00 NA 0.00 0.00
NA 0.00 0.00 0.00 0.00 0.00 NA 0.00 0.00
NA 0.00 0.00 0.00 0.00 0.00 NA 0.00 0.00
NA 0.00 0.00 0.00 0.00 0.00 NA 0.00 0.00
#DIV/0! 0.00 0.00 0.00 0.00 0.00 #DIV/0! 0.00 0.00
0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00
0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00
50% NaOH 32% NaOH
IEM 1 IEM 2 IEM 1
WEEK DAY DATE Online Tk A Tk B Online Tank 9 Online Tk A
Wed 26-Apr 0.00 NA NA 0.00 NA 0.00 NA
Thu 27-Apr 0.00 NA NA 0.00 NA 0.00 NA
Fri 28-Apr 0.00 NA NA 0.00 NA 0.00 NA
Sat 29-Apr 0.00 NA NA 0.00 NA 0.00 NA
Sun 30-Apr 0.00 NA NA 0.00 NA 0.00 NA
Mon 1-May 0.00 NA NA 0.00 NA 0.00 NA
5 Tue 2-May 0.00 NA NA 0.00 NA 0.00 NA
Average 0.00 #DIV/0! 0.00 #DIV/0! 0.00 #DIV/0!
Minimum 0.00 0.00 0.00 0.00 0.00 0.00
Maximum 0.00 0.00 0.00 0.00 0.00 0.00
32% NaOH HYDROCHLORIC ACID
IEM 1 IEM 2 IEM 1
Tk B Online Tank 9 Online Tank 1 Tank 2 Tank 3 Tank 4 Tank 5 Online
NA 0.00 NA NA NA NA NA NA NA 0.00
NA 0.00 NA NA NA NA NA NA NA 0.00
NA 0.00 NA NA NA NA NA NA NA 0.00
NA 0.00 NA NA NA NA NA NA NA 0.00
NA 0.00 NA NA NA NA NA NA NA 0.00
NA 0.00 NA NA NA NA NA NA NA 0.00
NA 0.00 NA NA NA NA NA NA NA 0.00
#DIV/0! 0.00 #DIV/0! #DIV/0! #DIV/0! 0.00
0.00 0.00 0.00 0.00 0.00 0.00
0.00 0.00 0.00 0.00 0.00 0.00
HLORIC ACID
IEM 2 NaOCl
CTA 1 CTA 2 CTA 3 CTB 1 CTB 2 Tk 1 Tk 2 Tk 3 Tk 4 Tk 5
NA NA NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA NA NA
#DIV/0! #DIV/0!
0.00 0.00
0.00 0.00
SODIUM HYPOCHLORITE
Excess NaOH SG
Tk 1 Tk 2 Tk 3 Tk 4 Tk 5 Tk 1 Tk 2 Tk 3 Tk 4 Tk 5
0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00
0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00
0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00
0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00
0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00
0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00
0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00
0.00 0.00
0.00 0.00
0.00 0.00
Polished brine
LIQUID CHLORINE Ca+Mg Ca + Mg in SPB Na2SO4 in SPB
Tank Feed % H2 IEM 1 IEM 2 IEM 1 IEM 2 IEM 1 IEM 2
NA NA NA 0.00 0.00 nil nil NA NA
NA NA NA 0.00 0.00 nil nil NA NA
NA NA NA 0.00 0.00 nil nil NA NA
NA NA NA 0.00 0.00 nil nil NA NA
NA NA 0.00 0.00 0.00 nil nil NA NA
NA NA NA 0.00 0.00 nil nil NA NA
NA NA NA 0.00 0.00 nil nil NA NA
#DIV/0! #DIV/0! 0.00 0.00 0.00 #DIV/0! #DIV/0! #DIV/0! #DIV/0!
0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00
0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00
CHLORATE Depleted brine
SPB Depleted brine NaCl Free Cl2 pH
IEM 1 IEM 2 IEM 1 IEM 2 IEM 1 IEM 2 IEM 1 IEM 2 IEM 2
NA NA NA NA 0 0 negative negative NA
NA NA NA NA 0 0 negative negative NA
NA NA NA NA 0 0 negative negative NA
NA NA NA NA 0 0 negative negative NA
NA NA NA NA 0 0 negative negative NA
NA NA NA NA 0 0 negative negative NA
NA NA NA NA 0 0 negative negative NA
#DIV/0! #DIV/0! #DIV/0! #DIV/0! 0.00 0.00 negative negative #DIV/0!
positive positive
0.00 0.00 0.00 0.00 0.00 0.00 0 0 0.00
negative negative
0.00 0.00 0.00 0.00 0.00 0.00 7 7 0.00

positive negative
GAS ANALYSIS - IEM 1
Instrument Line A Line B
H2SO4 Air SiO2 Cl2 H2 O2+CO2 Cl2 H2 O2+CO2
NA 0.0 NA NA 0 0 0 0 0
NA 0.0 NA NA 0 0 0 0 0
NA 0.0 NA NA 0 0 0 0 0
NA 0.0 NA NA 0 0 0 0 0
NA 0.0 NA NA 0 0 0 0 0
NA 0.0 NA NA 0 0 0 0 0
NA 0.0 NA NA 0 0 0 0 0
#DIV/0! 0.00 #DIV/0! #DIV/0! 0.00 0.00 0.00 0.00 0.00
positive
0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00
negative
0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00
GAS ANALYSIS - IEM 2
Line A Line B GAS ANALYSIS - FLUE GAS pH
Cl2 H2 O2+CO2 Cl2 H2 O2+CO2 CO CO2 O2 6:00 AM
NA 0 0 0 0 0 NA 0 0 0.00
NA 0 0 0 0 0 NA 0 0 0.00
NA 0 0 0 0 0 NA 0 0 0.00
NA 0 0 0 0 0 NA 0 0 0.00
NA 0 0 0 0 0 NA 0 0 0.00
NA 0 0 0 0 0 NA 0 0 0.00
NA 0 0 0 0 0 NA 0 0 0.00
#DIV/0! 0.00 0.00 0.00 0.00 0.00 #DIV/0! 0.00 0.00 0.00
0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00
0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00
S-2 S-5
pH
7:00 PM Hg, ppb TDS TSS Color COD pH Hg, ppb TDS TSS
0.00 NA NA NA NA NA NA NA NA NA
0.00 NA NA NA NA NA NA NA NA NA
0.00 NA NA NA NA NA NA NA NA NA
0.00 NA NA NA NA NA NA NA NA NA
0.00 NA NA NA NA NA NA NA NA NA
0.00 NA NA NA NA NA NA NA NA NA
0.00 NA NA NA NA NA NA NA NA NA
0.00 #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0!
0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00
0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00
S-5 S-8(Sludge Pond Outlet 1) S-9(Sludge Po

Color COD pH Hg, ppb TDS TSS Color COD pH Hg, ppb
NA NA NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA NA NA
#DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0!
0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00
0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00
S-9(Sludge Pond Outlet 2) LAGOON

TDS TSS Color COD pH Hg, ppb TDS TSS Color COD
NA NA NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA NA NA
#DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0!
0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00
0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00
JBC Evap Canal Total Canal

pH gpl NaOH pH gpl NaOH pH gpl NaOH S-3 S-4 S-7


NA 0.00 0.00 0.00 0.00 0.00 NA 0.00 0.00
NA 0.00 0.00 0.00 0.00 0.00 NA 0.00 0.00
NA 0.00 0.00 0.00 0.00 0.00 NA 0.00 0.00
NA 0.00 0.00 0.00 0.00 0.00 NA 0.00 0.00
NA 0.00 0.00 0.00 0.00 0.00 NA 0.00 0.00
NA 0.00 0.00 0.00 0.00 0.00 NA 0.00 0.00
NA 0.00 0.00 0.00 0.00 0.00 NA 0.00 0.00
#DIV/0! 0.00 0.00 0.00 0.00 0.00 #DIV/0! 0.00 0.00
0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00
0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00
50% NaOH 32% NaOH
IEM 1 IEM 2 IEM 1
WEEK DAY DATE Online Tk A Tk B Online Tank 9 Online Tk A
Wed 3-May 0.00 NA NA 0.00 NA 0.00 NA
Thu 4-May 0.00 NA NA 0.00 NA 0.00 NA
Fri 5-May 0.00 NA NA 0.00 NA 0.00 NA
Sat 6-May 0.00 NA NA 0.00 NA 0.00 NA
Sun 7-May 0.00 NA NA 0.00 NA 0.00 NA
Mon 8-May 0.00 NA NA 0.00 NA 0.00 NA
6 Tue 9-May 0.00 NA NA 0.00 NA 0.00 NA
Average 0.00 #DIV/0! 0.00 #DIV/0! 0.00 #DIV/0!
Minimum 0.00 0.00 0.00 0.00 0.00 0.00
Maximum 0.00 0.00 0.00 0.00 0.00 0.00
32% NaOH HYDROCHLORIC ACID
IEM 1 IEM 2 IEM 1
Tk B Online Tank 9 Online Tank 1 Tank 2 Tank 3 Tank 4 Tank 5 Online
NA 0.00 NA NA NA NA NA NA NA 0.00
NA 0.00 NA NA NA NA NA NA NA 0.00
NA 0.00 NA NA NA NA NA NA NA 0.00
NA 0.00 NA NA NA NA NA NA NA 0.00
NA 0.00 NA NA NA NA NA NA NA 0.00
NA 0.00 NA NA NA NA NA NA NA 0.00
NA 0.00 NA NA NA NA NA NA NA 0.00
#DIV/0! 0.00 #DIV/0! #DIV/0! #DIV/0! 0.00
0.00 0.00 0.00 0.00 0.00 0.00
0.00 0.00 0.00 0.00 0.00 0.00
HLORIC ACID
IEM 2 NaOCl
CTA 1 CTA 2 CTA 3 CTB 1 CTB 2 Tk 1 Tk 2 Tk 3 Tk 4 Tk 5
NA NA NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA NA NA
#DIV/0! #DIV/0!
0.00 0.00
0.00 0.00
SODIUM HYPOCHLORITE
Excess NaOH SG
Tk 1 Tk 2 Tk 3 Tk 4 Tk 5 Tk 1 Tk 2 Tk 3 Tk 4 Tk 5
0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00
0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00
0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00
0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00
0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00
0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00
0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00
0.00 0.00
0.00 0.00
0.00 0.00
Polished brine
LIQUID CHLORINE Ca+Mg Ca + Mg in SPB Na2SO4 in SPB
Tank Feed % H2 IEM 1 IEM 2 IEM 1 IEM 2 IEM 1 IEM 2
NA NA NA 0.00 0.00 nil nil NA NA
NA NA NA 0.00 0.00 nil nil NA NA
NA NA NA 0.00 0.00 nil nil NA NA
NA NA NA 0.00 0.00 nil nil NA NA
NA NA NA 0.00 0.00 nil nil NA NA
NA NA NA 0.00 0.00 nil nil NA NA
NA NA NA 0.00 0.00 nil nil NA NA
#DIV/0! #DIV/0! #DIV/0! 0.00 0.00 #DIV/0! #DIV/0! #DIV/0! #DIV/0!
0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00
0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00
CHLORATE Depleted brine
SPB Depleted brine NaCl Free Cl2 pH
IEM 1 IEM 2 IEM 1 IEM 2 IEM 1 IEM 2 IEM 1 IEM 2 IEM 2
NA NA NA NA 0 0 negative negative NA
NA NA NA NA 0 0 negative negative NA
NA NA NA NA 0 0 negative negative NA
NA NA NA NA 0 0 negative negative NA
NA NA NA NA 0 0 negative negative NA
NA NA NA NA 0 0 negative negative NA
NA NA NA NA 0 0 negative negative NA
#DIV/0! #DIV/0! #DIV/0! #DIV/0! 0.00 0.00 negative negative #DIV/0!
positive positive
0.00 0.00 0.00 0.00 0.00 0.00 0 0 0.00
negative negative
0.00 0.00 0.00 0.00 0.00 0.00 7 7 0.00

