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Equipments design
CHAPTER FOUR
Equipments design
The contents:
(4-1)Condenser design
(4-1-1) Introduction
(4-2)Reactor design
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4 Chapter
Equipments design
(4-1-1) Introduction :
When a saturated vapor is brought into contact with a cool surface, heat is transferred
from the vapor to the surface and a film of condensate is produced. the method first put
forward by NUSSELT and later modified by subsequent workers is followed. In Nusselt's
work it is assumed that the temperature of the film at the cool surface is equal to that of the
surface, arid at the other side was at the temperature of the vapor. In practice, there must
be some small difference in temperature between the vapor and the film, although this may
generally be neglected except where non-condensable gas is present in the vapor. (ref.
vol.1 p471)
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Equipments design
T1(methanol in shell)
t1 (water in pipe) t2
T2
inlet temperature (c ͦ) 67 25
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Equipments design
= 11.97 cͦ
(67−37)− ( 28.2−25)
= (67−37
𝑙𝑛( )
28.2−25
Then Ft = 0.94
Then the ∆Tm =Ft * ∆TLm = 0.94 * 11.97 = 11.25 c ͦ
(4-1-5-4)The area of condenser :
First we assume Overall all coefficient from table 12-1 vol.6
U = 740 w/m².c ͦ
Q =U A ∆Tm A = Q/U ∆Tm
8.916 ∗10ᵌ
A = 750 ∗ 11.25 = 1.312 m²
The standard dimension for steel tube we obtain it from table in vol.6 12-3
Outside diameter = 20 mm
Inside diameter = 16.8 mm
Length of tube = 4.88 m
Area of one tube = 3.14 * do * L
= 3.14 * 20*10^-3 *4.88 = 0.303 m²
(4-1-5-5)Number of tube :
Nt = trial Area / area at one tube
= 1.312 / 0.303 = 4.3 ≅ 5
Will used square pitch tube bundle diameter that mean
Pt = 1.25 * do
= 1.25 * 20 = 25 mm
Tube bundle diameter :
Db= do ( Nt/k) ^1/n1
The taken of k1 & n1 its depend on pitch if triangular or square and pass number .
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4 Chapter
Equipments design
where
𝑤
kL = condensate thermal conductivity , 𝑚.𝑐
𝑘𝑔
𝜌𝑙 = condensate density , 𝑚³
𝑘𝑔
𝜌𝑣 = vapor density , 𝑚³
𝑁.𝑆
𝜇𝑙 = condensate viscosity , 𝑚²
𝑚
g = gravitational acceleration , 9.81 𝑠𝑒𝑐²
= 1289.116 w/m².c
(4-1-5-7)Tube side coefficient
Tube cross – section area = 3.14 * d²i = 3.14 * ( 16.8) ²
At = 2.216 *10^ -4 m²
Tube per pass = 5/2
Total flow area = 2.5 *2.216 *10^-4
Total flow area = 5.54 *10^4 m²
Density of water at 31 c ͦ = 993 kg/mᵌ
Mass velocity per area = m/A
= 0.177/5.54*10^-4 =319.49 kg /m² .sec
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4 Chapter
Equipments design
where
hi = inside coefficient for water , w/m².c
t = water mean temperature , c
Ut = water velocity , m/s
di = inside diameter
4200(1.35+0.02∗(31)∗(0.3217)^0.8
hi = = 7562.49 w/m².c
(16.8∗10−3 )^0.2
where
𝑈 = the overall coefficient , w/m².c
ℎ𝑜 = outside fluid film coefficient , w/m².c
ℎ𝑖 = inside fluid film diameter , w/m².c
ℎ𝑜𝑑 = outside dirt coefficient , w/m².c
ℎ𝑖𝑑 = inside dirt coefficient , w/m².c
𝑘𝑤 = thermal conductivity of the tube wall material , w/m.c
𝑑𝑜 = tube outside diameter , m
𝑑𝑖 = tube inside diameter , m
20
1 1 1 20 𝑙𝑛( ) 20 1 20 1
16.8
= 1289.116 + 6000 + + ∗ 6000 + 16.8 ∗ 7562.5=
𝑈 2∗45 16.8
Where
Np= number of passes
Μw =viscosity of wall
Ρ =density of water
Ut= velocity of water in tube
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4 Chapter
Equipments design
𝑢𝑡 𝜌 𝑑𝑖 0.3217∗993∗16.8∗10^−3
Re = ( )= =6702.5 = 6.702 * 10^3
𝜇 0.8007∗10^−3
where
𝑁
∆Ps = shell side pressure drop,
𝑚²
(𝑃𝑡−𝑑𝑜)𝐷𝑠∗𝐿𝐵 (25−20)∗142.7∗142.7∗10^−6
As = = =4.07*10^-3
𝑃𝑡 25
𝑊𝑠
Gs = =22.768 kg/sec.m²
𝐴𝑠
1.27
De= 𝑑𝑜 (𝑃𝑡 2 − 0.785 ∗ 𝑑 2 𝑜)
1.27
De = ( 25² - 0.785 *20²) = 19.75 mm
20
𝐺𝑠∗𝑑𝑒 22.768∗19.75∗10^−3
Re = = =1126.98
𝜇𝑤 0.399∗10^−3
𝐺𝑠 22.768
Us = = =0.029 m/s
𝜌 764
= 0.03175 kpa
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Equipments design
Number of passes 2
Number of tubes 5
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Equipments design
(4-2)Reactor Design:
The reactor: is the heart of chemical process. It is the only place in the process where
raw materials are converted into products, and reactor design is the vital steps in the
overall design of the process. So the knowledge of chemical engineer about the nature and
mechanism of reaction is distinguished him than other in the plant.
S: 103 ,
60c
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Equipments design
(4-2-3)The calculation :
(4-2-3-1)Reactor volume:
Ʈ= 4 hr (Ref.12 )
where
𝑉
Ʈ = 𝑣˳
V:Reactor volume
V= v˳ * Ʈ = 0.9805 * 4 = 3.992 m³
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Equipments design
(4-2-3-3)Agitator dimensions :
b
D
3
d
D
3
h
D H
5
a r
D
4 a
r
D h
10
b
(4-2-3-4)Thickness of shell :
𝑝𝑖∗𝑑𝑖
e = (2𝑓 –𝑝𝑖 ) (volume 6)
where
e :minimum thickness required (mm)
Pi :internal pressure (n/𝑚𝑚2 )
f :design stress (n/𝑚𝑚2 ) from plant design standard
di: internal diameter (mm)
design pressure =10% excess of operating pressure
We add 2mm corrosion allowance
Design pressure = 0.1013*1.1 =0.11143 n/m𝑚2
From table (13-2 ( Ref.6)
Design stress at 60 c and selecting stainless steel = 160 n/mm²
0.11143 𝑥 1586
e = 2 𝑥 (160−0.11143) = 0.58 𝑚𝑚
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Equipments design
Parameter value
Residence time 4 hr
Area of reactor 2 m²
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