12 UNITS

NORMAG - LABORATORY GLASSWARE NORMAG - LABORATORY GLASSWARE

L 312 e.1

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FALLING FILM PHOTOREACTOR WITH FORCED LIQUID CIRCULATION
GENERAL
The synthesis via the photo chemistry is a commonly applied method. Organic synthesises often succeed only due to the radiation with UV-light or will be speeded up. Photochemical reactions are often run at room temperature and so they are gentler than other thermal processes. Photoreactors have a wide range of application, e.g. in synthesis, analysis and waste water treatment.

Construction of the Falling Film Photoreactor

The radiation vessel is the main component of the reactor. It has a capacity of approx. 200 ml and distinguish by the silver coated high vacuum jacket with side strips and tempering jacket. Cooling tube and immersion tube, both made of quartz glass, are located in the radiation vessel. The circulation is effected by the forced circulation pump "System Normag", which is controlled by a control unit. Delivery consists of four supply vessels with volumes of 100, 250, 500 and 1000 ml, as well as a low temperature thermometer for low temperature ranges between -30 C and + 100 C and small pieces. Catalogue No. SAA 09356

Pict. Falling Film Photoreactor with forced liquid circulation

The Normag Falling Film Photoreactor offers the following advantages:

m m m m m m

An effective circulation of the liquid to be radiated inside the reactor. Due to the falling film principle, an intensive radiation is reached. Only a small liquid volume is necessary. Operations in low temperature range ensure more application facilities. Used materials Borosilicate glass 3.3, quartz glass and plastic parts of PTFE. This photoreactor is suitable for mercury medium pressure lamps TQ 718 and TQ 150 and the mercury low pressure lamp TNN 15/32.

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Legend: 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 Radiation vessel Cooling tube, Quartz glass UV-lamp TQ 718 UV-lamp TNN 15/32 Power unit for UV-lamp TQ 718 Power unit for UV-lamp TNN 15/32 Gassing frit Thermometer Cooling water connections GL 14 Forced circulation pump Pump impeller Glass stopcock for sampling Spindle valve for drain off Motor Speed controller Ventilating and feeding connection Throttle valve Supply vessel for reaction solution Equalising line for small volumes

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Accessory for the Falling Film Photoreactor

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Mercury medium pressure lamp TQ 718 Capacity 700 W Lamp voltage 220 V Catalogue No. SAA 09380
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Mercury low pressure lamp TNN 15/32 Capacity 15 W, Lamp voltage 55 V Catalogue No. SAA 09370 Power unit fitting for TNN 15/32, Connecting voltage 230 V, 50 Hz Catalogue No. SAA 09371

Mercury medium pressure lamp TQ 718 Z1 With additional radiation intensity 400 - 450 nm Catalogue No. SAA 09381
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Mercury medium pressure lamp TQ 718 Z2 With additional radiation intensity 500 - 550 nm Catalogue No. SAA 09382 -

Mercury medium pressure lamp TQ 150 Capacity 150 W Lamp voltage 85 V Catalogue No. SAA 09360 Mercury medium pressure lamp TQ 150 Z1 With additional radiation intensity 400 - 450 nm Catalogue No. SAA 09361

Mercury medium pressure lamp TQ 718 Z3 With additional radiation intensity 280 - 360 nm and 460 - 510 nm Catalogue No. SAA 09383 -

Mercury medium pressure lamp TQ 150 Z2 With additional radiation intensity 500 - 550 nm Catalogue No. SAA 09362

Power unit fitting for TQ 718 lamps Connecting voltage 220 V, 50 Hz Catalogue No. SAA 09384 -

Table tripod frame for the mounting of the photoreactor, made of V4A tube, outer diameter 26.9 mm with powder-coated tube connectors, Dimensions: W 800 x D 550 x H 1080 mm Catalogue No. SAA 09385

Mercury medium pressure lamp TQ 150 Z3 With additional radiation intensity 280 - 360 nm and 460 - 510 nm Catalogue No. SAA 09363

Power unit fitting for TQ 150, TQ 150 Z1,TQ 150 Z2 and TQ 150 Z3 lamps Connecting voltage 220 V, 50 Hz Catalogue No. SAA 09364

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PHOTOREACTOR WITH FORCED LIQUID CIRCULATION
GENERAL
The synthesis via the photo chemistry is a commonly applied method. Organic synthesises often succeed only due to the radiation with UV-light or will be speeded up. Photochemical reactions are often run at room temperature and so they are gentler than other thermal processes. Photoreactors have a wide range of application, e.g. in synthesis, analysis and waste water treatment.