positive negative
GAS ANALYSIS - IEM 1
Instrument Line A Line B
H2SO4 Air SiO2 Cl2 H2 O2+CO2 Cl2 H2 O2+CO2
NA 0.0 NA NA 0 0 0 0 0
NA 0.0 NA NA 0 0 0 0 0
NA 0.0 NA NA 0 0 0 0 0
NA 0.0 NA NA 0 0 0 0 0
NA 0.0 NA NA 0 0 0 0 0
NA 0.0 NA NA 0 0 0 0 0
NA 0.0 NA NA 0 0 0 0 0
#DIV/0! 0.00 #DIV/0! #DIV/0! 0.00 0.00 0.00 0.00 0.00
positive
0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00
negative
0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00
GAS ANALYSIS - IEM 2
Line A Line B GAS ANALYSIS - FLUE GAS pH
Cl2 H2 O2+CO2 Cl2 H2 O2+CO2 CO CO2 O2 6:00 AM
NA 0 0 0 0 0 NA 0 0 0.00
NA 0 0 0 0 0 NA 0 0 0.00
NA 0 0 0 0 0 NA 0 0 0.00
NA 0 0 0 0 0 NA 0 0 0.00
NA 0 0 0 0 0 NA 0 0 0.00
NA 0 0 0 0 0 NA 0 0 0.00
NA 0 0 0 0 0 NA 0 0 0.00
#DIV/0! 0.00 0.00 0.00 0.00 0.00 #DIV/0! 0.00 0.00 0.00
0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00
0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00
S-2 S-5
pH
7:00 PM Hg, ppb TDS TSS Color COD pH Hg, ppb TDS TSS
0.00 NA NA NA NA NA NA NA NA NA
0.00 NA NA NA NA NA NA NA NA NA
0.00 NA NA NA NA NA NA NA NA NA
0.00 NA NA NA NA NA NA NA NA NA
0.00 NA NA NA NA NA NA NA NA NA
0.00 NA NA NA NA NA NA NA NA NA
0.00 NA NA NA NA NA NA NA NA NA
0.00 #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0!
0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00
0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00
S-5 S-8(Sludge Pond Outlet 1) S-9(Sludge Po

Color COD pH Hg, ppb TDS TSS Color COD pH Hg, ppb
NA NA NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA NA NA
#DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0!
0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00
0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00
S-9(Sludge Pond Outlet 2) LAGOON

TDS TSS Color COD pH Hg, ppb TDS TSS Color COD
NA NA NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA NA NA
#DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0!
0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00
0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00
JBC Evap Canal Total Canal

