Leaching Gold from concentrates using Chlorine Based Halides this is a Slower leach and you need to maintain it for several hours to even a d ay. The principle is not to let the solution go acid or over salt on you and keep the h alides available to extract the Gold.
Leaching Gold from concentrates using Chlorine Based Halides this is a Slower leach and you need to maintain it for several hours to even a d ay. The principle is not to let the solution go acid or over salt on you and keep the h alides available to extract the Gold.
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Leaching Gold from concentrates using Chlorine Based Halides this is a Slower leach and you need to maintain it for several hours to even a d ay. The principle is not to let the solution go acid or over salt on you and keep the h alides available to extract the Gold.
Copyright:
Attribution Non-Commercial (BY-NC)
Available Formats
Download as TXT, PDF, TXT or read online from Scribd
Leaching Gold from Concentrates using Chlorine Based Halides
This is a basic tutorial, we accept absolutely no responsiblity for injury, acci
dent or death caused by this basic tutorial instruction. It is reccommended that you as an individual researc h the process further to get a clearer picture of how it should be done. How to Leach Gold using Chlorine Halides This is a Slower Leach and you need to maintain it for several hours to even a d ay. NOT USING ACIDS LIKE NITRIC AND SULFURIC ______________________________________ Leaching Chemicals Red Devil Lye= Sodium hydroxide "caustic soda" Pool Chlorine= Calcium hypochlorite ______________________________________ How to mix Ad Pool chlorine to water appx 1/2 cup per/2 gallons. Mix a Lye solution, add just enough to allow pool chlorine to dissolve in the wa ter. Stir carefully, using a plastic stir rod or paddle Use rubber gloves,eye protection and respirator even an apron thats chemical pro of to caustic soda. ______________________________________ After mixing together to form leaching solution "NOW Sodium Hypochlorite" measur e w/Ph meter for a 8 - 8.5Ph factor. If solution starts to run away "boils chlorine off strong irritating chlorine od or" add very small amount of Lye solution to bring it back into control by bringing the solution out of the a cid composition. If the leach solution seems to be slowing down or goes dead by appearance add a touch of muriatic acid. If the Ph goes to low mix more pool chlorine and lye and add to boost Ph back to 8 - 8.5Ph. The whole idea is to keep that Ph factor in the required zone of 8 - 8.5 on your Ph meter. The principle is not let the solution go acid or over salt on you and keep the h alides available to extract the Gold. _________________________________________ Neutralizer= Sodium thiosulfate "chlorine neutralizer 4oz powder to 1 gallon of H20". This is the stuff you use to neutralizes the chlorine in tropical fish tanks. Use to neutralize the used concentrates after leaching. makes it safe to dump af ter thorough rinse. Rinse at least 2 times, 3 is better then discard. __________________________________________ 1, After leaching, in the clear solution is where the Gold will be, it's invisib le. 2, So to precipitate the Gold Out use zinc powder even a peice of zinc will poss ibly work. 3, Add zinc powder into solution little at a time, you'll see dark black or brow n material start to collect or appear in bottom of solution tank, that is the Gold. 4, Once the black stops falling and the solution stops reacting. 5, Drain the solution off into a separate tank, leaving the brown/black mud behi nd. 6, Now neutralize the mud w/sodium thiosulfate and water. 7, Stir it all and allow it to settle out once again. 8, Now drain off the neutralizing solution and discard it, its safe and neutral to dump. 9, Now take the mud and place it into a glass container that'll work on a hot pl ate without shattering "old coffee pot". 10,Allow the remainder of the liquid in the coffee pot to evaporate off "do not boil it". 11, You can re admit the drained off leaching solution back into the tank for an other run. Check it and boost and balance it if necessary. Its actually so inexpensive to make, you can also neutralize the old solution and discard it too and make up a new batch for the next run. Once dry you can take the dried mud "almost pure Gold .995+" to the furnace to s melt and melt. Remember, YOU ARE USING VERY VOLATILE CHEMICAL COMBINATIONS... Extreme care and caution must be observed. Do this OUTDOORS w/ventilation fans blowers what ever. Stand upwind of draft... This method can be used on any amounts of concentrates you need to Leach from a pound to a mountain of heap leach covering a football field. Its what you can handle safely and feel comfortable w ith. I would reccommend that you use small batches first to practice. Then move up to larger ones. The chemicals you will need are: 1, Sodium Thiosulfate 2, Calcium Hypochlorite 3, Sodium Hydroxide [caustic soda "lye"] 4, Muratic acid 5, Critic acid Buy them in the quantites you want for your process. "SPECIAL NOTE" Remember to read the tutorial on Blacksands and removing the sulfides and iron u sing acedic or citric acid and roasting before you leach your cons. Because excessive sulfid es and iron will, if not totally kill your leaching process and gum it all up. Also, do not use sodium bi carbonate "baking soda" in this process. it'll turn the entire process into a foaming fizzy gooey gloppy mess. Hey grunk, you know about that... :P Additional Note: You can purchase all of the Chemicals you may need from the Che mistry Store in Pompano beach, Fl. Their url is: http://www.chemistrystore.com In order to purchase the Sodium Hydroxide [caustic soda "lye"] you will need to print their Hazmat release form and fax it in to them, before they will ship the product. The calcium Hypochlorite is swimming pool chlorine, buy it anywhere at a pool su pplier. For the basic Prospector w/concentrates, this is the easiest and least expensive method of extracting that micro Gold.
Nitro Compounds: Proceedings of the International Symposium Held at the Institute of Organic Synthesis, Polish Academy of Sciences, Warszawa, 18-20 September 1963