Construction of the Photoreactor

The radiation vessel is the main component of the reactor. It has a capacity of approx. 350 - 400 ml. Cooling tube and immersion tube, both made of quartz glass, are located in the radiation vessel. The circulation of the liquid is effected by the forced circulation pump "System Normag", which is controlled by a control unit. A thermometer for temperature range from 0 C - 150 C is part of delivery as well as small pieces. Catalogue No. SAA 09316

Pict. Photoreactor with forced liquid circulation

The Normag Photoreactor offers the following advantages:

m m m m

An effective circulation of the liquid to be radiated inside the reactor. Only a small liquid volume is necessary. Used materials Borosilicate glass 3.3, quartz glass and plastic parts of PTFE. This photoreactor is suitable for the mercury low pressure lamp TNN 15/32 and for the mercury medium pressure lamps TQ 150, TQ 150 Z1, TQ 150 Z2 and TQ 150 Z3.

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Accessory for the Photoreactor: r Mercury low pressure lamp TNN 15/32 Capacity 15 W, Lamp voltage 55 V Catalogue No. SAA 09370 r Power unit fitting for TNN 15/32, connecting voltage 230 V, 50 Hz Catalogue No. SAA 09371 r Mercury medium pressure lamp TQ 150 Capacity 150 W Lamp voltage 85 V Catalogue No. SAA 09360 Mercury medium pressure lamp TQ 150 Z1 With additional radiation intensity 400 - 450 nm Catalogue No. SAA 09361 Mercury medium pressure lamp TQ 150 Z2 With additional radiation intensity 500 - 550 nm Catalogue No. SAA 09362 Mercury medium pressure lamp TQ 150 Z3 With additional radiation intensity 280 - 360 nm and 460 - 510 nm Catalogue No. SAA 09363 r Power unit fitting for TQ 150, TQ 150 Z1, TQ 150 Z2 and TQ 150 Z3 lamps Connecting voltage 220 V, 50 Hz Catalogue No. SAA 09364 r Table tripod frame for the mounting of the photoreactor, made of V4A tube, outer diameter 26.9 mm with powder-coated tube connectors, Dimensions: W 800 x D 550 x H 1080 mm Catalogue No. SAA 09385

Legend: 1 2 3 4 5, 6 7 8 9 10 11 12 13 14 15 16 Radiation vessel Cooling tube, quartz glass Mercury medium pressure lamp TQ150 Mercury medium pressure lamp TNN 15/32 Power unit Gassing frit Thermometer Cooling water connections GL 14 Forced liquid pump Pump impeller Glass stopcock Spindle valve for drain off Motor Speed regulation device Ventilating and feeding connection

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LABORATORY UNIT FOR GAS ABSORPTION
GENERAL
Absorption is the intake of gases in a washing liquid by physical solving or reversible chemical reaction. Depending on whether the gas by physical solving or by chemical binding is bound it is a physical or a chemical absorption. When a mixture CO2/air gets in touch with water, the CO2 gas is absorbed in the water but the air is not solved. The absorption capacity of the water for carbon dioxide depends on the influence time, the pressure and the temperature. This unit provides the facility the carbon dioxide to wash out of the carbon dioxide/air mixture. Due to the ratio of the both components determining the separating effect, the solvent flow and the gas flow are aimed varied.

Pict. 1 Laboratory unit for gas absorption

The unit offers the following advantages:

m m m

Due to the slight construction height, use in almost all laboratories is possible. All media-touching parts are made of Borosilicate glass 3.3 or PTFE. The single components of the unit are connected with standardised connectors.

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Construction of the Laboratory unit for gas absorption
The core of the unit is the absorption column consisting of the absorption tube (K), a gas inlet (G) and a siphon part (S). The mentioned parts are connected with conical ground joints NS 45/40 and fitted with a silver coated high vacuum jacket. The absorption column has an inner diameter DN 50 and a length of approx. 1400 mm. The inlet component (E) seats on the upper end of the column and at the lower end seats the siphon part with the drain valve. The both gases air and CO2 are introduced via the connections 1 and 2, adjusted with the valves (V2) and (V3) and mixed together in the mixer (M) then fed over the heat exchanger into the absorption column which is filled with Raschig rings 4/4 mm. The absorption liquid water is directed from the top towards the gas in counter flow from vessel (B1) with the pump (P) and over a flow meter (Q1) and the heat exchanger (W1). The both heat exchanger (W1) and (W2) are connected with a thermostat (TS). Through this is reached that absorption gas and absorption liquid are fed with the same temperature into the absorption column. The issued gas is directed for analysis into a gas analyser (GA). The inlet gas can be also analysed by switching of the three way stopcock (VD). Following data can be captured via a data logger in the unit: Temperature at the water inlet (T1) Temperature at the gas inlet (T2) Temperature in the siphon (T3) Electric conductivity at the water inlet (L1) Electric conductivity in the siphon (L2) Differential pressure above the column (DD) Gas concentration (GA)