pH gpl NaOH pH gpl NaOH pH gpl NaOH S-3 S-4 S-7


NA 0.00 0.00 0.00 0.00 0.00 NA 0.00 0.00
NA 0.00 0.00 0.00 0.00 0.00 NA 0.00 0.00
NA 0.00 0.00 0.00 0.00 0.00 NA 0.00 0.00
NA 0.00 0.00 0.00 0.00 0.00 NA 0.00 0.00
NA 0.00 0.00 0.00 0.00 0.00 NA 0.00 0.00
NA 0.00 0.00 0.00 0.00 0.00 NA 0.00 0.00
NA 0.00 0.00 0.00 0.00 0.00 NA 0.00 0.00
#DIV/0! 0.00 0.00 0.00 0.00 0.00 #DIV/0! 0.00 0.00
0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00
0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00
50% NaOH 32% NaOH
IEM 1 IEM 2 IEM 1
WEEK DAY DATE Online Tk A Tk B Online Tank 9 Online Tk A
Wed 29-Mar 49.98 49.92 NA 49.59 NA NA NA
Thu 30-Mar 49.73 NA NA SD NA 31.15 NA
Fri 31-Mar 49.64 50.00 NA 51.59 48.26 30.07 NA
Sat 1-Apr 49.28 49.71 NA 49.09 NA 30.44 NA
Sun 2-Apr 49.81 49.87 NA SD NA 30.17 NA
Mon 3-Apr 0.00 NA NA 0.00 NA 0.00 NA
1 Tue 4-Apr 49.49 NA NA 51.50 48.83 30.45 NA
Wed 5-Apr 48.96 49.76 NA SD NA 30.77 NA
Thu 6-Apr 49.27 NA NA 50.04 NA 29.66 NA
Fri 7-Apr SD 49.70 NA SD NA SD NA
Sat 8-Apr 49.87 49.56 NA 49.83 NA 30.76 NA
Sun 9-Apr 49.70 NA NA 46.88 NA 30.78 NA
Mon 10-Apr 50.35 50.56 NA SD 49.35 30.08 NA
2 Tue 11-Apr 50.14 49.67 NA SD NA 29.53 NA
Wed 12-Apr 48.77 NA NA NA NA 30.29 NA
Thu 13-Apr 49.38 NA NA SD SD 29.66 NA
Fri 14-Apr 50.14 49.66 NA 50.27 NA 29.88 NA
Sat 15-Apr 49.70 49.63 NA SD NA 30.59 NA
Sun 16-Apr 48.49 49.40 NA SD 48.67 30.13 NA
Mon 17-Apr 49.94 49.37 NA 48.44 48.44 29.45 NA
3 Tue 18-Apr SD 0.00 0.00 48.28 NA SD 0.00
Wed 19-Apr 0.00 NA NA 0.00 NA 0.00 NA
Thu 20-Apr 0.00 NA NA 0.00 NA 0.00 NA
Fri 21-Apr 0.00 NA NA 0.00 NA 0.00 NA
Sat 22-Apr 0.00 NA NA 0.00 NA 0.00 NA
Sun 23-Apr 0.00 NA NA 0.00 NA 0.00 NA
Mon 24-Apr 0.00 NA NA 0.00 NA 0.00 NA
4 Tue 25-Apr 0.00 NA NA 0.00 NA 0.00 NA
Wed 26-Apr 0.00 NA NA 0.00 NA 0.00 NA
Thu 27-Apr 0.00 NA NA 0.00 NA 0.00 NA
Fri 28-Apr 0.00 NA NA 0.00 NA 0.00 NA
Sat 29-Apr 0.00 NA NA 0.00 NA 0.00 NA
Sun 30-Apr 0.00 NA NA 0.00 NA 0.00 NA
Mon 1-May 0.00 NA NA 0.00 NA 0.00 NA
5 Tue 2-May 0.00 NA NA 0.00 NA 0.00 NA
Wed 3-May 0.00 NA NA 0.00 NA 0.00 NA
Thu 4-May 0.00 NA NA 0.00 NA 0.00 NA
Fri 5-May 0.00 NA NA 0.00 NA 0.00 NA
Sat 6-May 0.00 NA NA 0.00 NA 0.00 NA
Sun 7-May 0.00 NA NA 0.00 NA 0.00 NA
Mon 8-May 0.00 NA NA 0.00 NA 0.00 NA
6 Tue 9-May 0.00 NA NA 0.00 NA 0.00 NA
Average 22.32 43.12 15.48 48.71 13.18 0.00
Minimum 0.00 0.00 0.00 48.26 0.00 0.00
Maximum 50.35 50.56 51.59 49.35 31.15 0.00
32% NaOH HYDROCHLORIC ACID
IEM 1 IEM 2 IEM 1
Tk B Online Tank 9 Online Tank 1 Tank 2 Tank 3 Tank 4 Tank 5 Online
NA 31.13 30.98 SD NA NA NA NA NA 33.01
NA 31.72 30.79 SD NA NA NA NA NA 33.07
NA 31.09 NA SD NA NA NA NA NA 33.31
NA 31.13 NA NA NA NA NA NA NA 32.39
NA 30.91 30.90 NA NA NA NA NA NA 33.09
NA 0.00 NA NA NA NA NA NA NA 0.00
NA 31.42 NA NA NA NA NA NA NA 33.42
NA 30.82 30.88 NA NA NA NA NA NA 33.15
NA 31.05 31.04 NA NA NA NA NA NA 33.20
NA 30.86 31.30 SD NA NA NA NA NA 34.05
NA 31.15 NA 32.68 NA NA 33.20 NA NA 33.57
NA 30.56 NA 33.50 NA NA NA NA 32.87 33.50
NA SD NA 33.03 32.82 NA NA NA NA SD
NA SD 31.22 32.59 NA NA NA NA NA SD
NA 30.37 NA 32.34 NA NA 32.51 NA NA 32.59
NA 30.52 30.41 NA NA NA NA NA 32.16 33.19
NA 31.27 NA NA NA NA NA NA NA 33.56
NA 31.01 NA NA NA NA NA NA NA 33.87
NA 30.76 NA NA NA NA NA NA NA 33.73
NA 30.64 NA NA NA NA NA NA NA 32.07
0.00 30.76 30.68 SD NA NA NA NA NA 32.86
NA 0.00 NA NA NA NA NA NA NA 0.00
NA 0.00 NA NA NA NA NA NA NA 0.00
NA 0.00 NA NA NA NA NA NA NA 0.00
NA 0.00 NA NA NA NA NA NA NA 0.00
NA 0.00 NA NA NA NA NA NA NA 0.00
NA 0.00 NA NA NA NA NA NA NA 0.00
NA 0.00 NA NA NA NA NA NA NA 0.00
NA 0.00 NA NA NA NA NA NA NA 0.00
NA 0.00 NA NA NA NA NA NA NA 0.00
NA 0.00 NA NA NA NA NA NA NA 0.00
NA 0.00 NA NA NA NA NA NA NA 0.00
NA 0.00 NA NA NA NA NA NA NA 0.00
NA 0.00 NA NA NA NA NA NA NA 0.00
NA 0.00 NA NA NA NA NA NA NA 0.00
NA 0.00 NA NA NA NA NA NA NA 0.00
NA 0.00 NA NA NA NA NA NA NA 0.00
NA 0.00 NA NA NA NA NA NA NA 0.00
NA 0.00 NA NA NA NA NA NA NA 0.00
NA 0.00 NA NA NA NA NA NA NA 0.00
NA 0.00 NA NA NA NA NA NA NA 0.00
NA 0.00 NA NA NA NA NA NA NA 0.00
0.00 13.93 30.91 32.83 32.71 14.94
0.00 0.00 30.41 32.34 32.16 0.00
0.00 31.72 31.30 33.50 33.20 34.05
HLORIC ACID
IEM 2 NaOCl
CTA 1 CTA 2 CTA 3 CTB 1 CTB 2 Tk 1 Tk 2 Tk 3 Tk 4 Tk 5
NA NA NA 32.54 NA NA NA NA 7.77 NA
NA NA NA NA 32.96 NA NA NA NA 7.78
NA 33.25 NA NA 33.10 NA NA NA 7.57 NA
NA NA NA 33.27 NA NA NA NA NA 7.97
NA 33.16 NA NA NA NA NA NA 7.89 NA
NA NA NA NA NA NA NA NA NA NA
NA 32.54 NA 33.33 NA NA NA NA 7.48 NA
NA NA NA NA 33.37 NA NA NA NA 7.55
NA NA NA 33.33 NA NA NA NA 7.54 NA
NA 33.30 NA 33.44 NA NA NA NA NA NA
NA NA NA NA 32.88 NA NA NA 7.80 7.61
NA 33.41 NA NA NA NA NA NA NA 8.70
NA NA NA NA 33.18 NA NA NA 7.80 7.72
NA NA NA NA NA NA NA NA 7.68 NA
NA NA NA 33.39 NA NA NA NA 7.61 NA
NA NA NA NA 33.38 NA NA NA NA 7.80
NA NA NA NA NA NA NA NA NA NA
NA NA 33.45 33.13 NA NA NA NA 7.56 7.77
NA 33.45 NA NA NA NA NA NA 7.45 NA
NA NA 33.19 NA 32.67 NA NA NA NA 7.96
NA NA NA 33.16 NA NA NA NA 7.68 NA
NA NA NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA NA NA
33.17 7.75
32.54 7.45
33.45 8.70
SODIUM HYPOCHLORITE
Excess NaOH SG
Tk 1 Tk 2 Tk 3 Tk 4 Tk 5 Tk 1 Tk 2 Tk 3 Tk 4 Tk 5
0.00 0.00 0.00 0.82 0.00 0.00 0.00 0.00 1.13 0.00
0.00 0.00 0.00 0.00 0.57 0.00 0.00 0.00 0.00 1.14
0.00 0.00 0.00 0.65 0.00 0.00 0.00 0.00 1.13 0.00
0.00 0.00 0.00 0.00 0.53 0.00 0.00 0.00 0.00 1.14
0.00 0.00 0.00 0.72 0.00 0.00 0.00 0.00 1.13 0.00
0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00
0.00 0.00 0.00 0.72 0.00 0.00 0.00 0.00 1.13 0.00
0.00 0.00 0.00 0.00 0.70 0.00 0.00 0.00 0.00 1.13
0.00 0.00 0.00 0.75 0.00 0.00 0.00 0.00 1.13 0.00
0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00
0.00 0.00 0.00 0.81 0.82 0.00 0.00 0.00 1.13 1.15
0.00 0.00 0.00 0.00 0.91 0.00 0.00 0.00 0.00 1.13
0.00 0.00 0.00 0.75 0.73 0.00 0.00 0.00 1.14 1.13
0.00 0.00 0.00 0.68 0.00 0.00 0.00 0.00 1.13 0.00
0.00 0.00 0.00 0.70 0.00 0.00 0.00 0.00 1.13 0.00
0.00 0.00 0.00 0.00 0.64 0.00 0.00 0.00 0.00 1.14
0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00
0.00 0.00 0.00 0.60 0.53 0.00 0.00 0.00 1.13 1.14
0.00 0.00 0.00 0.72 0.00 0.00 0.00 0.00 1.13 0.00
0.00 0.00 0.00 0.00 0.74 0.00 0.00 0.00 0.00 1.14
0.00 0.00 0.00 0.79 0.00 0.00 0.00 0.00 1.14 0.00
0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00
0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00
0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00
0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00
0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00
0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00
0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00
0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00
0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00
0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00
0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00
0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00
0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00
0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00
0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00
0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00
0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00
0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00
0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00
0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00
0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00
0.07 0.11
0.00 0.00
0.91 1.15
Polished brine
LIQUID CHLORINE Ca+Mg Ca + Mg in SPB Na2SO4 in SPB
Tank Feed % H2 IEM 1 IEM 2 IEM 1 IEM 2 IEM 1 IEM 2
NA NA NA 0.00 0.00 14 8 NA NA
NA NA NA 3.56 5.34 34 4 2.96 4.74
NA NA NA 0.00 0.00 14 20 NA NA
NA NA NA 0.00 0.00 68 nil NA NA
NA NA NA 0.00 0.00 0 0 0.00 0.00
NA NA NA 0.00 0.00 nil nil NA NA
NA NA NA 0.00 0.00 12 12 NA NA
NA NA NA 0.00 0.00 25 4 NA NA
NA NA NA 0.00 0.00 18 nil 2.81 5.48
NA NA NA 0.00 0.00 25 nil NA NA
NA NA NA 0.00 0.00 5 nil NA NA
NA NA NA 0.00 0.00 0 0 0.00 0.00
NA NA NA 0.00 0.00 34 0 2.22 0.00
NA NA NA 4.00 0.00 2 0 2.22 0.00
NA NA NA 0.00 0.00 12 10 NA NA
NA NA NA 2.67 1.78 30 2 2.22 4.14
NA NA NA 0.00 0.00 0 0 0.00 0.00
NA NA NA 0.00 0.00 36 2 NA NA
NA NA NA 0.00 0.00 0 0 0.00 0.00
NA NA NA 2.67 7.12 12 nil 2.52 4.14
NA NA NA 0.00 0.00 0 4 0.00 NA
NA NA NA 0.00 0.00 nil nil NA NA
NA NA NA 0.00 0.00 nil nil NA NA
NA NA NA 0.00 0.00 nil nil NA NA
NA NA NA 0.00 0.00 nil nil NA NA
NA NA NA 0.00 0.00 nil nil NA NA
NA NA NA 0.00 0.00 nil nil NA NA
NA NA NA 0.00 0.00 nil nil NA NA
NA NA NA 0.00 0.00 nil nil NA NA
NA NA NA 0.00 0.00 nil nil NA NA
NA NA NA 0.00 0.00 nil nil NA NA
NA NA NA 0.00 0.00 nil nil NA NA
NA NA 0.00 0.00 0.00 nil nil NA NA
NA NA NA 0.00 0.00 nil nil NA NA
NA NA NA 0.00 0.00 nil nil NA NA
NA NA NA 0.00 0.00 nil nil NA NA
NA NA NA 0.00 0.00 nil nil NA NA
NA NA NA 0.00 0.00 nil nil NA NA
NA NA NA 0.00 0.00 nil nil NA NA
NA NA NA 0.00 0.00 nil nil NA NA
NA NA NA 0.00 0.00 nil nil NA NA
NA NA NA 0.00 0.00 nil nil NA NA
#DIV/0! #DIV/0! 0.00 0.31 0.34 17.05 4.40 1.36 1.85
0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00
0.00 0.00 0.00 4.00 7.12 68.00 20.00 2.96 5.48
CHLORATE Depleted brine
SPB Depleted brine NaCl Free Cl2 pH
IEM 1 IEM 2 IEM 1 IEM 2 IEM 1 IEM 2 IEM 1 IEM 2 IEM 2
NA NA NA NA 196 226 negative negative NA
5.96 25.76 11.57 37.51 197 227 negative negative 1.83
NA NA NA NA 202 225 negative negative NA
NA NA NA NA 204 222 positive negative NA
0.00 0.00 0.00 0.00 NA NA 0 0 0.00
NA NA NA NA 0 0 negative negative NA
NA NA NA NA 228 240 negative negative NA
NA NA NA NA 209 226 negative negative NA
NA NA NA NA 209 226 negative negative NA
NA 25.41 0.00 34.97 SD 226 0 negative 2.89
NA NA NA NA 207 222 negative negative NA
0.00 0.00 0.00 0.00 NA NA 0 0 0.00
NA 0.00 NA 0.00 198 SD positive 0 0.00
3.51 0.00 8.06 0.00 181 SD positive 0 0.00
NA NA NA NA 183 184 negative negative NA
4.82 18.84 8.33 29.36 183 215 negative negative NA
0.00 0.00 0.00 0.00 NA NA 0 0 0.00
NA NA NA NA 188 244 negative negative NA
0.00 0.00 0.00 0.00 NA NA 0 0 0.00
4.38 18.49 9.46 28.39 182 211 negative negative 2.11
0.00 NA 0.00 NA SD 212 0 negative NA
NA NA NA NA 0 0 negative negative NA
NA NA NA NA 0 0 negative negative NA
NA NA NA NA 0 0 negative negative NA
NA NA NA NA 0 0 negative negative NA
NA NA NA NA 0 0 negative negative NA
NA NA NA NA 0 0 negative negative NA
NA NA NA NA 0 0 negative negative NA
NA NA NA NA 0 0 negative negative NA
NA NA NA NA 0 0 negative negative NA
NA NA NA NA 0 0 negative negative NA
NA NA NA NA 0 0 negative negative NA
NA NA NA NA 0 0 negative negative NA
NA NA NA NA 0 0 negative negative NA
NA NA NA NA 0 0 negative negative NA
NA NA NA NA 0 0 negative negative NA
NA NA NA NA 0 0 negative negative NA
NA NA NA NA 0 0 negative negative NA
NA NA NA NA 0 0 negative negative NA
NA NA NA NA 0 0 negative negative NA
NA NA NA NA 0 0 negative negative NA
NA NA NA NA 0 0 negative negative NA
2.07 8.85 3.74 13.02 76.86 86.28 negative negative 0.76
0.00 0.00 0.00 0.00 0.00 0.00 3 0 0.00
5.96 25.76 11.57 37.51 228.00 244.00 33 36 2.89

