You are on page 1of 26

TRNG I HC CNG NGHIP TPHCM KHOA CNG NGH HA HC

MN HC: PHN TCH CNG NGHIP


TI: THNH PHN, CH BIN M CAO SU. XC NH HM LNG CN, TR S KOH C TRONG M CAO SU LY TM

GVGD: SVTH: LP :

Th.s TRN NGUYN AN SA L TRN THY TIN DHPT5 09085701

Ni dung

LOGO

1 2

Tng quan v cao su Quy trnh ch bin m cao su ly tm

3
4

Xc nh mt s ch tiu trong cao su ly tm


Ti liu tham kho

Tng quan v cao su

LOGO

Cao su thuc loi polyterpene c cng thc phn t (C5H8)n

.Cao su thin nhin trch t m cao su.


Trong m cao su c hydrocarbon (90-95%), protein, ng, acid bo nha. Trong nha cao su c khong 40% l cht rn,

trong c ti 90% l hp cht cao su phn hy ca


hidrocacbon khng no, 10% l cc thnh phn thnh phn khc nh protein, lipit, gluxit, mui v c,

Tng quan v cao su


V mt ha hc, cao su thin nhin l polyisopren -polyme ca
isopren

LOGO

Mch i phn t ca cao su thin nhin c hnh thnh t cc mt xch isopren ng phn cis lin kt vi nhau v tr 1,4.

Tng quan v cao su

LOGO

Thm acid acetic hoc acid bo vo m cao su th cao su ng vn


li v tch ra khi dung dch. p ng khun v sy kh bng khng kh hoc hun khi thu c cao su th. Cao su t nhin l poliisopren c cu hnh cis. Cao su thin nhin mm kt dnh d ha nha khi c nhit

Quy trnh ch bin m cao su ly tm

LOGO

Cng on x l nguyn liu Cng on gia cng c hc

2 3
4

Cng on sy Cng on hon thin sn phm

Quy trnh ch bin m cao su ly tm


Cng on x l nguyn liu: m mi thu hoch c chng ng bng amoniac, sau c a v x vo b cha, trn

LOGO

u bng my khuy. Tip theo, m nc c dn vo cc


mng nh ng bng cc mng dn inox, y m c lm ng nh axit acetic 5% ( HCOOH)

Quy trnh ch bin m cao su ly tm

LOGO

Mng nh ng

Quy trnh ch bin m cao su ly tm


Cng on gia cng c hc: m ng trong cc mng nh ng c a qua my cn, my ko, my cn to t, my ct bm cm cui cng on to ra cc ht cao su cm sau s c ra sch trong h cha m.

LOGO

My cn, my p

Quy trnh ch bin m cao su ly tm

LOGO

My cn, my p

Quy trnh ch bin m cao su ly tm


Cng on sy: nh h thng bm thi ra v h thng phn phi m t ng c sn rung lm ro nc v to xp cho m, sau m c cho vo xe y a vo l sy nhit 110 120 0C trong khong 90 pht th m chn v

LOGO

vn chuyn ra khi l sy.

Quy trnh ch bin m cao su ly tm

LOGO

L sy

Quy trnh ch bin m cao su ly tm


Cng an hon thin sn phm: m c qut ngui, em

LOGO

cn v p bnh vi kch thc v trng lng theo tiu chun


TCVN 3769 83 (33,3 kg mi bnh). Cc bnh cao su c bc bng bao PE v a vo kho tr sn phm.

Quy trnh ch bin m cao su ly tm

LOGO

Cc ch tiu trong cao su ly tm

LOGO

Xc nh hm lng cn

Xc nh tr s KOH

Xc nh hm lng cn
PHM VI P DNG

LOGO

Tiu chun ny qui nh phng php xc nh hm lng cn ca latex cao su thin nhin c c. Phng php ny ch thch hp vi latex t ngun gc Hevea

brasiliensis, khng thch hp cho latex phi liu hoc latex lu


ha.

Xc nh hm lng cn
NGUYN TC

LOGO

Ly tm phn mu th. Ra nhiu ln phn cn thu c

bng dung dch cn-amoniac.Sau sy kh cn n khi


lng thay i

Xc nh hm lng cn
Cn latex c c t 40g n 45g, chnh xc n 0,1 Ly tm khong 20 pht

LOGO

khi lng b mt gia 2 ln cn nh hn 1mg

ly ra phn cht lng ni cch b mt cn khong 10 mm.


gn dung dch trn n vch 10 mm Cho cn vo y np trong 20 pht

Sy kh 70

Trong 30 pht

lm bay hi cho n cn
Chn chu nhit

Xc nh hm lng cn
Tnh kt qu
Tnh tng hm lng cn ( TSC) bng phn trm khi lng theo cng thc:

LOGO

m1 100 m0
Trong
m0 l khi lng ca phn mu th, tnh bng gam m1 l khi lng ca cn sy kh, tnh bng gam Chnh lch gia hai kt qu khng c qu 0,002% ( khi lng ).

Xc nh tr s KOH
nh ngha
Tr s KOH ( ca latex) : s gam ca kali hydroxyt cn thit
trung ho cc gc axit c lin kt vi amoniac trong latex cha 100 g tng hm lng cht rn

LOGO

Xc nh tr s KOH
PHM VI P DNG

LOGO

Tiu chun ny quy nh phng php xc nh tr s KOH ca

latex cao su thin nhin c c c bo qun ton b hay mt


phn bng amoniac. Phng php ny c th p dng cho cc loi latex c bo

qun bng axit boric. Phng php ny khng p dng cho cc


loi latex bo qun bng kali hydroxyt . N khng thch hp vi cc loi latex c ngun gc t nhin khc vi Heavea brasiliensis, hoc latex tng hp, latex phi liu, latex lu ho hoc cao su khuych tn nhn to

Xc nh tr s KOH
CCH TIN HNH

LOGO

Cn 50 g tng cht rn mt lng mu th.

Cho vo cc thu tinh dung tch 400 ml kim 0,5 0,1% NH3

Xc nh im un ca ng cong chun

Nhng in cc ca my o pH vo latex c c pha long v ghi pH.

Pha long latex bng nc n 30 % tng cht rn.

Xc nh tr s KOH
Tnh th tch dung dch formaldehyt c thm vo theo cng thc sau:

LOGO

m(100 WTS)(A 0,5) 1134C (HCHO)


Trong :
C(HCHO) l nng thc t ca dung dch formaldehyt tnh bng mol /dm3

Xc nh tr s KOH
Tr s KOH ca latex caosu thin nhin c c c tnh bng % khi lng theo cng thc:

LOGO

561CV W TS xM
Trong :

C l nng thc t ca dung dch kali hydroxyt, c biu th


bng phn t lng KOH / dm3 V l th tch ca dung dch kali hydroxyt , tnh bng cm3

WTS l tng hm lng cht kh ca latex tnh bng % khi


lng. m l khi lng ca mu th latex, tnh bng gam.

Ti liu tham kho


TCVN 6089: 2004 Cao su thin nhin Xc nh hm lng cht bn TCVN 6315 : 2007 Latex, cao su-Xc nh tng hm lng cht rn TCVN 4856 : 2007 Latex cao su thin nhin c c-Xc nh tr s KOH

LOGO

THE END

You might also like