TI 1 KIM TRA CHT LNG BIA

LP D10-TP02 NHM 12 NGUYN TH NGC L TH KIM DUYN V TH THANH TRC V TH NGUYN PHN LNG TH NH TUYN

I. GII THIU TNG QUAN V BIA

1. NH NGHA
Bia (t ting Php: bire : Anh: beer hoc c: bier) l mt loi ung cha cn Sn xut bng qu trnh ln men ng l lng trong mi trng lng Khng c chng ct sau khi ln men Dung dch ng khng b ln men thu c t qu trnh ngm nc gi l hm bia hay "nc bia Qu trnh sn xut bia c gi l nu bia

2. PHN LOI
Theo mu sc v hng v:

Bia vng

Bia

2. PHN LOI

Bia en Bia trng

2. PHN LOI

Theo phng thc ln men: Ln men ni Ln men chm Ln men t nhin

2. PHN LOI
Loi bia hn hp:
- Bia hoa qu v bia rau c - Bia tho mc v bia gia v

- Bia truyn thng hay thc nghim

- Bia hun khi - Bia c bit

3. VAI TR CA BIA

a) Thnh phn dinh dng: - Nc chim 90% trong bia, cung cp mt s cht khong v nng lng.

90% Nc

3. VAI TR CA BIA

- Ngoi ra trong bia cn c Polyphenol (mt cht chng oxi ha v ung th), CO2 gip tiu ho nhanh, gim cng thng, cung cp mt s vitamin cho c th.

3. VAI TR CA BIA
b) ch li: - Bia l ngun chnh cung cp silicon cho c th gip xng chc hn. - Vitamin B6 trong bia gip ngn nga s pht trin ca bnh tim - Hoa bia c trong bia cha xanthohumol, mt cht chng oxy ha mnh m, phng chng bnh ung th v long xng - Gim Cholesterol, gim mt ng, gim ri ro ca bnh tiu ng

3. VAI TR CA BIA
c) Tc hi: - Vim d dy - Vim tuyn tu cp tnh - X gan - Thai ph ung bia ru c th tc ng xu n bo thai

4. CNG NGH SN XUT BIA

a) Nguyn liu: Nc Malt Hoa bia (hublong) Men bia Cht ph gia

4. CNG NGH SN XUT BIA

Quy trnh sn xut:

II. CC PHNG PHP KIM TRA

1. I VI NGUYN LIU:
a) i vi Malt: - Mu sc: vng ti, v ng nh - Mi thm t nhin , khng mi l, mi mc - V khng qu 7- 9% trng lng ht - Lc ny mm sau ngy th 3 t 80- 85% v sau 6 ngy l 95%

1. I VI NGUYN LIU:

m: <5% Protein: 9-12% Tinh bt: 63-65% sch: khng ln tp cht, rm rc, ng cc khc. Ht khng b v. - Ht kh, v mng, khng t vt su, mc, nt lp hay xanh - Khi kim tra: cn ht c mi tinh bt v v hi ngt

1. I VI NGUYN LIU:
b) i vi nc: Khng mi, khng v; khng mu cng tm thi vo khong 0,72 mg ng lng/1lit cng vnh cu 0,26 0,72 mg ng lng/lit oxi ha 2 mg O2/lit Tng s VSV < 100 tbo /ml E.coli khng qu 3 tbo /l pH l 6,8 7,2

1. I VI NGUYN LIU:
b) i vi nc: - Hm lng mui cacbonat: 50ml/H2O - Hm lng mui Mg: 100ml/H2O - Hm lng mui clorua: 75 - 150ml/H2O - Hm lng CaSO4: 130 - 200ml/H2O - Hm lng Fe++: 0.3ml/H2O - NH3 v cc mui ca NO3-, NO2-

1. I VI NGUYN LIU:
c) i vi hoa bia: - Mu sc: cnh hoa phi vng c, khng c mu nu sm hoc en. V hoa sm b oxi ha nhiu, khng t c cht lng. - Mi: thm c trng, khng hc. - Phn: bc cnh hoa ra cn nhiu phn vng sng - m: 10-12% - Tp cht: khng ln l vo cun hoa