The measuring can be analysed at the PC with a suitable software. We will be pleased to submit you our detailed offer.

Drain for Gas Air

Drain

Legend: B1,B2 DD E G GA K

Vessels Differential pressure sensor Inlet part Gas inlet part Gas analyser Absorption tube

L1,L2 M ME P Q1 Q2,Q3 S

Conductivity sensor Mixer Data logger Pump Flow rate meter Rotameter Siphon part

TP TS T1-T3 V VD V1-V3 W1,W2

Cartridge Thermostat Pt 100-thermometer Overpressure valve Three way stopcock Valves Heat exchanger

Pict. 2 schematic description

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LABORATORY UNIT FOR ABSORPTION OF REACTION GASES
GENERAL
This NORMAG unit for absorption of reaction gas distinguished by its compact construction which meets the high requirements for such units. The only used materials are Borosilicate glass 3.3 and PTFE. Additional safety give powder coated glass parts if required. Only one flange connection will contact the absorption liquid, the other connections are located in the gas part. The flange connections and all other spherical ground joints are polished and allow a long dwell time of the unit. Due to this fact, high concentrated bases as absorption liquids can be used. The connections are sealed with PTFE seals. High vacuum spindle valves made of Borosilicate glass 3.3 and PTFE serve for the locking of the gases and the absorption liquid. The unit is suitable for use under vacuum and available in different types. The sizes 6 litres and 10 litres are designed for laboratory purposes. For this unit we offer a mobile frame, made of stainless steel tube, with safety bath.

Pict. 1 Laboratory unit for the absorption of reaction gases

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Construction of the absorption unit
The core of this NORMAG unit for absorption of reaction gas is the absorption column which is sealed on the receiver for the absorption liquid. The absorption liquid is cooled by a double coil, made of Borosilicate glass 3.3, inside the absorption receiver. Connections for the cooling are flanges Pl 15 providing the facility to connect a thermostat hose. Two glass adapter for coupling flange Pl 15 and olive D11 are part of the delivery. The NORMAG glass pump for forced liquid circulation of the absorption liquid with magnet drive is located below the receiver, guaranteeing a quick exchange. Normally, the pump volume is 120 litres/h by 1500 revs/min, but the pump volume can be changed with the control device. Due to safety reasons, the suction and pressure tubes are inside the absorption column. To increase the reaction surface, Raschig rings as packing are used. The gas to be purified is introduced via the HV spindle valve 3 into the unit and rises in the absorption column. The pumped up absorption liquid runs over the Raschig rings towards the gas and the mass transfer can start. The drain off of the purified gas is effected by the connected manifold with spindle valves. The flange and thread connections at the receiver serve for the refilling of the absorption liquid and for taking a thermometer or pH-sensor. A connection, which serves for cleaning the unit is sealed on the head of the absorption column. The used absorption liquid can be drained off by opening the spindle valve at the pump, then the unit can be cleaned and after closing the valve a new absorption liquid can be introduced. For automatic use, an addition funnel is tightly connected with the receiver, so that the absorption liquid can be refilled automatically.

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control device

Legend: 1 2 3 4 5 6 Control device Cooling water connection Gas inlet Connection for absorption liquid Outlet for purified gas Connection for cleaning the unit

Pict. 2 schematic description

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LABORATORY UNIT FOR DISCONTINUOUS DISTILLATION
GENERAL
This discontinuous distillation unit can be used for diverse purposes in laboratory. The unit can be employed for preparative work, for processing of solvents as well as for research and teaching. The reachable separation efficiency depends on the used column type and the throughput.

Pict.1 Laboratory unit for discontinuous distillation

The laboratory unit for discontinuous distillation offers the following advantages:
m m m m m m

Due to its small construction height, use in almost all laboratories is possible. In most cases, the unit can be fitted in a flue. All product-touching parts are made of Borosilicate glass 3.3 enabling the use of a wide range of substances. All single parts of the unit are fitted with standardised connections as NS ground joints, spherical ground joints or flanges. The unit can be operated under normal pressure and under vacuum. The operation temperatures can reach up to +200 C. The unit has an high safety standard, but does not have an EX protection.