positive positive

negative negative
positive

negative negative

positive negative
GAS ANALYSIS - IEM 1
Instrument Line A Line B
H2SO4 Air SiO2 Cl2 H2 O2+CO2 Cl2 H2 O2+CO2
NA 0.0 NA NA 0 0 0 0 0
NA UNDER REPAIR 130 NA 0 0 0 0 0
NA UNDER REPAIR NA NA 0 0 0 0 0
NA for repair NA NA 0 0 0 0 0
NA NA NA NA 0 0 0 0 0
NA 0.0 NA NA 0 0 0 0 0
NA for repair NA NA 0 0 0 0 0
NA for repair NA NA 0 0 0 0 0
NA for repair NA NA 0 0 0 0 0
NA for repair NA NA 0 0 0 0 0
NA 5.7 NA NA 0 0 0 0 0
NA NA NA NA 0 0 0 0 0
NA 8.6 NA NA 0 0 0 0 0
NA 7.6 NA NA 0 0 0 0 0
NA 5.6 NA NA 0 0 0 0 0
NA 8.6 NA NA 0 0 0 0 0
NA NA NA NA 0 0 0 0 0
NA 7.1 NA NA 0 0 0 0 0
NA NA NA NA 0 0 0 0 0
97.22 6.5 NA NA 0 0 0 0 0
NA 6.5 NA NA 0 0 0 0 0
NA 0.0 NA NA 0 0 0 0 0
NA 0.0 NA NA 0 0 0 0 0
NA 0.0 NA NA 0 0 0 0 0
NA 0.0 NA NA 0 0 0 0 0
NA 0.0 NA NA 0 0 0 0 0
NA 0.0 NA NA 0 0 0 0 0
NA 0.0 NA NA 0 0 0 0 0
NA 0.0 NA NA 0 0 0 0 0
NA 0.0 NA NA 0 0 0 0 0
NA 0.0 NA NA 0 0 0 0 0
NA 0.0 NA NA 0 0 0 0 0
NA 0.0 NA NA 0 0 0 0 0
NA 0.0 NA NA 0 0 0 0 0
NA 0.0 NA NA 0 0 0 0 0
NA 0.0 NA NA 0 0 0 0 0
NA 0.0 NA NA 0 0 0 0 0
NA 0.0 NA NA 0 0 0 0 0
NA 0.0 NA NA 0 0 0 0 0
NA 0.0 NA NA 0 0 0 0 0
NA 0.0 NA NA 0 0 0 0 0
NA 0.0 NA NA 0 0 0 0 0
97.22 1.81 130.00 #DIV/0! 0.00 0.00 0.00 0.00 0.00
97.22 0.00 130.00 0.00 0.00 0.00 0.00 0.00 0.00
97.22 8.60 130.00 0.00 0.00 0.00 0.00 0.00 0.00

positive

negative
negative
GAS ANALYSIS - IEM 2
Line A Line B GAS ANALYSIS - FLUE GAS pH
Cl2 H2 O2+CO2 Cl2 H2 O2+CO2 CO CO2 O2 6:00 AM
NA 0 0 0 0 0 NA 0 0 8.66
NA 0 0 0 0 0 NA 0 0 8.63
NA 0 0 0 0 0 NA 0 0 8.58
NA 0 0 0 0 0 NA 0 0 8.56
NA 0 0 0 0 0 NA 0 0 NA
NA 0 0 0 0 0 NA 0 0 0.00
NA 0 0 0 0 0 NA 0 0 8.55
NA 0 0 0 0 0 NA 0 0 8.54
NA 0 0 0 0 0 NA 0 0 8.55
NA 0 0 0 0 0 NA 0 0 8.68
NA 0 0 0 0 0 NA 0 0 8.68
NA 0 0 0 0 0 NA 0 0 NA
NA 0 0 0 0 0 NA 0 0 8.68
NA 0 0 0 0 0 NA 0 0 8.88
NA 0 0 0 0 0 NA 0 0 8.85
NA 0 0 0 0 0 NA 0 0 8.70
NA 0 0 0 0 0 NA 0 0 NA
NA 0 0 0 0 0 NA 0 0 8.58
NA 0 0 0 0 0 NA 0 0 NA
NA 0 0 0 0 0 NA 0 0 8.78
NA 0 0 0 0 0 NA 0 0 8.60
NA 0 0 0 0 0 NA 0 0 0.00
NA 0 0 0 0 0 NA 0 0 0.00
NA 0 0 0 0 0 NA 0 0 0.00
NA 0 0 0 0 0 NA 0 0 0.00
NA 0 0 0 0 0 NA 0 0 0.00
NA 0 0 0 0 0 NA 0 0 0.00
NA 0 0 0 0 0 NA 0 0 0.00
NA 0 0 0 0 0 NA 0 0 0.00
NA 0 0 0 0 0 NA 0 0 0.00
NA 0 0 0 0 0 NA 0 0 0.00
NA 0 0 0 0 0 NA 0 0 0.00
NA 0 0 0 0 0 NA 0 0 0.00
NA 0 0 0 0 0 NA 0 0 0.00
NA 0 0 0 0 0 NA 0 0 0.00
NA 0 0 0 0 0 NA 0 0 0.00
NA 0 0 0 0 0 NA 0 0 0.00
NA 0 0 0 0 0 NA 0 0 0.00
NA 0 0 0 0 0 NA 0 0 0.00
NA 0 0 0 0 0 NA 0 0 0.00
NA 0 0 0 0 0 NA 0 0 0.00
NA 0 0 0 0 0 NA 0 0 0.00
#DIV/0! 0.00 0.00 0.00 0.00 0.00 #DIV/0! 0.00 0.00 3.64
0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00
0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 8.88
S-2 S-5
pH
7:00 PM Hg, ppb TDS TSS Color COD pH Hg, ppb TDS TSS
8.58 NA NA NA NA NA 8.66 NA NA NA
8.54 0.056 204 4 40 NA 8.61 0.168 263 2
8.52 NA NA NA NA NA 8.67 NA NA NA
8.66 NA NA NA NA NA 9.20 NA NA NA
0.00 NA NA NA NA NA NA NA NA NA
0.00 NA NA NA NA NA NA NA NA NA
9.23 NA NA NA NA NA 8.68 NA NA NA
8.52 NA NA NA NA NA 8.83 NA NA NA
8.44 NA NA NA NA NA 8.63 NA NA NA
8.61 NA NA NA NA NA 8.62 NA NA NA
8.48 0.056 256 6 43 NA 8.62 0.335 368 3
0.00 NA NA NA NA NA NA NA NA NA
8.64 NA NA NA NA NA 8.62 NA NA NA
8.62 NA NA NA NA NA 8.53 NA NA NA
8.79 0.112 3800 5 35 NA 8.70 0.224 251 2
8.65 NA NA NA NA NA 8.63 NA NA NA
0.00 NA NA NA NA NA NA NA NA NA
8.63 NA NA NA NA NA 8.67 NA NA NA
0.00 NA NA NA NA NA NA NA NA NA
8.71 NA NA NA NA NA 8.65 NA NA NA
8.57 NA NA NA NA NA 8.62 NA NA NA
0.00 NA NA NA NA NA NA NA NA NA
0.00 NA NA NA NA NA NA NA NA NA
0.00 NA NA NA NA NA NA NA NA NA
0.00 NA NA NA NA NA NA NA NA NA
0.00 NA NA NA NA NA NA NA NA NA
0.00 NA NA NA NA NA NA NA NA NA
0.00 NA NA NA NA NA NA NA NA NA
0.00 NA NA NA NA NA NA NA NA NA
0.00 NA NA NA NA NA NA NA NA NA
0.00 NA NA NA NA NA NA NA NA NA
0.00 NA NA NA NA NA NA NA NA NA
0.00 NA NA NA NA NA NA NA NA NA
0.00 NA NA NA NA NA NA NA NA NA
0.00 NA NA NA NA NA NA NA NA NA
0.00 NA NA NA NA NA NA NA NA NA
0.00 NA NA NA NA NA NA NA NA NA
0.00 NA NA NA NA NA NA NA NA NA
0.00 NA NA NA NA NA NA NA NA NA
0.00 NA NA NA NA NA NA NA NA NA
0.00 NA NA NA NA NA NA NA NA NA
0.00 NA NA NA NA NA NA NA NA NA
3.29 0.07 1420.00 5.00 39.33 #DIV/0! 8.68 0.24 294.00 2.33
0.00 0.06 204.00 4.00 35.00 0.00 8.53 0.17 251.00 2.00
9.23 0.11 3800.00 6.00 43.00 0.00 9.20 0.34 368.00 3.00
S-5 S-8(Sludge Pond Outlet 1) S-9(Sludge Po

