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SOLID STATE

BACKSCATTERED
ELECTRON DETECTOR

• EXCELLENT ATOMIC NUMBER


RESOLUTION 0.1Z at Z = 30

• HIGH BANDWIDTH-TV RATE


OPERATION

• LOW NOISE IN SLOW SCAN


MODE
24mm Silicon Detector
• 4 QUADRANT DETECTOR FOR
COMPOSITION OR TOPOGRAHIC
STUDIES.

• RANGE OF DETECTORS FOR,


0.4KeV, 1keV, 4keV, UHV, & STEM
APPLICATIONS.

BACKSCATTERED ELECTRON DETECTOR


The Backscattered Electron Detector
uses a large area silicon diode specially
fabricated for electron detection. Its
development over the years has led to a
compact highly sensitive device. The
four quadrant annular construction Corrosion of Steel.
achieves almost perfect symmetry Composition Image 15kv, x60
virtually eliminating topographic
information and producing a pure
compositional signal.

The ability to select quadrants allows it


to be used for topographical studies with
the compositional information
suppressed.

State of the art electronic amplifiers and


processing use surface mount
technology in critical areas permitting
the highest possible gain and lowest Corrosion of Steel.
possible noise level. Topographic Image 15kv, x60

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The 4 Quadrant system offers the Above 10keV Standard, Low Voltage
greatest flexibility in imaging with and Ultra Low Voltage devices exhibit
backscattered electrons, and is often similar characteristics but the Low and
specified as standard by SEM Ultra Low Voltage detectors are ideal
manufacturers. for the more sensitive biological and
semiconductor specimens that could be
THE SOLID STATE DETECTOR damaged by high acceleration voltages.

The K.E.Developments Backscattered The Low and Ultra Low Voltage


Detector may be used routinely with detectors may however be affected by
most types of SEM specimen. It gives Cathodoluminescence signals or other
excellent atomic number contrast and is stray light, particularly infra red which is
seldom affected by specimen charging sometimes used for the stage position
and edge effects normally associated sensors.
with secondary electron images.

Due to its symmetrical design


topographic information is virtually
eliminated but by quadrant selection the
topographic information may be
enhanced and the atomic number
contrast completely suppressed.

DETECTOR TYPES

Detector elements are available in a


selection of segmentations, sizes and
sensitivities suitable for most
applications. Polishing Block. Grit Embedded
Rubber. Composition Image.
The Standard detector is used for all Uncoated Specimen
general applications. It has a threshold
sensitivity of around 4KeV. This is the
ideal detector for most systems and is
especially recommended for SEMs with
WDX and EDX capabilities where
general applications require high keV’s
and large probe currents.

The Low Voltage detector was


developed for operation over a wide
range of kV’s and is sensitive to signals
as low as 1keV.

The Ultra Low Voltage detector was


developed with low vacuum operation in
mind, and operates over a wide range of Topographic Image of Above
keVs from as low as 0.4keV.

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DETECTOR SIZES SPECIAL DETECTORS

The detector elements are available in a Whilst it is feasible to undertake


variety of internal diameters, external CATHODOLUMINESCENCE detection
diameters and segmentations to suit the utilizing a light sensitive silicon detector,
application. Standard sizes are 18mm a semiconductor CL detector will never
and 24mm. be as sensitive as a dedicated
photomultiplier based system. For
The 18mm element is ideal for general regular CL applications at lower beam
applications and is most sensitive at currents the K.E.Developments
working distances around 8mm. It is CENTAURUS detector offers far greater
slightly less sensitive than the 24mm performance and flexibility.
device due to its smaller area.
A UHV version of the standard detector
The 24mm are best for longer working is fully UHV compatible and allows the
distances and gives peak output at a detector to be baked at up to 200°C
working distance of about 12mm. without sustaining permanent damage.

Other sizes of detectors in the range The STEM detector uses a small
6mm-35mm are available for specific rectangular silicon device, which is built
applications. In particular a 10mm into a standard 12.7mm specimen stub.
element can be used for very short The 3.05mm grid is fitted above the
working distances or for applications detector and held securely in position
where space is restricted due to the size during analysis. It may be used for both
of the stage. bright field and dark field studies. When
the STEM detector is used a system
with a retractable arm an adaptor
assembly be required.