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Construction of the discontinuous distillation unit
The boiling flask (B) with a reaction volume of approx. 2 litres has three necks. The packed column (K) DN 30 with a length of 600 mm is fitted onto the centre neck of the reaction vessel with ground joint NS 29/32. The column is fitted with a high vacuum jacket, is silver coated and has sight strips. The both side necks of the boiling flask with NS ground joints take the constant addition funnel (DT) with approx. 1000 ml volume, glass needle valve and vacuum equalising line and the Pt 100-thermometer. The packed column contains 4x4 Raschig rings. The column head (KK) with electromagnetic funnel, vacuum connection with ventilation and connection for Pt 100-thermometer is on the top of the column. The taken distillate is led into the graduated receiver (V) with a volume of approx. 1000 ml and outlet valve. The control of the permanent cooling water flow in the column head during the distillation is ensured per flow watcher sensor (DS) with control unit for switching off the heating. A heating mantle (H) with a capacity of 600 W serves for the heating of the distillation unit and a power controller (LS) supervises the heating capacity and the temperature for the boiling flask. The time impulse for outlet or reflux of the distillate are controlled with a timer (TG). A chemical resistant vacuum pump stand (VP) combined with a vacuum controller (VC) with pressure sensor (PS) and magnet valve (MV) ensure a constant working under vacuum lower than 10 mbar. The pre-fitted cold trap serves for the condensation of the gases. Power controller, timer and vacuum controller are fitted with a digital interface. This offers the possibility to connect the devices at one PC and to analyse the captured data of e.g. temperature and pressure with a suitable software. The unit is mounted in a robust frame with safety bath and trays, all made of stainless steel. Dimensions: L x D x H: 1600 x 600 x 2000 mm

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Cooling water

Legend: B DS DT H K KF KK LS M MV PC PS Pt TG V VC VP Boiling flask Flow watch sensor Addition funnel Heating mantle Packed column Cold trap Column head Power controller Magnet for reflux control Magnet valve for vacuum locking PC Vacuum pressure sensor Pt 100-thermometer Timer Receiver, graduated Vacuum controller Vacuum pump

Data line RS 232

Pict. 2 schematic description

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LABORATORY UNIT FOR CONTINUOUS DISTILLATION
GENERAL
This continuous distillation unit can be used for diverse purposes in laboratory. Its use reaches from processing of solvents, the application in research and teaching to process development and process optimising. The reachable separating efficiency depends on the used column type and the volume to be distilled.

Pict. 1 Laboratory unit for continuous distillation

This laboratory unit offers the following advantages:

m m m m m m m

Due to the small construction height, use in almost all laboratories is possible. All product-touching parts are made of Borosilicate glass 3.3 or PTFE, enabling the use of a wide range of substances. All single parts of the unit are fitted with standardised connections as NS-ground joints, spherical ground joints or flanges. The unit can be operated under normal pressure and under vacuum. The operation temperatures can reach up to 200 C. The measurement and control technology is modularly constructed, so the unit can be manually or automatically operated. The unit has an high safety standard, but does not have an EX-protection.

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Construction of the continuous distillation unit
The basic part of the unit is an horizontal circulating evaporator (V) with a capacity of approx. 2 litres, which is heated by a heating plug (HK). A condenser (K) is located below the evaporator for cooling the sump product during the drain off per pump (P2) into the vessel (B2). The unit consists of two packed columns DN 50 (K1) and (K2). Between these two columns the infeed part (E) is located which is fitted with a pre-heater. Above the column is an electromagnetic controlled column head (KK). During the operation of the unit, the start product is pumped per pump (P1) from the vessel (B1) into the pre-heater (VH) and flows via the infeed part into the column. For taking the temperatures inside the evaporator, pre-heater, column and column head, Pt 100-thermometer are used. Light rod sensors (LS) ensure the monitoring of the fill level in the evaporator. A timer (TG), a differential pressure regulating valve (DR) and a power controller are used for measurement and control of the unit. All measuring data are captured per data logger and analysed with a computer with belonging software. The measurement and control technology provides the facility for a fully automatical operation of the unit. A flow rate sensor, integrated in the cooling water circulation, will switch off the unit if necessary.