Color COD pH Hg, ppb TDS TSS Color COD pH Hg, ppb
NA NA 6.52 NA NA 38 152 nil 8.21 NA
17 NA 6.87 NA NA 22 98 NA 8.25 NA
NA NA 7.07 NA NA 16 96 NA 8.28 NA
NA NA 7.33 NA NA 7 75 NA 8.25 NA
NA NA NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA NA NA
NA NA 7.97 NA NA 9 43 NA 8.43 NA
NA NA 7.40 NA NA 16 104 NA 8.62 NA
NA NA 7.83 NA NA 17 89 NA 8.33 NA
NA NA 7.78 NA NA 11 73 NA 8.36 NA
24 NA 7.63 NA NA 9 110 NA 8.42 NA
NA NA NA NA NA NA NA NA NA NA
NA NA 7.67 NA NA 12 116 NA 8.32 NA
NA NA 7.27 NA NA 7 14 25 8.28 NA
17 NA 7.23 NA NA 7 8 NA 8.68 NA
NA NA NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA NA NA
NA NA 7.50 NA NA 2 14 NA 8.77 NA
NA NA NA NA NA NA NA NA NA NA
NA NA 7.49 NA NA 12 16 15 8.44 NA
NA NA 7.57 NA NA 5 15 NA 8.26 NA
NA NA NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA NA NA
19.33 #DIV/0! 7.41 #DIV/0! #DIV/0! 12.67 68.20 20.00 8.39 #DIV/0!
17.00 0.00 6.52 0.00 0.00 2.00 8.00 15.00 8.21 0.00
24.00 0.00 7.97 0.00 0.00 38.00 152.00 25.00 8.77 0.00
S-9(Sludge Pond Outlet 2) LAGOON

TDS TSS Color COD pH Hg, ppb TDS TSS Color COD
NA 1 16 nil NA NA NA NA NA NA
NA 1 8 NA NA NA NA NA NA NA
NA 2 8 NA NA NA NA NA NA NA
NA 2 0 NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA NA NA
NA 2 7 NA NA NA NA NA NA NA
NA 1 11 NA NA NA NA NA NA NA
NA 3 25 NA NA NA NA NA NA NA
NA 3 11 NA NA NA NA NA NA NA
NA 11 15 NA 8.26 0.056 159 4 28 NA
NA NA NA NA NA NA NA NA NA NA
NA 4 12 NA NA NA NA NA NA NA
NA 2 2 10 NA NA NA NA NA NA
NA 3 4 NA 8.28 0.056 280 5 30 NA
NA NA NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA NA NA
NA 4 12 NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA NA NA
NA 5 6 4 NA NA NA NA NA NA
NA 3 15 NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA NA NA
#DIV/0! 3.13 10.13 7.00 8.27 0.06 219.50 4.50 29.00 #DIV/0!
0.00 1.00 0.00 4.00 8.26 0.06 159.00 4.00 28.00 0.00
0.00 11.00 25.00 10.00 8.28 0.06 280.00 5.00 30.00 0.00
JBC Evap Canal Total Canal

pH gpl NaOH pH gpl NaOH pH gpl NaOH S-3 S-4 S-7


NA 0.00 0.00 0.00 0.00 0.00 NA 0.00 0.00
8.23 ND 8.31 ND 8.07 ND 7.63 8.85 7.84
NA 0.00 0.00 0.00 0.00 0.00 NA 0.00 0.00
NA 0.00 0.00 0.00 0.00 0.00 NA 0.00 0.00
NA 0.00 0.00 0.00 0.00 0.00 NA 0.00 0.00
NA 0.00 0.00 0.00 0.00 0.00 NA 0.00 0.00
NA 0.00 0.00 0.00 0.00 0.00 NA 0.00 0.00
NA 0.00 0.00 0.00 0.00 0.00 NA 0.00 0.00
NA 0.00 0.00 0.00 0.00 0.00 NA 0.00 0.00
NA 0.00 0.00 0.00 0.00 0.00 NA 0.00 0.00
8.17 ND 8.34 ND 8.03 ND 8.25 8.82 8.48
NA 0.00 0.00 0.00 0.00 0.00 NA 0.00 0.00
NA 0.00 0.00 0.00 0.00 0.00 NA 0.00 0.00
NA 0.00 0.00 0.00 0.00 0.00 NA 0.00 0.00
7.78 ND 2.12 ND 6.12 ND 7.95 .8.78 9.68
NA 0.00 0.00 0.00 0.00 0.00 NA 0.00 0.00
NA 0.00 0.00 0.00 0.00 0.00 NA 0.00 0.00
NA 0.00 0.00 0.00 0.00 0.00 NA 0.00 0.00
NA 0.00 0.00 0.00 0.00 0.00 NA 0.00 0.00
NA 0.00 0.00 0.00 0.00 0.00 NA 0.00 0.00
NA 0.00 0.00 0.00 0.00 0.00 NA 0.00 0.00
NA 0.00 0.00 0.00 0.00 0.00 NA 0.00 0.00
NA 0.00 0.00 0.00 0.00 0.00 NA 0.00 0.00
NA 0.00 0.00 0.00 0.00 0.00 NA 0.00 0.00
NA 0.00 0.00 0.00 0.00 0.00 NA 0.00 0.00
NA 0.00 0.00 0.00 0.00 0.00 NA 0.00 0.00
NA 0.00 0.00 0.00 0.00 0.00 NA 0.00 0.00
NA 0.00 0.00 0.00 0.00 0.00 NA 0.00 0.00
NA 0.00 0.00 0.00 0.00 0.00 NA 0.00 0.00
NA 0.00 0.00 0.00 0.00 0.00 NA 0.00 0.00
NA 0.00 0.00 0.00 0.00 0.00 NA 0.00 0.00
NA 0.00 0.00 0.00 0.00 0.00 NA 0.00 0.00
NA 0.00 0.00 0.00 0.00 0.00 NA 0.00 0.00
NA 0.00 0.00 0.00 0.00 0.00 NA 0.00 0.00
NA 0.00 0.00 0.00 0.00 0.00 NA 0.00 0.00
NA 0.00 0.00 0.00 0.00 0.00 NA 0.00 0.00
NA 0.00 0.00 0.00 0.00 0.00 NA 0.00 0.00
NA 0.00 0.00 0.00 0.00 0.00 NA 0.00 0.00
NA 0.00 0.00 0.00 0.00 0.00 NA 0.00 0.00
NA 0.00 0.00 0.00 0.00 0.00 NA 0.00 0.00
NA 0.00 0.00 0.00 0.00 0.00 NA 0.00 0.00
NA 0.00 0.00 0.00 0.00 0.00 NA 0.00 0.00
8.06 0.00 0.45 0.00 0.53 0.00 7.94 0.43 0.62
7.78 0.00 0.00 0.00 0.00 0.00 7.63 0.00 0.00
8.23 0.00 8.34 0.00 8.07 0.00 8.25 8.85 9.68
MABUHAY VINYL CORPORATION
Quality Control Analysis - Weekly Report

Date Prepared : November 15, 2018


Period: 42823 - 42829

To : JSG
Cc : SSCP, RSCO, NAA, CPE

IEM 1 IEM 2
Average Range Average Range
Online 42.56 0 - 49.98 40.35 0 - 51.59
50% NaOH Tanks 49.88 49.71 - 50 48.55 48.26 - 48.83
Online 25.38 0 - 31.15 26.77 0 - 31.72
32% NaOH Tanks #DIV/0! 0-0 30.89 30.79 - 30.98
Online #DIV/0! 0-0 28.33 0 - 33.42
%HCl Tanks #DIV/0! 0-0 33.02 32.54 - 33.33
Polished Brine Ca + Mg, ppm 0.51 0 - 3.56 0.76 0 - 5.34
NaCl, gpl 171.17 0 - 228 190.00 0 - 240
Depleted Brine Free Cl2 negative negative
NaClO3, gpl 5.79 0 - 11.57 18.76 0 - 37.51
After Headtank After T-181
Average Range Average Range
Ca + Mg, ppb 23.67 0 - 68 8.80 0 - 20
SPB Na2SO4, gpl 1.48 0 - 2.96 2.37 0 - 4.74
NaClO3, gpl 2.98 0 - 5.96 12.88 0 - 25.76