1. I VI NGUYN LIU:
d) i vi men bia: Tc ln men nhanh S dng ng c hiu qu to cn cao C kh nng chu cn, p sut thm thu, nhit , p sut, nng ph hp tng nh my C kh nng sng st cao ti s dng c tnh di truyn n nh Sn phm to ra c mi v v c trng cho bia

1. I VI NGUYN LIU:
e) i vi go: - Go phi trng, sch - T l ht c < 7% - T l ht np 2% - m:14,5 0,5% - T l ht tm 20%

2. XC NH HM LNG ETANOL (TCVN 5562:2009)

Cch tin hnh

Tch CO2 ra khi mu Lc dch bia Chun b bnh t trng Cn vo bnh sch 100g bia. Thm vo khong 20ml nc ct. Cho vo bnh hng 50-100ml nc ct. Kim tra kn ca h thng chng ct v lng nc lm lnh. Tin hnh chng ct Dch sau ct c gi 200C + 0,50C trong thi gian 30 pht . Xc nh t trng ca dch ct

2. XC NH HM LNG ETANOL (TCVN 5562:2009) Tnh kt qu:

T trng tng i ( d 20/200C) tnh theo cng thc:

d20/200C

m3 m1 = m2 m1

Trong : m1 : khi lng bnh t trng, g m2 : khi lng bnh t trng vi nc 200C, g m3 : khi lng bnh t trng vi dch nc ct 200C,g

2. XC NH HM LNG ETANOL (TCVN 5562:2009)

Hm lng etanol (WA ) tnh bng % khi lng Nu khi lng dch ct khng ng 100g th kt qu c nhn vi h s hiu chnh k tnh theo cng thc sau:

mD K= mB
Trong : MD : khi lng ca dch ct,g MB : khi lng ca mu bia,g Kt qu cui cng : l gi tr trung bnh cng, kt qu 2 php xc nh song song c tnh chnh xc n 0,01% cn. Chnh lch kt qu ca 2 php xc nh song song do cng mt ngi phn tch khng vt qu 0,06%.

3. XC NH CO2 BNG PHNG PHP CHUN

NGUYN TC: Bn cht phng php: phng php da vo phn ng ca cacbon ioxit c trong bia vi 1 th tch xt d to thnh mui natri cacbonat. Dng H2SO4 chun lng mui natri cacbonat ny, t tnh ra hm lng CO2 c trong bia.

Cch tin hnh 10ml bia vo pipet Vi git phenolphtalein 50 ml nc ct bnh tam gic 250ml

nh t t dd H2SO4 0,1 N

dd mt mu hng

Thm 1-3 git metyl da cam

DD mu vng Chun dd mu cam

4. PHNG PHP XC NH MU
(TCVN 5566:1991)
Phng php da trn c s so snh mu ca bia vi mu ca dung dch iod 0,1N vi nhng lng khc nhau trong 100ml nc ct.

4. PHNG PHP XC NH MU
(TCVN 5566:1991)
Xc nh mu bng phng php quang ph (TCVN 6061:2009) Tiu chun ny quy nh phng php xc nh mu ca bia bng quang ph.

5. PHNG PHP XC NH TC LNG BT THEO CH S SIGMA (TCVN 6062:1995)

Phm vi p dng: Tiu chun ny quy nh phng php xc nh tc lng bt ca bia theo phng php ch s sigma. Singma =
,( )
+

Trong : t: thi gian h bt (225230 giy) b: s ml bia thu c t bt trong thi gian t c: s ml bia t bt cn thi im t Bo co chnh xc n s nguyn.