18mm Detector
in a typical holder
STEM Detector

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seal it can be prone to slight vacuum
leakage so is less suitable for high
vacuum and cold field emission SEM’s.

The Swing Arm is suitable for most


large SEM chambers and can be swung
out of the way by means of an external
control knob.

A Screw Retractable system can also


be supplied for virtually any chamber
and offers most of the advantages of the
Push Pull system and can be fitted to
STEM Image of Microfossil 25kV,X4000 high vacuum and field emission SEMs.
With the recommended addition of
RETRACTION SYSTEMS bellows sealing

Retraction systems are provided to hold


the detector element and to accurately
position it just underneath the final lens.

Retraction enables the element to be


moved away from the final lens when
not in use and helps minimize the risk of
accidental damage.

The system also allows the microscope


to be used at very short working
distances and with fine mechanical
adjustment for high resolution
applications.
Swing Arm
As a low cost solution the detector
element may be permanently attached
to the final lens cap. This type of Fixed
system whilst allowing a very short
working distance leaves the element
permanently exposed to damage and
may restrict access for other detection
systems unless a less than optimal
small element detector is used.

The Push Pull Arm is the most versatile


retraction system and can be supplied
for virtually any chamber. Because it
takes up less space internally it is
particularly suitable for the smaller
chambers. As it uses a sliding vacuum Push-Pull Arm

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The chance of accidental damage to the SPECIFICATIONS
detector element can be minimized by
the use of a K.E.Developments Infrared DETECTOR ASSEMBLY
Chamberscope, which gives a
continuous overall view of the inside of Annular 4 quadrant N-type diffused
the specimen chamber. junction. Atomic Number resolution
better than 0.1Z when Z = 30.

DETECTOR TYPES

Standard. General purpose applications


Threshold sensitivity approx. 4keV.
Good immunity to stray light.

Low Voltage. Similar to Standard


detector but with increased sensitivity
below 10keV. Threshold sensitivity
1keV. Poor immunity to straylight.

Ultra Low Voltage. Similar to Low


Voltage detector but with Threshold
sensitivity below 400eV. Poor immunity
Brass showing ά and β Phases. Mean to stray light.
Atomic Differences 0.1Z.

STEM. Small single element device


accepts standard 3.05mm TEM grids.

UHV. High temperature version of the


standard detector made with UHV
compatible materials. Can be baked up
to 200°c.

Various other detectors in the


mechanical range 6mm to 35mm and
with a variety of segmentations can be
supplied to special order.

Multiphase Metal Alloy

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SPECIFICATIONS

PREAMPLIFIER

High sensitivity, low noise design using


surface mount components. Size;
144mm(L) x 92mm(H) x 25mm(W).

CONTROL UNIT
Video output level configured for SEM
Quadrant and gain switching using push
button controls with Led indication.
Four gain ranges with noise filtering.
STEM Thin section of kidney
Bandwidth Gain 1 & 2, 4MHz
Gain 3, 200kHz
Gain 4, 50kHz
Free standing case or compatible
modules for some SEMs.

Field Emission correction for some cold


FE SEMs
Auto Bandwidth control for some digital
SEMs

Power Supply 100, 120, 220 & 230V


ac., 50/60Hz.

WARRANTY. Two years from date of


Sandstone Cathodoluminescence taken
purchase.
with Centaurus CL detector

ORDERING DETAILS
When ordering please state make and most cost effective solution for the
model of SEM and preferred port. application. If a particular type is preferred
The Backscattered Detector normally please specify.
fits into a specific port. Where this is Where a retractable arm is not requested
already in use it may be possible to offer a fixed lens mounting system and a
an alternative position. Please inquire separate vacuum feedthrough will be
for details. necessary.
Please also state detector type and size K.E.Developments are continuously
i.e.”Low Voltage 18mm”. improving its products. The product
Where a retractable arm is supplied may therefore differ in detail to
required we will normally supply the that described in this brochure.

K.E.DEVELOPMENTS LIMITED
The Mount, Toft, Cambridge, CB3 7RL, England
Telephone +44 1223 263532 Fax +44 1223 263948
Web Site. WWW.KEDEV.CO.UK Email. sem@kedev.com

BSD Issue 4 dated 05/07/04

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