1 AS 2365.1.

2—1990

Australian Standard
Methods for the sampling and analysis of
indoor air

Method 1.2: Determination of nitrogen

dioxide—Spectrophotometric method—
Treated filter/passive badge sampling
procedure
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PREFACE

This Standard was prepared by the Standards Australia Committee on Methods for
Examination of Air under the direction of the Chemical Standards Board.

CONTENTS
Page
1 SCOPE . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . ... .. .. .. . 1
2 APPLICATION . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . ..... .... . 1
3 REFERENCED DOCUMENTS . . . . . . . . . . . . . . . . . . . .. ... ..... 2
4 PRINCIPLE . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .. . . .... 2
5 DEFINITION . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . ..... .. . .. 2
6 REAGENTS AND MATERIALS . . . . . . . . . . . . . . . . . . ... .. ..... 2
7 APPARATUS . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . ..... ... .. 2
8 PREPARATION OF PASSIVE SAMPLING BADGES . . . . .. .. . .. .. 3
9 SAMPLING . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . ..... ..... 3
10 PROCEDURE . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . ..... ... .. 4
11 CALCULATION AND EXPRESSION OF RESULTS . . . . .. .. . .. .. 5
12 PRECISION . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . ..... .. ... 5
13 TEST REPORT . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . ..... .... . 6
14 BIBLIOGRAPHY . . . . . . . . . . . . . . . . . . . . . . . . . . . . . ... .. ..... 6

METHOD

1 SCOPE. This Standard sets out a spectrophotometric method for the

determination of nitrogen dioxide in indoor air using a passive sampling, treated filter
technique. This method is applicable to indoor air in which the expected nitrogen
dioxide concentration is within the range 0 to 3 p.p.m. (V/V) (0 to 6 000 µg/m 3) for an
exposure time of 1 h, and has a detection limit of 0.035 p.p.m. for a 2 h sampling
period.
2 APPLICATION. Passive sampling badges exhibit sampling rates dependent on
the dimensions of the device and the properties of the diffusion barrier. If decreased
sensitivity or increased sampling duration is required, the method in AS 2365.1.1
should be used. This method is unsuitable for use in areas where the air velocity is
greater than that produced by a ventilation rate of two air changes per hour. In
addition, a sampling time of less than 2 h is not recommended; the method gives best
results for sampling times between 2 h and 12 h. The sampling procedure specified is
not suitable for indoor atmospheres which fall below 0°C.

COPYRIGHT
 This is a free preview. Purchase the entire publication at the link below:

AS 2365.1.2-1990, Methods for the sampling and

analysis of indoor air Determination of nitrogen
dioxide - Spectrophotometric method - Treated
This is a free 1 page sample. Access the full version at http://infostore.saiglobal.com.

filter/passive badge sampling procedures

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