6. PHNG PHP TH (PHNG PHP XC NH DIAXETIL V CC CHT DIXETON KHC) (TCVN 6058 : 1995, TCVN 6059 : 1995)
Nguyn tc:
Tch cht dixeton t bia bng chng ct. Cho phn ng phn

chng ct vi dung dch O-fenilendiamin v to thnh cht dn

xut ca quinoxalin. Axit ha v o quang ph cc cht thu c t phn ng. Tnh nng cc cht dixeton nh mt h s c xc nh qua cht chun

7. CC CH TIU CM QUAN (TCVN 6063 : 1995)

xc nh cht lng bia, tin hnh kim nghim cc ch tiu

sau: - trong v mu sc - Trang thi v bn ca bt - Mi - V

Bng cho im
Ch im tiu Trong v Mu Sc Trng thi v bn ca bt Bt nh, u, xp rt bn khi ln khi mt thong. Thi gian gi bt lu 5 4 3 Km trong, m 2 c d nhn , m 1 c, m hn hoc nht hn so

Trong sut, mu c trng Trong sut, hi m cho sn phm

hi nht so vi mu hoc nht hn so vi hn hoc nht hn so c trng ca sn phm Bt nh, u, xp bn khi ln khi mt thong. Thi gian gi bt kh lu

mu c trng ca vi mu c trng ca vi mu ca sn sn phm Bt nh u, xp, km bn khi ln khi mt thong sn pha73m Bt to, d v. Thi gian gi bt thp phm Rt t bt

Mi

Thm d chi, c trng cho sn phm c sn xut hon ton ha, khng c l mi l

Thm d chi nhng km c trng , mt mt cht, khng c mi l

Thm d chu. Xut Km thm, xut hin hin mi khuyt tt nh mi nng, chua

Rt t bt

Ha hp, m du, d chu

Ha hp, m du d

V mnh hn hoc V qu mnh hoc qu V qu mnh hoc nht hn v c trng mt cht. Xut hin v l nht khc xa nhiu so qu nht, khc

hon ton c trng cho v chu nhng c phn ca sn phm c sn xut hon ho km c trng

vi v c trng. V l nhiu so vi v c xut hin trng. V l rt r

8. PHNG PHP XC NH NG (TCVN 6059:1995)

Thuc th - 2,2,4- Trimetylpentan (isooctan) - Ancol octyl:Cho mt git ancol octyl vo 20ml isooctan tng hp th trong cuvet 1cm bc sng 275nm.

- Axit clohydric: dung dch 3M.

Tnh v biu th kt qu ng ca bia, X, tnh bng n v ng (BU), theo cng thc sau:

X=A275 x 50
Trong A275 l hp th o c bc sng 275nm. Ly kt qu chnh xc n 0,5 n v BU.

9. PHNG PHP XC NH HM LNG CHT HA TAN BAN U (TCVN 5565:1991)

Tin hnh xc nh - S dng dung dch cn li trong bnh ct sau khi ct 100g bia mu xc nh etanol. - Dung dch cn li trong bnh ct c lm ngui n nhit phng, thm nc ct vo cho bng lng cn ban u (100g 0,1g) lc u. a nhit dung dch v 200C bng my iu nhit v xc nh t trng ca dung dch.Trng hp thm nc ct b qu khi lng ban u, phi dng h s hiu chnh. - Tin hnh xc nh t trng ca dung dch Tnh kt qu - Hm lng cht chit thc (WN), tnh bng phn trm khi lng - Trng hp lng dung dch sau khi pha long c khi lng lch vi lng mu cn ban u th gi tr tht tm c trong bng phi nhn vi h s hiu chnh (K) theo cng thc: K=

m2 m1

(1)

Trong : + m1 : khi lng mu bia (g) + m2 : khi lng ton b dung dch pha long (g)

9. PHNG PHP XC NH HM LNG CHT HA TAN BAN U (TCVN 5565:1991)

- Hm lng cht ha tan ban u (Wp) tnh bng trm khi lng theo cng thc:
WD=
+,. +,.

Trong : : Hm lng etanol trong bia, % khi lng. : Hm lng cht chit thc trong bia, % khi lng. 2,0665: Hng s iu kin theo Baling (lng cht ha tan thc t to ra 1g ru etylic). 1,0665: Hng s iu kin theo Baling (lng cht ha tan thi ra khi to thnh 1g ru etylic).

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