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ISSUES TO ADDRESS...
• How do flaws in a material initiate failure?
• How is fracture resistance quantified; how do different
material classes compare?
• How do we estimate the stress to fracture?
• Ductile failure:
--one piece
--large deformation
• Brittle failure:
--many pieces
--small deformation
3
DUCTILE FRACTURE
• Resulting 50μm
50 μm
fracture
surfaces
(steel)
100 μm
particles From V.J. Colangelo and F.A. Heiser, Fracture surface of tire cord wire
serve as void Analysis of Metallurgical Failures loaded in tension. Courtesy of F.
(2nd ed.), Fig. 11.28, p. 294, John Roehrig, CC Technologies,
nucleation Wiley and Sons, Inc., 1987. (Orig. Dublin, OH.
sites. source: P. Thornton, J. Mater. Sci.,
Vol. 6, 1971, pp. 347-56.) 4
BRITTLE FRACTURE SURFACES
• Intergranular • Intragranular
(between grains) 304 S. Steel (within grains)
(metal) 316 S. Steel
Reprinted w/permission from
"Metals Handbook", 9th ed, Fig. (metal)
633, p. 650. Copyright 1985, ASM Reprinted w/ permission from
International, Materials Park, OH. "Metals Handbook", 9th ed, Fig.
(Micrograph by J.R. Keiser and A.R. 650, p. 357. Copyright 1985, ASM
Olsen, Oak Ridge National Lab.) International, Materials Park, OH.
(Micrograph by D.R. Diercks,
Argonne National Lab.)
160μm
4 mm
Polypropylene Al Oxide
(polymer) (ceramic)
Reprinted w/ permission from Reprinted w/ permission from
R.W. Hertzberg, "Defor-mation "Failure Analysis of Brittle
and Fracture Mechanics of Materials", p. 78. Copyright 1990,
Engineering Materials", (4th ed.) The American Ceramic Society,
Fig. 7.35(d), p. 303, John Wiley Westerville, OH. (Micrograph by
and Sons, Inc., 1996. R.M. Gruver and H. Kirchner.)
3μm
1 mm
(Orig. source: K. Friedrick, Fracture 1977, 5
Vol. 3, ICF4, Waterloo, CA, 1977, p. 1119.)
BRITTLE FAILURE
Examples: Refractory oxides (ceramics), intermetallics, BCC metals at low
temperature (below about ¼ of the melting point).
• Very little plastic flow prior to failure;
• The two sides of the fracture surface fit together well after
failure.
• The fracture surface appears faceted – you distinguish
individual grains and atomic planes.
• In some materials, fracture occurs along certain
crystallographic planes. In others, fracture occurs along grain
boundaries
DUCTILE FAILURE
Examples: FCC metals at all temperatures; BCC metals at high
temperatures; polymers at high temperature.
• Extensive plastic flow occurs in the material prior to fracture
• There is usually evidence of considerable necking in the
specimen
• Fracture surfaces don’t fit together.
• The fracture surface has a dimpled appearance – you can see
little holes, often with second phase particles inside them.
Ductile vs Brittle Fracture
A designer point of view
• Ductile: Basically we design against yielding.
– “Internal defects” that reduce yield strength can be taken into
account by the introduction of a safety factor
– Reduction of strength due to internal defects is not “excessive”,
unless the defects are of “large” dimensions compared to the
cross section
– Statistical variation of properties of parts from a well controlled
process is limited.
– Visible deformation before failure is an effective warning
mechanism
• Brittle:
– Statistical variation of properties of parts may be significant.
– Reduction of strength due to internal defects is significant,
defects need to be taken into account and directly or indirectly
“measured”
– The “sudden” nature of the event makes this type of failure very
dangerous
EARLY STUDIES IN BRITTLE FRACTURE
E By considering the
F
maximum force per bond
Fmax we calculate that the ideal
strength is about E/10
a a
Griffith (1920)
IN REALITY WE
ARE FAR BELOW
FLAWS ARE STRESS
CONCENTRATORS!