Average Range
Sodium % NaOCl 7.74 7.48 - 7.97
Hypochlorite % NaOH 0.11 0 - 0.82
Instrument Air Dew Point 0.00 0-0
Compressor
Sulfuric Acid
( @ LCP) #DIV/0! 0-0

1. IEM1 : NaOH(50%), Depleted brine(Free Cl2, NaClO3)


Non-Conforming
2. IEM2 : Depleted brine(Free Cl2, NaClO3), SPB(Na2SO4)
/ Remarks
3.Utilities : Instrument air(dewpoint)

OVAromin
QC/Technical Lab Supervisor
\ova
MABUHAY VINYL CORPORATION
Quality Control Analysis - Weekly Report

Date Prepared : April 11, 2017


Period: April 5-11, 2017

To : JSG
Cc : SSCP, RSCO, NAA, CPE

IEM 1 IEM 2
Average Range Average Range
Online 49.72 48.96 - 50.35 48.92 46.88 - 50.04
50% NaOH Tanks 49.67 49.56 - 49.76 49.35 49.35 - 49.35
Online 30.26 29.53 - 30.78 30.89 30.56 - 31.15
32% NaOH Tanks NA 31.11 30.88 - 31.3
Online 32.95 32.59 - 33.5 33.49 33.15 - 34.05
%HCl Tanks 32.96 32.82 - 33.2 33.27 32.88 - 33.44
Polished Brine Ca + Mg, ppb 4.00 NA NA
NaCl, gpl 200.80 181 - 209 225.00 222 - 226
Depleted Brine Free Cl2 negative negative
NaClO3, gpl 8.06 NA 34.97 NA
After Headtank After T-181
Average Range Average Range
Ca + Mg, ppm 18.17 2 - 34 1.00 0-4
SPB Na2SO4, gpl 2.42 2.22 - 2.81 2.74 0 - 5.48
NaClO3, gpl 3.51 NA 25.41 NA

Average Range
Sodium % NaOCl 7.80 7.54 - 8.7
Hypochlorite % NaOH 0.77 0.68 - 0.91
Instrument Air Dew Point 7.30 5.7 - 8.6
Compressor
Sulfuric Acid
( @ LCP) NA NA

1. IEM1 : None
Non-Conforming
2. IEM2 : Depleted brine, SPB(NaClO3)
/ Remarks
3.Utilities : Instrument air(dewpoint)

OVAromin
QC/Technical Lab Supervisor

\ova
MABUHAY VINYL CORPORATION
Quality Control Analysis - Weekly Report

Date Prepared : November 15, 2018


Period: April 12-18, 2017

To : JSG
Cc : SSCP, RSCO, NAA, CPE

IEM 1 IEM 2
Average Range Average Range
Online 49.40 48.49 - 50.14 49.00 48.28 - 50.27
50% NaOH Tanks 49.52 49.37 - 49.66 48.56 48.44 - 48.67
Online 30.00 29.45 - 30.59 30.76 30.37 - 31.27
32% NaOH Tanks NA 30.55 30.41 - 30.68
Online 32.34 NA 33.12 32.07 - 33.87
%HCl Tanks 32.34 32.16 - 32.51 33.23 32.67 - 33.45
Polished Brine Ca + Mg, ppb 2.67 NA 4.45 1.78 - 7.12
NaCl, gpl 184.00 182 - 188 213.20 184 - 244
Depleted Brine Free Cl2 negative negative
NaClO3, gpl 8.90 8.33 - 9.46 28.88 28.39 - 29.36
After Headtank After T-181
Average Range Average Range
Ca + Mg, ppm 22.50 12 - 36 3.60 0 - 10
SPB Na2SO4, gpl 2.37 2.22 - 2.52 4.14 NA
NaClO3, gpl 4.60 4.38 - 4.82 18.67 18.49 - 18.84

Average Range
Sodium % NaOCl 7.69 7.45 - 7.96
Hypochlorite % NaOH 0.67 0.53 - 0.79
Instrument Air Dew Point 6.86 5.6 - 8.6
Compressor
Sulfuric Acid
( @ LCP) 97.22 NA

1. IEM1 : SPB(Ca+Mg), Depleted brine(NaCl)


Non-Conforming
2. IEM2 : Depleted brine(NaClO3
/ Remarks
3.Utilities : Instrument air(dewpoint)

OVAromin
QC/Technical Lab Supervisor

\ova
MABUHAY VINYL CORPORATION
Quality Control Analysis - Weekly Report

Date Prepared : November 15, 2018


Period: 42844 - 42850

To : JSG
Cc : SSCP, RSCO, NAA, CPE

IEM 1 IEM 2
Average Range Average Range
Online 0.00 0-0 0.00 0-0
50% NaOH Tanks #DIV/0! 0-0 #DIV/0! 0-0
Online 0.00 0-0 0.00 0-0
32% NaOH Tanks #DIV/0! 0-0 #DIV/0! 0-0
Online #DIV/0! 0-0 0.00 0-0
%HCl Tanks #DIV/0! 0-0 #DIV/0! 0-0
Polished Brine Ca + Mg, ppm 0.00 0-0 0.00 0-0
NaCl, gpl 0.00 0-0 0.00 0-0
Depleted Brine Free Cl2 negative negative
NaClO3, gpl #DIV/0! 0-0 #DIV/0! 0-0
After Headtank After T-181
Average Range Average Range
Ca + Mg, ppb #DIV/0! 0-0 #DIV/0! 0-0
SPB Na2SO4, gpl #DIV/0! 0-0 #DIV/0! 0-0
NaClO3, gpl #DIV/0! 0-0 #DIV/0! 0-0

Average Range
Sodium % NaOCl #DIV/0! 0-0
Hypochlorite % NaOH 0.00 0-0
Instrument Air Dew Point 0.00 0-0
Compressor
Sulfuric Acid
( @ LCP) #DIV/0! 0-0

1. IEM1 : NaOH(50%), Depleted brine(Free Cl2, NaClO3)


Non-Conforming
2. IEM2 : Depleted brine(Free Cl2, NaClO3), SPB(Na2SO4)
/ Remarks
3.Utilities : Instrument air(dewpoint)

OVAromin
QC/Technical Lab Supervisor

\ova
MABUHAY VINYL CORPORATION
Quality Control Analysis - Weekly Report

Date Prepared : November 15, 2018


Period: 42851 - 42857

To : JSG
Cc : SSCP, RSCO, NAA, CPE

IEM 1 IEM 2
Average Range Average Range
Online 0.00 0-0 0.00 0-0
50% NaOH Tanks #DIV/0! 0-0 #DIV/0! 0-0
Online 0.00 0-0 0.00 0-0
32% NaOH Tanks #DIV/0! 0-0 #DIV/0! 0-0
Online #DIV/0! 0-0 0.00 0-0
%HCl Tanks #DIV/0! 0-0 #DIV/0! 0-0
Polished Brine Ca + Mg, ppm 0.00 0-0 0.00 0-0
NaCl, gpl 0.00 0-0 0.00 0-0
Depleted Brine Free Cl2 negative negative
NaClO3, gpl #DIV/0! 0-0 #DIV/0! 0-0
After Headtank After T-181
Average Range Average Range
Ca + Mg, ppb #DIV/0! 0-0 #DIV/0! 0-0
SPB Na2SO4, gpl #DIV/0! 0-0 #DIV/0! 0-0
NaClO3, gpl #DIV/0! 0-0 #DIV/0! 0-0

Average Range
Sodium % NaOCl #DIV/0! 0-0
Hypochlorite % NaOH 0.00 0-0
Instrument Air Dew Point 0.00 0-0
Compressor
Sulfuric Acid
( @ LCP) #DIV/0! 0-0

1. IEM1 : NaOH(50%), Depleted brine(Free Cl2, NaClO3)


Non-Conforming
2. IEM2 : Depleted brine(Free Cl2, NaClO3), SPB(Na2SO4)
/ Remarks
3.Utilities : Instrument air(dewpoint)

OVAromin
QC/Technical Lab Supervisor

\ova
MABUHAY VINYL CORPORATION
Quality Control Analysis - Weekly Report

Date Prepared : November 15, 2018


Period: 42837 - 42843

To : JSG
Cc : SSCP, RSCO, NAA, CPE

IEM 1 IEM 2
Average Range Average Range
Online 0.00 0-0 0.00 0-0
50% NaOH Tanks #DIV/0! 0-0 #DIV/0! 0-0
Online 0.00 0-0 0.00 0-0
32% NaOH Tanks #DIV/0! 0-0 #DIV/0! 0-0
Online #DIV/0! 0-0 0.00 0-0
%HCl Tanks #DIV/0! 0-0 #DIV/0! 0-0
Polished Brine Ca + Mg, ppm 0.00 0-0 0.00 0-0
NaCl, gpl 0.00 0-0 0.00 0-0
Depleted Brine Free Cl2 negative negative
NaClO3, gpl #DIV/0! 0-0 #DIV/0! 0-0
After Headtank After T-181
Average Range Average Range
Ca + Mg, ppb #DIV/0! 0-0 #DIV/0! 0-0
SPB Na2SO4, gpl #DIV/0! 0-0 #DIV/0! 0-0
NaClO3, gpl #DIV/0! 0-0 #DIV/0! 0-0

Average Range
Sodium % NaOCl #DIV/0! 0-0
Hypochlorite % NaOH 0.00 0-0
Instrument Air Dew Point 0.00 0-0
Compressor
Sulfuric Acid
( @ LCP) #DIV/0! 0-0

1. IEM1 : NaOH(50%), Depleted brine(Free Cl2, NaClO3)


Non-Conforming
2. IEM2 : Depleted brine(Free Cl2, NaClO3), SPB(Na2SO4)
/ Remarks
3.Utilities : Instrument air(dewpoint)