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Legend: B1 B2 DR DS DV Vessel (start product) Vessel (sump product) Differential pressure controller Differential pressure sensor Receiver

E HK K KK K1 K2 LS

Infeed part Heating plug Condenser Column head Lower column Upper column Light rod

N P1, P2 T TG TR V VH

Mains connection Pumps Pt 100-thermometer Timer Temperature controller Circulating evaporator Pre-heater

Pict. 2 schematic description

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MICRO SPINNING BAND COLUMN
GENERAL
The micro spinning band column can be used for different purposes. Its use reaches from research and teaching to solutions for specific separating tasks in the industry. After the separation of the substances, the distillate drain off is electromagnetic according to the vapour division principle. The effective column length is approx. 1000 mm. The test mixture n-Heptan / Methylcyclohexan reaches a separating efficiency of approx. 50 theoretic plates under normal pressure and infinite reflux.

Pict. Micro spinning band column

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Construction of the micro spinning band column

The basic part of the unit is the micro jacket column DN 6 with sealed electromagnetic controlled vapour divider and AnschtzThiele receiver. The spinning band column has a silver coated high vacuum jacket with bellows and sight strips. A vacuum magnet stirrer seal made of stainless steel is fitted via a flat flange DN 50. Inside the column is the HOSTAFLON band which is brought in rotation with the driving motor. A control unit adjusts the revs of the spinning band. The drain and reflux of the distillate is controlled with the digital timer which receives the measuring from a Pt 100-thermometer. The heating of the boiling flask can be effected either with a circulating thermostat or with a heating mantle with power control. The individual fractions are collected in a vacuum rotary receiver.

Accessories for the micro spinning band column: Special boiling flasks with tempering jacket, volumes 25 ml, 50 ml, 100 ml Special boiling flasks with tempering jacket and additional silver coated high vacuum jacket, volumes 25 ml and 50 ml Magnet stirrer with rev control Lab jack, made of stainless steel Circulating thermostat with working temperature range from +20 to +250 C Circulating condenser with working temperature range from -10 C to +40 C Normag digital thermometer Normag digital vacuum controller Pt 100-thermometer, installation length 35 mm Pt 100-thermometer for special boiling flasks Vacuum spinning receiver Frame to bear the unit, made of stainless steel tube, diameter 26.9 mm, powder coated tube connectors, Dimensions L x D x H: 1600 x 600 x 2000 mm

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UNIVERSAL REACTION UNIT FOR DISCONTINUOUS OPERATION
GENERAL
The discontinuously working reaction unit has been designed for various reactions in the liquid phase. It is an universal unit, typical for laboratory technique, multifunctional and expandable standard unit. The reaction vessel made of Borosilicate glass 3.3 can have different volumes reaching from 0.5 to 10 litres and more. The unit can be used for synthesis and separation as well as for bio-reactions.

Pict. 1 Universal reaction unit for discontinuous operation

The universal reaction unit offers the following advantages:

m m m m m m

The unit can be operated under vacuum, normal pressure or slight overpressure. It is possible to realise reactions in temperature ranges from -30 C to +200 C, provided the thermostat is suitable. All product-touching parts are made of Borosilicate glass 3.3 or PTFE, providing the facility for use of many different substances. Due to the use of Borosilicate glass 3.3, reactions can be watched. A controlled running of reactions is possible in a certain temperature range and a reproducible addition of several liquids is granted. The measurement and control technology is modularly constructed and can be operated with different sensors. Data can be captured and analysed in time intervals.

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Construction of the universal reaction unit
The core of this unit is the flat flange reaction vessel DN 200 with a volume of approx. 10 litres with silver coated high vacuum and tempering jacket and adjustable PTFE bottom outlet valve DN 15. A flat flange lid DN 200 with centre neck socket NS 29/32 and side neck sockets NS 29/32, NS 14/23 and GL threads 18 and 25 allows the connecting of peripheral components for stirring, feeding and measuring. The robust triple clamp DN 200, made of stainless steel, closes the lid and the vessel and offers additionally the possibility to secure the unit in the frame. Lid and vessel are sealed with an O-ring, made of silicone and FEP-lined. A stainless steel anchor stirrer, shaft diameter 10 mm, is introduced over a suitable stirrer seal with double PTFE sealing and serves for a fine mixing of the substances. With a jacketed reflux condenser with off-distilling function can be distilled off via the Anschtz-Thiele receiver into the round bottom flask. The used agitator offers the rev range from 12 to 2000 revs/min. and has a digital display. Different liquids can be introduced into the reactor either via a temperable addition funnel of 1000 ml or via two diaphragm pumps with a range of 0.08 to 80 ml/min. An efficient circulating thermostat provides a large temperature range for operations. A chemical resistant diaphragm pump with a pumping speed of 1m/h allows to carry out reactions under vacuum. Two Pt 100-thermometer and a pH-sensor take the data which are captured and analysed with a computer with belonging software. The unit is mounted in a robust and mobile frame of stainless steel tubes, diameter 26.9 mm, with trays and safety bath. Dimensions of the frame: L x D x H: 1600 x 600 x 2000 mm.

