BEURRE FONDANT CORPS

HOT FILLING

CONDENSATION
PENETROMETRY
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Mixa beurre fondant corps- hot filling implementation

Product presentation
Formula 603991/2: To obtain a butter texture in other words a firm and not sticky cream with melting application Fabrication process : Concentrate/dilution on one time process with end of manufacturing at 40C Filling process: Filling at 40C without cooling tunnel Quality Controls: texture analysed by penetrometry Product history: at the beginning, this texture was for Garnier brand with production at Karlsruhe plant on the 20T Skid with TMS target of 150min and real TM 150/180min (product is on stand by for the moment). Then the R&I developed this product for Mixa with production at Israel plant. This texture will be used for other formulae for the other brands of the Group. Now: we made several trials of fabrication and filling to analyse the texture impact. Study to limit the problem of condensation into the storage vessels. The Israel plant produced 8 fabrications of 3,6T ( 107 Ku FG) with real TM = 140min

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Mixa beurre fondant corps- hot filling implementation

Keys points of production Process To add 12% of hot 511S into the oily phase Heating temperature of the oily phase : 65 70C: we determined this temperature according to cold 511S temperature To add gelling phase 75238 + 52022 after the emulsion Dosing 511S of dilution ( 19C in Isral) less of 20 minutes Dispersion after dilution less of 10 minutes RT = 40C Not cooling step at the end and final Temperature= 40C Filling at 40C at the maximum volume of the jar to limit condensation problem 3/8

Mixa beurre fondant corps Hot filling implementation The goal- filling the bulk at a temperature between 3743 C. Solution Isolation of mobile storage vessels to keep the temperature. Step 1 Isolating the mobile storage vessels with foaming polyethylene. Step 2 validation of the bulk temperature over a defined period of time. .

Date

Filling room-mobile vessel

temperature

Production date-22/11/2010 24/11/2010 25/11/2010 26/11/2010

42c 40c 38.5c 37.5c

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Mixa beurre fondant corps- hot filling implementation Main issue Condensation in the storage vessels

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Mixa beurre fondant corps- hot filling implementation Main issue Condensation in the storage vessels Solution leveling the temperature of the vessel surface to the bulks Step 1 Installation of heating device over the upper area of the vessel Step 2 Installation of heating device over the manhole cover

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Mixa beurre fondant corps- hot filling implementation Main issue Condensation in the storage vessels Results- No condensation found on the top surface of the bulk.

Ambiant

Heated

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Mixa beurre fondant corps- hot filling implementation

Evaluation of the cosmeticity : Penetrometry

Method: Followed by penetrometry measures during the time (measure of strength by compression) with a specific equipment. Measures done on FG at 20C. Final result is the strenght resultant in gram g.
Strenght (g)
Force (g)
120 100

allure de plateau = texture homogn

F 1

80

60

40

Proto 36013 prlv2 Mobile P20 T> 16h

0 2 4 6 8 10

20

0 -2

Distance (mm)

Distance (mm)
-20

-40

-60

-80

-100

Conclusion: We propose to the R&I to use the penetrometry with sensorial analysis when they look for a particular texture that is difficult to well analysed with classical controls
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A retenir

Cette nouvelle texture est trs demande par les marketing qui recherchent de plus en plus de textures riches et beurre notamment pour les produits corps. Cette formule est une mulsion coule en pot 40C et refroidie en PF temprature ambiante. Les difficults rencontres concernent la temprature laquelle elle devait tre coule pour obtenir la texture souhaite sans tunnel de refroidissement en tenant compte de la fragilit de la texture cisaillement et en limitant la formation de condensation critique dun point de vue qualitatif et microbiologique. Lquipement industriel a t adapt et les conditions de production ont t affines lors dun pilote industriel. Dun point de vue caractrisation de la texture ce projet a fait lobjet dun dveloppement de protocole de pntromtrie . La spcification contient donc une mesure de pntromtrie sur PF. Dautres projets similaires sont en cours dtude plus ou moins avance pour les marques CCB, Vichy. Prcdemment un projet Garnier avait t dvelopp mais navait pas abouti.