OVAromin
QC/Technical Lab Supervisor

\ova
POLLUTION CONTROL SUMMARY
29-Mar

To : EHS/ELBayor

GAS ANALYSIS - S-2 S-5 S-8


FLUE GAS pH Hg, Hg, Hg,
DATE CO CO2 O2 6 AM 7 PM ppb TDS TSS Color COD pH ppb TDS TSS Color COD pH ppb TDS TSS Color
29-Mar
30-Mar
31-Mar
1-Apr
2-Apr
3-Apr
4-Apr
Average ### ### ### ### ### ### ### ### ### ### ### ### ### ### ### ### ### ### ### ### ###
Minimum 0.0 0.0 0.0 0.00 0.00 0.000 0 0 0 0 0.00 0.000 0 0 0 0 0.00 0.000 0 0 0
Maximum 0.0 0.0 0.0 0.00 0.00 0.000 0 0 0 0 0.00 0.000 0 0 0 0 0.00 0.000 0 0 0

S-9 LAGOON JBC Evap Canal Total Canal


Hg, Hg, gpl gpl gpl
DATE pH ppb TDS TSS Color COD pH ppb TDS TSS Color COD pH NaOH pH NaOH pH NaOH S - 3 S-4 S-7
29-Mar
30-Mar
31-Mar
1-Apr
2-Apr
3-Apr
4-Apr
Average ### ### ### ### ### ### ### ### ### ### ### ### ### ### ### ### ### ### ### ### ###
Minimum 0.00 0.000 0 0 0 0 0.00 0.000 0 0 0 0 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00
Maximum 0.00 0.000 0 0 0 0 0.00 0.000 0 0 0 0 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00

OVAromin
QC/Technical Lab Supervisor

\ova
04/04/17
COD

###
0
0
POLLUTION CONTROL SUMMARY
April 5- 11, 2017

To : EHS/ELBayor

GAS ANALYSIS - S-2 S-5 S-8


FLUE GAS pH Hg, Hg, Hg,
DATE CO CO2 O2 6 AM 7 PM ppb TDS TSS Color COD pH ppb TDS TSS Color COD pH ppb TDS TSS Color COD
5-Apr 8.54 8.52 8.83 7.40 16 104
6-Apr 8.55 8.44 8.63 7.83 17 89
7-Apr 8.68 8.61 8.62 7.78 11 73
8-Apr 8.68 8.48 0.056 256 6 43 8.62 0.335 368 3 24 7.63 9 110
9-Apr
10-Apr 8.68 8.64 8.62 7.67 12 116
11-Apr 8.88 8.62 8.53 7.27 7 14 25
Average ### ### ### 8.67 8.55 0.056 256 6 43 ### 8.64 0.335 368 3 24 ### 7.60 ### ### 12 84 25
Minimum 0.0 0.0 0.0 8.54 8.44 0.056 256 6 43 0 8.53 0.335 368 3 24 0 7.27 0.000 0 7 14 25
Maximum 0.0 0.0 0.0 8.88 8.64 0.056 256 6 43 0 8.83 0.335 368 3 24 0 7.83 0.000 0 17 116 25

S-9 LAGOON JBC Evap Canal Total Canal


Hg, Hg, gpl gpl gpl
DATE pH ppb TDS TSS Color COD pH ppb TDS TSS Color COD pH NaOH pH NaOH pH NaOH S - 3 S-4 S-7
5-Apr 8.62 1 11
6-Apr 8.33 3 25
7-Apr 8.36 3 11
8-Apr 8.42 11 15 8.26 0.056 159 4 28 8.17 0.00 8.34 0.00 8.03 0.00 8.25 8.82 8.48
9-Apr
10-Apr 8.32 4 12
11-Apr 8.28 2 2 10
Average 8.39 ### ### 4 13 10 8.26 0.056 159 4 28 ### 8.17 0.00 8.34 0.00 8.03 0.00 8.25 8.82 8.48
Minimum 8.28 0.000 0 1 2 10 8.26 0.056 159 4 28 0 8.17 0.00 8.34 0.00 8.03 0.00 8.25 8.82 8.48
Maximum 8.62 0.000 0 11 25 10 8.26 0.056 159 4 28 0 8.17 0.00 8.34 0.00 8.03 0.00 8.25 8.82 8.48

OVAromin
QC/Technical Lab Supervisor

\ova
04/11/17
POLLUTION CONTROL SUMMARY
April 12-18, 2017

To : EHS/ELBayor

GAS ANALYSIS - S-2 S-5 S-8


FLUE GAS pH Hg, Hg, Hg,
DATE CO CO2 O2 6 AM 7 PM ppb TDS TSS Color COD pH ppb TDS TSS Color COD pH ppb TDS TSS Color COD
12-Apr 8.85 8.79 0.112 3800 5 35 8.70 0.224 251 2 17 7.23 7 8
13-Apr 8.70 8.65 8.63
14-Apr
15-Apr 8.58 8.63 8.67 7.50 2 14
16-Apr
17-Apr 8.78 8.71 8.65 7.49 12 16 15
18-Apr 8.60 8.57 8.62 7.57 5 15
Average ### ### ### 8.70 8.67 0.112 3800 5 35 ### 8.65 0.224 251 2 17 ### 7.45 ### ### 7 13 15
Minimum 0.0 0.0 0.0 8.58 8.57 0.112 3800 5 35 0 8.62 0.224 251 2 17 0 7.23 0.000 0 2 8 15
Maximum 0.0 0.0 0.0 8.85 8.79 0.112 3800 5 35 0 8.70 0.224 251 2 17 0 7.57 0.000 0 12 16 15

S-9 LAGOON JBC Evap Canal Total Canal


Hg, Hg, gpl gpl gpl
DATE pH ppb TDS TSS Color COD pH ppb TDS TSS Color COD pH NaOH pH NaOH pH NaOH S - 3 S-4 S-7
12-Apr 8.68 3 4 8.28 0.056 280 5 30 7.78 0.00 2.12 0.00 6.12 0.00 7.95 .8.78 9.68
13-Apr
14-Apr
15-Apr 8.77 4 12
16-Apr
17-Apr 8.44 5 6 4
18-Apr 8.26 3 15
Average 8.54 ### ### 4 9 4 8.28 0.056 280 5 30 ### 7.78 0.00 2.12 0.00 6.12 0.00 7.95 ### 9.68
Minimum 8.26 0.000 0 3 4 4 8.28 0.056 280 5 30 0 7.78 0.00 2.12 0.00 6.12 0.00 7.95 0.00 9.68
Maximum 8.77 0.000 0 5 15 4 8.28 0.056 280 5 30 0 7.78 0.00 2.12 0.00 6.12 0.00 7.95 0.00 9.68

OVAromin
QC/Technical Lab Supervisor

\ova
04/18/17
POLLUTION CONTROL SUMMARY
19-Apr

To : EHS/ELBayor

GAS ANALYSIS - S-2 S-5 S-8


FLUE GAS pH Hg, Hg, Hg,
DATE CO CO2 O2 6 AM 7 PM ppb TDS TSS Color COD pH ppb TDS TSS Color COD pH ppb TDS TSS Color COD
19-Apr
20-Apr
21-Apr
22-Apr
23-Apr
24-Apr
25-Apr
Average ### ### ### ### ### ### ### ### ### ### ### ### ### ### ### ### ### ### ### ### ### ###
Minimum 0.0 0.0 0.0 0.00 0.00 0.000 0 0 0 0 0.00 0.000 0 0 0 0 0.00 0.000 0 0 0 0
Maximum 0.0 0.0 0.0 0.00 0.00 0.000 0 0 0 0 0.00 0.000 0 0 0 0 0.00 0.000 0 0 0 0

S-9 LAGOON JBC Evap Canal Total Canal


Hg, Hg, gpl gpl gpl
DATE pH ppb TDS TSS Color COD pH ppb TDS TSS Color COD pH NaOH pH NaOH pH NaOH S - 3 S-4 S-7
19-Apr
20-Apr
21-Apr
22-Apr
23-Apr
24-Apr
25-Apr
Average ### ### ### ### ### ### ### ### ### ### ### ### ### ### ### ### ### ### ### ### ###
Minimum 0.00 0.000 0 0 0 0 0.00 0.000 0 0 0 0 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00
Maximum 0.00 0.000 0 0 0 0 0.00 0.000 0 0 0 0 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00

OVAromin
QC/Technical Lab Supervisor

\ova
04/25/17
POLLUTION CONTROL SUMMARY
26-Apr

To : EHS/ELBayor

GAS ANALYSIS - S-2 S-5 S-8


FLUE GAS pH Hg, Hg, Hg,
DATE CO CO2 O2 6 AM 7 PM ppb TDS TSS Color COD pH ppb TDS TSS Color COD pH ppb TDS TSS Color COD
26-Apr
27-Apr
28-Apr
29-Apr
30-Apr
1-May
2-May
Average ### ### ### ### ### ### ### ### ### ### ### ### ### ### ### ### ### ### ### ### ### ###
Minimum 0.0 0.0 0.0 0.00 0.00 0.000 0 0 0 0 0.00 0.000 0 0 0 0 0.00 0.000 0 0 0 0
Maximum 0.0 0.0 0.0 0.00 0.00 0.000 0 0 0 0 0.00 0.000 0 0 0 0 0.00 0.000 0 0 0 0

S-9 LAGOON JBC Evap Canal Total Canal


Hg, Hg, gpl gpl gpl
DATE pH ppb TDS TSS Color COD pH ppb TDS TSS Color COD pH NaOH pH NaOH pH NaOH S - 3 S-4 S-7
26-Apr
27-Apr
28-Apr
29-Apr
30-Apr
1-May
2-May
Average ### ### ### ### ### ### ### ### ### ### ### ### ### ### ### ### ### ### ### ### ###
Minimum 0.00 0.000 0 0 0 0 0.00 0.000 0 0 0 0 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00
Maximum 0.00 0.000 0 0 0 0 0.00 0.000 0 0 0 0 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00