• Elliptical hole in • Maximum stress at the tip
a plate:
σo ⎛ a⎞
σ max = σ ⎜1 + 2 ⎟
⎝ b⎠
σ a = b ⇒ σ max = 3σ
a = 10b ⇒ σ max = 21σ
2a
a
ρ = b /a ⇔ a/b =
2
ρ
⎛ a⎞ a
σ max = σ ⎜⎜1 + 2 ⎟ ≈ 2σ
⎟ ( a >> ρ )
⎝ ρ ⎠ ρ
For sharp cracks
stress → ∞ 7
WHEN DOES A CRACK PROPAGATE?
2a
2a 2a
2a
πσ 2 a 2t
UA =UB + − + 4atγ S
E
aCR a
dU A 2πσ 2 aCR t πσ 2 aCR
=0⇒− + 4tγ S = 0 ⇒ = 2γ S
da E E
2γ S E
σ FAILURE =
πa
σ πa = 2γ S E
Stress
Intensity Fracture
Factor Toughness
K KC
K = σ πa K = 1.1σ πa
10
FRACTURE TOUGHNESS metals
Kc
increasing
Graphite/
Metals/ Composites/
Alloys
Ceramics/ Polymers
fibers comp
Semicond Kc
100
C-C(|| fibers)1
70 Steels cer≈ poly
60 Ti alloys
Kc Kc
50
40
Al alloys
30 Mg alloys Based on data in Table B5,
KIc(MPa · m0.5)
Callister 6e.
20 Composite reinforcement geometry
Al/Al oxide(sf) 2
is: f = fibers; sf = short fibers; w =
Y 2O 3/ZrO2(p)4 whiskers; p = particles. Addition
10 C/C( fibers)1 data as noted (vol. fraction of
Al oxid/SiC(w)3 reinforcement):
Diamond Si nitr/SiC(w)5
7 Al oxid/ZrO2(p)4
1. (55vol%) ASM Handbook, Vol. 21, ASM
6 Int., Materials Park, OH (2001) p. 606.
Si carbide Glass/SiC(w)6 2. (55 vol%) Courtesy J. Cornie, MMC, Inc.,
5 Al oxide PET
Si nitride Waltham, MA.
4 3. (30 vol%) P.F. Becher et al., Fracture
PP
Mechanics of Ceramics, Vol. 7, Plenum
3 PVC Press (1986). pp. 61-73.
4. Courtesy CoorsTek, Golden, CO.
2 PC 5. (30 vol%) S.T. Buljan et al., "Development
of Ceramic Matrix Composites for
Application in Technology for Advanced
Engines Program", ORNL/Sub/85-22011/2,
1 ORNL, 1992.
<100>
Si crystal PS Glass6 6. (20vol%) F.D. Gace et al., Ceram. Eng.
<111> Sci. Proc., Vol. 7 (1986) pp. 978-82.
0.7 Glass-soda
0.6 Polyester
Concrete 11
0.5
Geometry factor Y
K = Y σ πa
DESIGN AGAINST CRACK
GROWTH
• Crack growth condition: K = Kc
Yσ πa
• Largest, most stressed cracks grow first!
--Result 1: Max flaw size --Result 2: Design stress
dictates design stress. dictates max. flaw size.
Kc 1 ⎛ Kc ⎞ 2
σdesign < a max < ⎜ ⎜ ⎟
Y πa max π ⎝ Yσdesign ⎟⎠
amax
σ
fracture fracture
no no
fracture amax fracture σ
12
How do we know what is the crack size?
By inspection
- magnetic particles
- liquid dye penetrant
- ultrasound
- electromagnetic (eddy current)
- X-ray
We focus on KIC
because it is a
true material
property
(i.e., it does not
depend on
geometry of the
specimen)
FRACTURE TOUGHNESS
TESTING
ASTM 399
FRACTURE TOUGHNESS TESTING
P95% /PQ<1.1
maxslope
BUT …
Validity
• Sharp crack – fatigue generated
• Plane strain?
2.5(K/σY)2 << thickness, crack size, (specimen
width – crack size) and half height?
2 E (γ S + γ plasticity )
σ critical =
πa
a a+da
What about fracture toughness of
ductile materials?
x
Small scale yielding
Plane Strain
2
1 ⎛K ⎞
rY = ⎜⎜ ⎟⎟
6π ⎝σY ⎠
Plain Stress
Plastically
yielded area
bad around crack tip OK
Summary of conditions
• Sharp crack
• Pmax/PQ<1.1
• Plane strain
• Small scale yielding