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Legend: AT B D1 D2 DT ME Pict. 2 schematic description Anschtz-Thiele receiver Receiver Pump 1 Pump 2 Addition funnel Data capture P PC RK RW T Vacuum pump PC Reflux condenser Agitator Thermostat

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HIGH VACUUM PUMP STAND FOR VARIABLE USE IN LABORATORIES
GENERAL
In many cases, the use of vacuum is necessary for the running of different chemical processes. Especially in research and development of new products in laboratory, processes run under vacuum or with feeding in of inert gas. Due to this reason, the NORMAG LABOR- und PROZESSTECHNIK GmbH has developed a mobile vacuum pump stand meeting the highest requirements.

Pict. 1 High vacuum pump stand for variable use in laboratories

Technical data: Standard dimensions of the pump stand (L/H/D) 500 x 500 x 1400 mm Combined pump stand consisting of: - Chemical resistant diaphragm pump - Two stage rotary vane pump - Connecting voltage: 230 V, 50 Hz - Pumping speed: 3.7 m/h - Ultimate pressure: 3 x 10-3 mbar Vacuum meter with CAP 120 / Measuring range: 200 - 0.1 mbar

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Construction of the high vacuum pump stand
The pump stand consists of two easy to dismantle single elements, connected with high vacuum flanges in different sizes. Between the flanges are centring rings with Viton sealing, giving a safe seal and centring of the flanges. The connections for taking vacuum and inert gas are robust high vacuum double spindle valves. The stems of these valves can be made as NS-cone, glass thread or olives, just for customer's requirements. Two safety/overpressure valves guarantee that the unit will not be injured, caused by failure in operating. Due to the pre-fitting of several cold traps it is possible to condense gaseous parts in the suction line. A connection with a high vacuum flange DN 16 provides the facility to connect a vacuum meter with capacitive sensor. The locking of the unit versus the vacuum pump is effected with a great high vacuum spindle valve DN 15. A chemvac combined pump stand serves as vacuum pump. This guarantees the reaching of a sufficient vacuum, and the chemical resistant design ensures a wide range of applications. The vacuum pump stand is integrated in a mobile frame of stainless steel tubes, tube diameter 26.9 mm. Rollers give the possibility to move the stand within the laboratory. Pump stand, vacuum pump and frame can be designed to customer's requirements.

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All ground joints are also available in other standard sizes, e.g. US-standard.

Connections - cones ground standard 14/23 Connection vacuum measurement device

Pict. 2 schematic description

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Connection metalhose on vacuum pump

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SHORT PATH EVAPORATOR UNIT DSV 80

Pict. Short path evaporator unit DSV 80

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Construction of the short path evaporator unit DSV 80
This short path evaporator with roll wiper cage is used for distillation of temperature sensitive products in vacuum ranges from 1-10-3 mbar. The dwell time in the heating zone is only a few seconds. The composition of the condenser in the centre of the evaporator, direct in face to the heating surface, enables the running of short path distillations. The short path evaporator type DSV 80 is made of Borosilicate glass 3.3 and is suitable for short path distillations in laboratories. The evaporator has an inner diameter of 75 mm and a heating surface of 0.058 m. The heating is effected with a liquid medium. A rotating roll wiper cage produces a liquid film on the evaporator surface. The armature is powered from outside via a laboratory agitator and vacuum magnet stirrer seal. The vapours condense at the condenser in the centre of the evaporator. The distillate runs down over the condenser into the distilling receiver. The not distilled sump product is sampled in a ring line below the heating zone and lateral led into the sump receiver. The evaporator can be used for liquid substances with an higher viscosity too. Operation pressure: Medium heating temperature: Distillation volume: Dimensions of the frame: 760 mbar to 10-3 mbar max. 250 C 0.3 to 1 kg/h L x H x D 1500 x 2000 x 600 mm

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