OVAromin
QC/Technical Lab Supervisor

\ova
05/02/17
POLLUTION CONTROL SUMMARY
3-May

To : EHS/ELBayor

GAS ANALYSIS - S-2 S-5 S-8


FLUE GAS pH Hg, Hg, Hg,
DATE CO CO2 O2 6 AM 7 PM ppb TDS TSS Color COD pH ppb TDS TSS Color COD pH ppb TDS TSS Color COD
3-May
4-May
5-May
6-May
7-May
8-May
9-May
Average ### ### ### ### ### ### ### ### ### ### ### ### ### ### ### ### ### ### ### ### ### ###
Minimum 0.0 0.0 0.0 0.00 0.00 0.000 0 0 0 0 0.00 0.000 0 0 0 0 0.00 0.000 0 0 0 0
Maximum 0.0 0.0 0.0 0.00 0.00 0.000 0 0 0 0 0.00 0.000 0 0 0 0 0.00 0.000 0 0 0 0

S-9 LAGOON JBC Evap Canal Total Canal


Hg, Hg, gpl gpl gpl
DATE pH ppb TDS TSS Color COD pH ppb TDS TSS Color COD pH NaOH pH NaOH pH NaOH S - 3 S-4 S-7
3-May
4-May
5-May
6-May
7-May
8-May
9-May
Average ### ### ### ### ### ### ### ### ### ### ### ### ### ### ### ### ### ### ### ### ###
Minimum 0.00 0.000 0 0 0 0 0.00 0.000 0 0 0 0 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00
Maximum 0.00 0.000 0 0 0 0 0.00 0.000 0 0 0 0 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00

OVAromin
QC/Technical Lab Supervisor

\ova
05/09/17
MONTHLY REPORT
QUALITY CONTROL/TECHNICAL LAB SECTION
2017
1. WEIGHTED AVERAGE CONCENTRATION
50% 43.12 ( 0.00 - 50.56 ) 48.71 ( 48.26 - 49.35 )
CAUSTIC SODA, % NaOH IEM 1 IEM 2
32% 0.00 ( 0.00 - 0.00 ) 30.91 ( 30.41 - 31.30 )

HYDROCHLORIC ACID, % HCl IEM 1 32.71 ( 32.16 - 33.20 ) IEM 2 33.17 ( 32.54 - 33.45 )

SODIUM HYPOCHLORITE, % NaOCl 7.75 ( 7.45 - 8.70 )

LIQUID CHLORINE, % Cl2 #DIV/0! ( 0.00 - 0.00 )

2. PRODUCT DELIVERIES
Date Tank No. Vessel Destination % Purity
CAUSTIC SODA
Bulk Deliveries

HYDROCHLORIC ACID
Bulk Deliveries

SODIUM HYPOCHLORITE
Bulk Deliveries

RAW MATERIALS Date PR/PO # Remarks

3. NON-CONFORMING PRODUCTS AND MATERIALS


CAUSTIC SODA HYDROCHLORIC ACID SODIUM HYPOCHLORITE LIQUID CHLORINE RAW MATERIALS

4. POLLUTION CONTROL
pH Hg, ppb TDS, ppm Susp. Solids, mg/L Color, Pt-Co units
Source
(Range) (Range) (Range) (Range) (Range) COD mg/L
3.47 0.075 1420 5 39
S-2 #DIV/0!
( 0.00 - 9.23 ) ( 0.056 - 0.112 ) ( 204 - 3800 ) ( 4-6 )( 35 - 43 )
8.68 0.242 294 2 19
S-5 #DIV/0!
( 8.53 - 9.20 ) ( 0.168 - 0.335 ) ( 251 - 368 )( 2-3 )( 17 - 24 )
7.41 #DIV/0! #DIV/0! 13 68 20
S-8
( 6.52 - 7.97 ) ( 0.000 - 0.000 ) ( 0 -0 ) ( 2 - 38 ) ( 8 - 152 ) ( 15 - 25 )
8.39 #DIV/0! #DIV/0! 3 10 7
S-9
( 8.21 - 8.77 ) ( 0.000 - 0.000 ) ( 0 -0 ) ( 1 - 11 ) ( 0 - 25 ) ( 4 - 10 )
8.27 0.056 220 5 29
Lagoon #DIV/0!
( 8.26 - 8.28 ) ( 0.056 - 0.056 ) ( 159 - 280 )( 4-5 )( 28 - 30 )
JBC Evap Canal Total Canal S-3 S-4 S-7
pH 8.06 0.45 0.53 7.94 0.43 0.62
(Range) ( 7.78 - 8.23 )( 0.00 - 8.34 ) ( 0.00 - 8.07 ) ( 7.63 - 8.25 ) ( 0.00 - 8.85 ) ( 0.00 - 9.68 )
NaOH, gpl 0.00 0.00 0.00
(Range) ( 0.00 - 0.00 )( 0.00 - 0.00 ) ( 0.00 - 0.00 ) NA NA NA
% CO % CO2 % O2
Flue Gas
#DIV/0! 0.00 0.00

5. OTHERS
CELL GAS, %
Boiler Water Instrument Air LCP Feed Cl2 IEM 1 IEM 2
ppm SiO2 Dewpoint, °C % Cl2 % H2 Cl2 H2 CO2 + O2 Cl2 H2 CO2 + O2
1.8 Line A ### 0.0 0.0 #DIV/0! 0.0 0.0
130 ( 0.0 - 8.6 ) ### 0.0 Line B 0.0 0.0 0.0 0.0 0.0 0.0
Na2SO4, gpl ave. NaClO3, gpl ave. Ca + Mg, ppb ave. pH
SPB 1.36 ( 0.00 - 2.96 ) 2.07 ( 0.00 - 5.96 ) 17 ( 0 - 68 ) NA
IEM-1
Depleted Brine NA 3.74 ( 0.00 - 11.57 ) NA NA
SPB 1.85 ( 0.00 - 5.48 ) 8.85 ( 0.00 - 25.76 ) 4 ( 0 - 20 ) NA
IEM-2
Depleted Brine NA 13.02 ( 0.00 - 37.51 ) NA 0.76 ( 0.00 - 2.89

6. REMARKS

OV AROMIN
QC/Tech Lab Supervisor
ova 00/00/17
ity

ALS
)
WEIGHTED AVERAGE REPORT
2017

CAUSTIC SODA, HYDROCHLORIC ACID, SODIUM HYPOCHLORITE

To : IEM-1/IEM-2/Accounting/Distribution Date : /01/17


From : Quality Control Ref. : QC-SR-17-

PRODUCT SOURCE Wted. Average Conc. Specific Gravity


IEM-1 43.12
1.0 CAUSTIC SODA - 50%
IEM-2 48.71

IEM-1 0.00
1.0 CAUSTIC SODA - 32%
IEM-2 30.91

IEM-1 32.71
1.0 HYDROCHLORIC ACID
IEM-2 33.17

1.0 SODIUM HYPOCHLORITE IEM-2 7.75 0.114

OV AROMIN
QC/Tech Lab Supervisor
qc.00.01.17

WEIGHTED AVERAGE REPORT


2017

CAUSTIC SODA, HYDROCHLORIC ACID, SODIUM HYPOCHLORITE

To : IEM-1/IEM-2/Accounting/Distribution Date : /01/17


From : Quality Control Ref. : QC-SR-17-

PRODUCT SOURCE Wted. Average Conc. Specific Gravity


IEM-1 43.12 0.000
1.0 CAUSTIC SODA - 50%
IEM-2 48.71 0.000

IEM-1 0.00 0.000


1.0 CAUSTIC SODA - 32%
IEM-2 30.91 0.000

IEM-1 32.71 0.000


1.0 HYDROCHLORIC ACID
IEM-2 33.17 0.000

1.0 SODIUM HYPOCHLORITE IEM-2 7.75 0.114

OV AROMIN
QC/Tech Lab Supervisor
qc.00.01.17
4.1 Caustic Soda

Weighted Average Concentration transferred to Marketing, %


50% 43.12 48.71
IEM 1 IEM 2
32% 0.00 30.91
Bulk Shipment
Delivery Date Tank No. Vessel Concentration, %

12/30/99 0 0 0.00
12/30/99 0 0 0.00
12/30/99 0 0 0.00
12/30/99 0 0 0.00
12/30/99 0 0 0.00
Non-conforming NaOH:

4.2 Hydrochloric Acid

Weighted Average Concentration transferred to Marketing, %


IEM 1 32.71 IEM 2 33.17
Bulk Shipment
Delivery Date Tank No. Vessel Concentration, %

12/30/99 0 0 0.00
12/30/99 0 0 0.00
12/30/99 0 0 0.00
12/30/99 0 0 0.00
12/30/99 0 0 0.00
12/30/99 0 0 0.00
Non-conforming HCl:

4.3 Sodium Hypochlorite

Weighted Average Concentration transferred to Marketing, % : 7.75


Bulk Shipment
Delivery Date Tank No. Vessel Concentration, %

12/30/99 0 0 0.00
12/30/99 0 0 0.00
12/30/99 0 0 0.00
12/30/99 0 0 0.00
Non-conforming NaOCl:

4.4 Liquid Chlorine

Average Purity, % : #DIV/0!


No. of Cylinders Rejected :

4.5 Raw Materials

Date Raw Material PO # Remarks


12/30/1899 0 0.00 0.00
12/30/1899 0 0.00 0.00
12/30/1899 0 0.00 0.00
12/30/1899 0 0.00 0.00
12/30/1899 0 0.00 0.00
12/30/1899 0 0.00 0.00
Non-conforming Material:
Destination

0
0
0
0
0

Destination

0
0
0
0
0
0

Destination

0.00
0.00
0.00
0.00